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APS-1650 Automated Prep Station
Operator’s Manual
COPYRIGHT
Copyright 2009, 2014 Teledyne
Technologies Inc.
480148 Rev 2 February, 2014
REPRODUCTION
All rights reserved.
Reproduction or
transmission of this document in whole or
in part, and by any means without the
express written consent of the copyright
owner or authorized agent is prohibited.
Requests for additional copies of this, or
any other CETAC publication, can be
filled by contacting an authorized
distributor or
Teledyne CETAC Technologies
Customer Service & Support
14306 Industrial Road
Omaha, Nebraska 68144, USA
Phone
(800) 369-2822 (USA only)
Phone
(402) 733-2829
Fax
(402) 733-1932
E-mail [email protected]
Web
www.cetac.com
REVISIONS
Teledyne CETAC Technologies strives to
provide the scientific community with an
unparalleled combination of effective
technology
and
continuing
value.
Modular
upgrades
for
existing
instruments will continue to be a prime
consideration as designs progress.
Teledyne CETAC Technologies reserves
the right to revise this document and/or
improve products described herein at any
time without notice or obligation.
Warranty registration entitles the named
owner exclusively to manual change
pages/new editions as they are published.
SAFETY
Instruments, accessories, components or
other associated materials may not be
returned to CETAC if contaminated with
biohazard or radioactive materials,
infectious agents, or any other materials
and/or conditions that could constitute a
health or injury hazard to CETAC
employees. Call Customer Service and
Support if there is any question or doubt
relative to decontamination requirements.
CAUTION and WARNING statements, as
applied in this document, shall be
interpreted consistent with the following
context:
CAUTION applies only to
potential property damage conditions;
WARNING applies to potential personal
injury conditions, in combination with or
exclusive of potential property damage.
NOTE
All user-serviceable components are
specifically identified in this document as
such; the balance shall be assumed to
require the expertise of a factory service
technician/engineer
for
adjustment,
repair, replacement, modification, etc.
Others not so qualified and performing
these actions shall do so at their own risk.
Furthermore,
never
operate
the
instrument without first reading and
understanding the APS-1650 Operator’s
Manual and ensuring that it is operated
safely and properly.
ORIGINAL PACKAGING
Retain original factory packaging for
moves and factory return shipments.
Shipping in anything other than the
original fitted foam and container can
result in incidental damage from which
the purchaser will not be protected under
warranty.
APS-1650 Automated Prep Station Operator’s Manual Addendum
Notices and Compliance Declarations
FEDERAL COMMUNICATIONS
COMMISSION (FCC) NOTICE
This equipment has been tested and found
to comply with the limits for a Class A
digital device, pursuant to Part 15 of the
FCC Rules. These limits are designed to
provide reasonable protection against
harmful interference in a commercial
installation.
This equipment generates, uses, and can
radiate radio frequency energy and, if not
installed and used in accordance with the
instructions,
may
cause
harmful
interference to radio communications.
Operation of this equipment in a
residential environment is likely to cause
harmful interference, in which case the
user will be required to correct the
interference at his own expense.
MODIFICATIONS
The FCC requires the user to be notified
that any changes or modifications made to
this device that are not expressly
approved by CETAC may void the user's
authority to operate the equipment.
CABLES
Connections to this device must be made
with shielded cables with metallic
RFI/EMI connector hoods to maintain
compliance
with
FCC
Rules
and
Regulations.
CANADIAN NOTICE
This digital apparatus does not exceed the
Class A limits for radio noise emissions
from digital apparatus as set out in the
interference-causing equipment standard
entitled "Digital Apparatus." ICES-001 of
the Department of Communications.
AVIS CANADIEN
Cet appareil numerique respecte les
limites
de
bruits
radioelectriques
applicables aux appareils numeriques de
Classe A prescrites dans la norme sur le
materiel
brouilleur:
"Appareils
Numeriques," NMB-001 edictee par le
ministre des Communications.
POWER CORD SET REQUIREMENTS
The power cord set supplied with your
instrument meets the requirements of the
country where you purchased the
instrument.
If you use the instrument in another
country, you must use a power cord set
that meets the requirements of that
country.
AD-1
APS-1650 Automated Prep Station Operator’s Manual Addendum
Notices and Compliance Declarations
This equipment is designed for connection to a grounded
(earthed) outlet. The grounding type plug is an important safety
feature. To reduce the risk of electrical shock or damage to the
instrument, do not disable this feature.
CAUTION
To reduce the risk of fire hazard and electrical shock, do not expose the
unit to rain or humidity. To reduce the risk of electrical shock, do not
open the cabinet. All maintenance is to be performed by an Authorized
CETAC Service Provider.
Protection provided by the equipment may be impaired if the equipment
is used in a manner not specified by the manufacturer.
CLEANING INSTRUCTIONS
To clean the exterior surfaces of the instrument, complete the following steps:
1 Shut down and unplug the instrument.
2 Wipe the instrument exterior surfaces
only using a towel dampened with a
lab-grade cleaning agent.
3 Repeat step 2, using a towel dampened
with clear water.
4 Dry the instrument exterior using a dry
towel.
Do not allow any liquid to enter the instrument cabinet, or come
into contact with any electrical components. The instrument
must be thoroughly dry before you reconnect power, or turn the
instrument on.
ENVIRONMENTAL
Operating Temperature:
Relative Humidity
Altitude
AD-2
10° to 30 C
0% to 95%
0 to 10000 Ft
APS-1650 Automated Prep Station Operator’s Manual Addendum
Notices and Compliance Declarations
AVERTISSEMEN T
POUR UN E PROTECTION CON TIN UÉ
CON TRE LES RISQUES D’IN CEN DIE,
REMPLACER UN IQUEMEN T PAR DES
FUSIBLES DE MÊME TYPE ET
AMPÈRAGE.
AVERTISSEMEN T
TOUT CON TACT AVEC LES H AUTES
TEN SION S PEUT EN TRAIN ER LA MORT
OU DES BLESSURES SÉVÈRES. CE
PAN N EAU N E DOIT ÊTRE EN LEVE QUE
PAR UN RÉPARATEUR QUALIFIÉ.
AVERTISSEMEN T
TOUT CON TACT AVEC LES H AUTES
TEN SION S PEUT EN TRAIN ER LA MORT
OU DES BLESSURES SÉVÈRES. CE
PAN N EAU N E DOIT ÊTRE EN LEVE QUE
PAR UN RÉPARATEUR QUALIFIÉ.
AVERTISSEMEN T
AVERTISSEMEN T
TOUT CON TACT AVEC LES H AUTES
TEN SION S PEUT EN TRAIN ER LA MORT
OU DES BLESSURES SÉVÈRES. CE
PAN N EAU N E DOIT ÊTRE EN LEVE QUE
PAR UN RÉPARATEUR QUALIFIÉ.
TOUT CON TACT AVEC LES H AUTES
TEN SION S PEUT EN TRAIN ER LA MORT
OU DES BLESSURES SÉVÈRES. CE
PAN N EAU N E DOIT ÊTRE EN LEVE QUE
PAR UN RÉPARATEUR QUALIFIÉ.
AD-3
APS-1650 Automated Prep Station Operator’s Manual Addendum
Notices and Compliance Declarations
WARN IN G
H IGH LEAKAGE CURREN T EN SURE PROPER GROUN DIN G
AVERTISSEMEN T
COURAN T DE FUITE ÉLEVÉ — FORN IR
UN E MISE À LA TERRE EFFICACE.
Crush Hazard / Pinch Point – Keep hands clear
of moving parts. X, Y, Z axis movement may
crush hand.
Puncture Hazard – Moving parts can cause
severe injury. Do not put hand under the
probe assembly!
Lifting Hazard – Single person lift could cause
injury. Use assistance when moving or lifting.
Attention – Refer to the manual. This symbol
indicates that information about usage of a
feature is contained in the manual.
AD-4
APS-1650 Automated Prep Station Operator’s Manual Addendum
Notices and Compliance Declarations
WARNING
If the automated prep station is used in a manner not specified by
CETAC Technologies, the protection provided the equipment may be
impaired.
WARNING
The power switchs on the rear panels are not the mains disconnect.
Mains disconnect is accomplished by disconnecting the detachable power
supply cords at the appliance coupler or at the mains plug. Ensure the
power cords are easily accessible and removable, in the event of an
emergency, which requires immediate disconnection.
CAUTION
The CAUTION notice denotes a hazard. It calls attention to a procedure,
practice, or the like, that, if not correctly performed or adhered to, could
result in personal injury. Do not proceed beyond a CAUTION notice
until the indicated conditions are fully understood, and met.
WARNING
This is a Safety Class 1 Product (provided with a protective earthing
ground incorporated in the power cord). The mains plug shall only be
inserted in a socket-outlet provided with a protective earth contact.
Intentional interruption is prohibited.
Safety Maintenance
The operator should check the detachable power supply cord condition.
The equipment should not be operated if the mains inlet is cracked or
broken. Any obvious damage to the case, (from a drop or fall), should be
checked by service personnel for loose or damaged parts. See individual
parts lists for approved replacement parts.
AD-5
APS-1650 Automated Prep Station Operator’s Manual Addendum
Notices and Compliance Declarations
Safety and Regulatory Information
Review this product and related documentation to familiarize with
safety markings and instructions before you operate the instrument.
WARNING
The WARNING notice denotes a hazard. It calls attention to a
procedure, practice, or the like, that, if not correctly performed or
adhered to, could result in personal injury. Do not proceed beyond a
WARNING notice until the indicated conditions are fully understood
and met.
WARN IN G
Do not operate in explosive atmosphere.
WARN IN G
All external I/O terminals allow a maximum current of 150 mA @
28V.
.
WARN IN G
Ensure that power is disconnected before removal of any covers.
WARN IN G
Equipment is not intended for wet locations. Miscellaneous liquids in
the equipment could cause hazardous conditions.
WARN IN G
Pollution Degree – 1.
NOTE: For instructions on how to return end-of-life
equipment, producer-supplied electrical accessories, or
auxiliary items for proper disposal please contact the
supplier or importer. In the event a supplier cannot be
reached, contact CETAC Technologies customer service
department at 1 (800) 369 2822.
AD-6
Contents
APS-1650 Automated Preparation System Operator’s Manual
Contents
Contents
Preface
xiii
Who Should Read This Book
xiii
How to Use This Book
xiii
Conventions Used in This Book
xiv
Instructions
Menu Items
Terminology
Notes
Cautions
Warnings
xiv
xv
xv
xvi
xvi
xvi
Where to Go for More Information
1 Introduction
Automated Prep Station Standard Components
Rack Adapter Plate
Sample Vial Rack
Collection Vial Rack
Flowing Rinse Station
Z-Drive Assembly
3-Channel Peristaltic Pump
RS/232 Serial I/O Ports
Multi-Channel Auxiliary Port
xvii
1----3
1---4
1-5
1-6
1-6
1-6
1-6
1-8
1-8
1-8
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APS-1650 Automated Prep Station Operator’s Manual
Contents
USB Communications Port
Stirrer Speed Control
Pump Speed Control
Auxiliary Speed Control
Liquid Level Sensor
External Desktop Power Supply --- Main
External Desktop Power Supply --- Pump Module
Sample Probe Kit
Sample Stirring Kit
USB Communications Cable
Rinse Station Tubing Kit
Pump Module Box
Pump Module Tubing Kit
Software CD
1-8
1-8
1-8
1-8
1-9
1-9
1-9
1-9
1-9
1-9
1-9
1-9
1-9
1-10
Optional Accessories
1-10
Serial Interface Null Adapter
Serial Interface Special Adapter Kit
Sample Probes
Serial Interface Kit
1-10
1-10
1-10
1-10
2 Preparing for Installation
2----3
Choosing a Location
2---3
Space Requirements
Rinse Solution Requirements
Power Requirements
2---3
2---3
2---4
Unpacking the APS-1650
2---5
3 Installing the Automated Prep Station
viii
3----3
APS-1650 Automated Preparation System Operator’s Manual
Contents
Shipping Fixture Process
3---3
Mounting the Z-Drive Assembly
3---4
Attaching the Z-Drive Assembly
3---4
Attaching the Z-Drive Cable
3---5
3-Channel Peristaltic Pump
3---6
Connecting the Rinse Station
3---6
Connecting the Pump Module Box
3---8
Installation / Removal of the Stirring Paddle
3---11
Installation / Removal of the Stirring Assembly
3---11
Installation / Removal of the Sample Probe
3---11
Emptying the Drip Cup
3---12
Placing the Sample and Collection Racks
3---12
Establishing External Connections
3---13
Connecting the APS-1650 to the Power Source
Connecting the APS-1650 to an Analytical Instrument
3---13
3---13
Connecting the APS-1650 to the Host Computer
3---13
Establishing a Serial Communications Interface
3---14
Establishing a USB Communications Interface
3---14
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APS-1650 Automated Prep Station Operator’s Manual
Contents
Determining the COM Port
3---15
Installing the Instruo Software
3---16
Calibrating the Liquid Level Sensor
3---16
4 Verifying Installation
4----3
Testing the Interface
4---3
Checking the Automated Prep Station Components
4---8
Testing the Sample Probe
4---9
5 Using the Automated Prep Station
5----3
Establishing Optimal Operating Conditions
5---3
Creating the Lab Environment
Replacing Automated Prep Station Components
Purchasing Supplies
5---4
5---5
5---5
Arranging the Sample Vial Racks
5---6
Starting the Automated Prep Station
5---6
Shutting Down the Automated Prep Station
5---7
Flushing the Rinse Station and Flow Path
5---8
x
APS-1650 Automated Preparation System Operator’s Manual
Contents
6 Maintaining the Automated Prep Station
6----3
Cleaning the Automated Prep Station
6---3
Daily External Cleaning
Weekly Cleaning
6---4
6---4
Checking for Leaks
6---6
Replacing Peristaltic Pump Tubing
6---7
Replacing the Sample Probe
6---7
Replacing the Rinse Station Tubing
6---8
7 Troubleshooting the Automated Prep Station
7----3
Power System Problems
7---3
Interface Problems
7---4
RS-232 Cable Problems
Software Configuration Problems
7---4
7---4
Z-Drive Assembly Problems
7-5
Drip Cup Problems
7-7
DIP Switch Settings
7-8
xi
APS-1650 Automated Prep Station Operator’s Manual
Contents
xii
Preface
APS-1650 Automated Prep Station Operator’s Manual
Preface
Preface
The APS-1650 Automated Prep Station Operator’s Manual explains the
procedures for installing, using, and maintaining the CETAC APS-1650.
It also provides information about troubleshooting APS-1650 problems
and describes the design of the automated prep station.
Who Should Read This Book
The primary audience for the APS-1650 Automated Prep Station
Operator’s Manual consists of analytical chemists and lab technicians.
To use this manual effectively, you should have a basic knowledge of
chemistry, a basic knowledge of electronic sampling equipment, and at
least a beginning level of computer experience.
How to Use This Book
The APS-1650 Automated Prep Station Operator’s Manual contains
seven chapters. You should read the chapters sequentially the first
time. Thereafter, refer to the chapters separately as needed. The first
chapter provides an introduction to the autosampler. Subsequent
chapters detail the primary tasks associated with the APS-1650.
This manual contains the following chapters:
Chapter 1, “Introduction,” provides you with an overview of the APS1650 Automated Prep Stations’s function and design.
Chapter 2, “Preparing for Installation,” discusses space and power
requirements that must be met before the APS-1650 is installed. It also
provides instructions for unpacking the autosampler.
xiii
APS-1650 Automated Prep Station Operator’s Manual
Preface
Chapter 3, “Installing the Automated Prep Station,” provides stepby-step procedures for installing the APS-1650 and connecting it to the
host computer.
Chapter 4, “Verifying Installation,” explains how to test the
communications interface between the APS-1650 and the host computer.
It also explains how to check autosampler components and test the
sample probe.
Chapter 5, “Using the Automated Prep Station,” describes the
tasks you perform during daily operation of the APS-1650.
Chapter 6, “Maintaining the Automated Prep Station,” explains
daily, weekly, and periodic maintenance tasks.
Chapter 7, “Troubleshooting the Automated Prep Station,”
describes how to diagnose and correct APS-1650 problems.
These chapters are followed by a glossary of related terms.
Conventions Used in This Book
This book uses certain conventions to distinguish different types of
information easily. This section describes these conventions.
Instructions
All step-by-step instructions are numbered and in bold, as in the
following example.
1) Replace the sample vial racks.
Many numbered instructions are followed by more detailed
explanations.
xiv
APS-1650 Automated Prep Station Operator’s Manual
Preface
Menu Items
This book uses the following format for referring to menu items:
Settings/Communication
The text before the forward slash symbol is the name of the menu; the
text after the forward slash symbol is the menu choice. This example
refers to the Communications Menu choice in the Settings Menu.
Terminology
This book frequently uses the following terms:
Host Computer The computer that controls operation of the CETAC
device.
Hz
Hertz.
ICP-AES
An inductively coupled plasma atomic emission
spectrometer.
ICP-MS
An inductively coupled plasma mass spectrometer.
ID
Inside diameter.
LED
Light-emitting diode.
PEEK
Polyetheretherketone.
VAC
Volts alternating current.
VDC
Volts direct current.
X-Axis
The left-to-right axis of the autosampler.
xv
APS-1650 Automated Prep Station Operator’s Manual
Preface
Y-Axis
The front-to-back axis of the autosampler.
Z-Axis
The up-and-down axis of the sample probe.
W-Axis
The up-and-down axis of the stirring paddle.
Notes
Notes contain a reminder about the effect of particular actions. They
are indicated as follows:
Note:
This example shows how a note is displayed.
Cautions
Cautions indicate situations that require immediate attention to prevent
harm to the autosampler. Cautions are indicated as follows:
CAUTION
This example shows how a caution is displayed.
Warnings
Warnings indicate situations that could cause bodily harm. Warnings
are indicated as follows:
WARNING
This example shows how a warning is displayed.
xvi
APS-1650 Automated Prep Station Operator’s Manual
Preface
Where to Go for More Information
In addition to the APS-1650 Autosampler Operator’s Manual, you can
refer to the following resources:
•
The software manual for the ICP-AES or ICP-MS instrument you
are using
•
CETAC Technologies Customer Service and Support:
Toll Free: 1 (800) 369-2822
Direct:
1 (402) 733-2829
Fax :
1 (402) 733-1932
E-mail:
[email protected]
Web:
www.cetac.com
xvii
APS-1650 Automated Prep Station Operator’s Manual
Preface
xviii
1
Introduction
APS-1650 Automated Prep Station Operator’s Manual
Introduction
1–2
APS-1650 Automated Prep Station Operator’s Manual
Introduction
Introduction
The APS-1650 Automated Prep Station is designed to be sturdy, reliable,
and easy to use. It provides automated sample dilution that enables you
to perform other tasks while the APS-1650 operates. The APS-1650
automatically dilutes and stirs up to 90 samples when fully loaded. It
contains a microprocessor that allows sequential or random sampling,
providing flexibility.
The APS-1650 System is typically controlled by a host computer using a
serial communications protocol. The computer may be user supplied or
acquired from CETAC. Computer requirements are given later in this
chapter. A picture of an APS-1650 System (Autosampler plus Dilution
Module) is shown below in Figure 1-1.
Figure 1–1. APS-1650 Automated Prep Station—Front View.
1–3
APS-1650 Automated Prep Station Operator’s Manual
Introduction
Automated Prep Station Standard
Components
Automated Prep Station components are made of corrosion-resistant
stainless steel alloys or anodized aluminum. The enclosure and base are
made from a high-strength aluminum alloy that is chromated and
finished with an epoxy powder coating.
The APS-1650 operates reliably under a wide variety of conditions.
Components
in
the
sample
flow
path
are
made
of
Polytetrafluoroethylene (PTFE), Polyurethane, and PEEK. When these
inert, non-metallic materials are used at temperatures less than 135°C,
they can withstand repeated exposure to the following substances:
•
1–4
Petroleum oils and derived fuels, kerosene, and hexane.
APS-1650 Automated Prep Station Operator’s Manual
Introduction
Figure 1–2. APS-1650 Diagram—Front View.
The following standard components are located on the front of the APS1650 and are shipped with the Automated Prep Station. Each item
corresponds with a callout in Figure 1–2.
1) Rack Adapter Plate. The sample tray accommodates one raw
sample rack and one diluted sample rack. The sample tray sits on
1–5
APS-1650 Automated Prep Station Operator’s Manual
Introduction
pegs located in the base unit. The sample tray is removable to allow
for easy clean-up.
2) Sample Vial Rack. The sample vial rack holds the raw samples.
Depending upon which version of the APS-1650 was purchased, the
standard rack configuration will include. a) One 45 position sample
rack. b) One 80 position sample rack. c) One 90 position sample rack.
Custom rack configurations can be used if desired. See the Instruo
Software manual for information on creating custom rack files.
3) Collection Vial Racks. The collection vial rack holds the prepared
samples. Depending upon which version of the APS-1650 was
purchased, the rack configuration will include a) One 80 position
collection rack, or b) One 90 position collection rack. Additional
racks can be purchased separately. Custom rack configurations can
be used if desired. See the Instruo Software manual for information
on creating custom rack files.
4) Flowing Rinse Station. The rinse station is located in the middle
of the chassis at the back of the sample base between the sample
and collection racks. It comes with tubing used to connect the rinse
station to the rinse source and the waste container. The rinse station
block includes rinse ports for both the sample probe and the stirring
paddle.
5) Z-Drive Assembly. The Z-Drive assembly includes a Z-Axis and WAxis motor assemblies. The Z-Axis holds the sample probe. The WAxis holds the stirrer assembly.
Note: Stirrer assembly is optional and may not be included in all
models
1–6
APS-1650 Automated Prep Station Operator’s Manual
Introduction
Figure 1–2. APS-1650 Automated Prep Station—Back View.
1–7
APS-1650 Automated Prep Station Operator’s Manual
Introduction
The following standard components are located on the back of the APS1650 and are shipped with the Automated Prep Station. Each item
corresponds with a callout in Figure 1---2.
6) On-board three channel peristaltic pump. The APS-1650 will be
standard with one on-board peristaltic pump. The pump is located in
the lower right-hand corner on the back of the Automated Prep
Station. The pump moves the rinse solution from the rinse source
through the flowing rinse station. In a typical installation, a gravity
drain is used to move the solution from the rinse station to waste.
7) Two RS-232 Serial I/O Ports (COM1 and COM2). The serial
ports are located on the left side at the back of the Automated Prep
Station. The COM1 port is an alternative communications interface
between the APS-1650 and the host computer. The COM2 port
connects the Automated Prep Station to other external devices.
8) Multi-channel (I/O) Auxiliary Port. The auxiliary port is located
on the back, in the center of the APS-1650. The auxiliary port is
used to connect the Automated Prep Station to other external
devices.
9) USB Communications Port. The APS-1650 comes standard with
a USB communications port. This port is the standard way to
interface the APS-1650 with the host computer.
10) Stirrer Speed Control. The Stirrer speed is controlled by software.
It should be set to ‘default’.
11) Pump Speed Control. The pump speed is controlled by software.
It should be set to ‘default’.
12) Auxiliary Speed Control. The auxiliary speed control is used with
the auxiliary peristaltic pump not included with the APS-1650. It
should be set to ‘default’.
1---8
APS-1650 Automated Prep Station Operator’s Manual
Introduction
13) Liquid Level Sensor. The liquid level sensor is an optical sensor
used to determine the level of the raw sample. When properly
calibrated the sensor prevents the probe from going to deep into the
sample; reducing the amount of rinse required.
The following standard components are also shipped with the APS-1650:
o
External Desktop Power Supply - Main. The input rating is AC
100V-240V, 3.2 A, with an output of DC 28V, maximum 4.6 A.
o
External Desktop Power Supply ---- Pump Module. The input
rating is AC 100V-240V, 1.9 A, with an output of DC 24V, maximum
3.33 A.
o
Sample Probe Kit. The kit includes the sample probe. The sample
probe ships in the Z-Drive assembly.
o
Sample Stirring Kit (Optional). The kit includes the sample
stirrer. The sample stirrer ships in the Z-Drive assembly.
o
USB Communications Cable. The APS-1650 uses a USB cable for
communication with the host computer.
•
Rinse Station Tubing Kit. The kit includes rinse tubing, drain
tubing, and peristaltic pump tubing required for operation of the
flowing rinse station.
•
Pump Module Box. The pump module box houses the syringe
pump, air pump, rinse pump, and solenoid valve used for sample
preparation. The module can be connected through USB or Serial
interface.
•
Pump Module Tubing Kit. The kit includes tubing, connectors,
filters, and sipper tubing for the pump module box to perform
sample preparation.
1---9
APS-1650 Automated Prep Station Operator’s Manual
Introduction
•
Software CD. The software CD contains this Operator’s Manual,
the Spare Parts catalog, Instruo Software used for operating the
APS-1650, alignment software, USB drivers, and additional
documentation.
Optional Accessories
If you are doing a specialized type of analysis or are connecting the APS1650 to a host computer that uses a non-RS-232 communications
protocol, you may need optional accessories in addition to the standard
components included with the Automated Prep Station. The following
accessories are available for the APS-1650:
o
Serial Interface Null Adapter. The null adapter replaces one
DB9F port adapter at the host computer. It is used for computers
with DCE-AT style serial ports.
o
Serial Interface Special Adapter Kit. The adapter kit replaces
one or both standard serial port adapters with unwired DB9M,
DB25M, and DB25F adapters for special applications or host
computers with serial ports not conforming to the RS-232 standard.
o
Serial Interface Kit. The kit includes two DB9F port adapters for
host computers with normal AT-style DTE serial ports, and a
1.828-meter modular cable.
o
Sample probes. The APS-1650 ships standard with a bevel tipped
stainless-steel sample probe. Early versions of the APS-1650 may
have shipped with a square tipped probe.
1---10
APS-1650 Automated Prep Station Operator’s Manual
Introduction
Note: Contact CETAC Technologies if you need additional accessories
not listed, need added features to integrate the APS-1650 Automated
Prep Station into your application, or have unique requirements.
Research and development of new features and accessories for the APS1650 Automated Prep Station, often inspired by customer requests, is a
continuing activity at CETAC Technologies.
1–11
2
Preparing for Installation
APS-1650 Automate Prep Station Operator’s Manual
Preparing for Installation
Preparing for Installation
Installing the APS-1650 requires preparation. Before you install the
automated prep station, you should evaluate the physical arrangement
of the laboratory to choose a suitable location. Once you choose a
location, you must carefully unpack the automated prep station prior to
beginning the installation.
This chapter discusses what requirements must be met when you choose
a location for the autosampler. It also describes how to unpack the APS1650 before installation.
Choosing a Location
Choosing a location for the APS-1650 involves evaluating the lab
environment for the availability of space and power. For the automated
prep station to function optimally, the location you select must meet
specific requirements associated with each of these items. The following
sections discuss space and power requirements.
Space Requirements
The recommended minimum footprint for countertop installation of the
APS-1650 including the Pump Module Box is 110 x 70 x 70 centimeters.
When evaluating a location, keep in mind rinse solution, diluents, and
waste containers and host computer positioning. The APS-1650 will also
need two grounded electrical outlets within 1.2 meters.
Rinse Solution Requirements
For most applications, kerosene is used for rinse agent in the APS-1650.
Place the rinse agent source within two meters of the APS-1650.
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APS-1650 Automated Prep Station Operator’s Manual
Preparing for Installation
Ensure that there is a liquid waste receptacle within two meters of the
APS-1650. The waste receptacle inlet should be at least 30 to 60
centimeters lower than the autosampler rinse station outlet to ensure
proper gravity drainage.
Power Requirements
Place the APS-1650 within 1.2 meters of a power outlet. The APS-1650
uses two external desktop power supplies. The input rating for the main
power supply is AC 100V-240V 3.2 A with an output of DC 28V,
maximum 4.6 A. The input rating for the pump module box power
supply is AC 100V-240V 1.9 A with an output of DC 24V, maximum 3.3
A.
Ensure that you position the APS-1650 so that the location where the
power supply cord plugs into it is easily accessible (is not blocked) and
can be quickly disconnected if needed.
The power supply socket is on the back of both the automated prep
station and the pump module box near the power switch. Connect the
power supplies to the unit first and then connect a line cord to the power
supply. Do not apply power to the power supply until ready to operate.
WARNING
The APS-1650 is intended to operate from an AC power source
that will not apply more than 240V AC between the supply
conductors and ground. A protective ground connection by way
of the grounding connector in the power cord is required for
safe operation.
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Preparing for Installation
Unpacking the APS-1650 Automated Prep
Station
The APS-1650 is shipped in a wooden crate to minimize damage during
shipment. Supplies and accessories are shipped in a second cardboard
box banded on top of the wooden crate.
If the APS-1650 is shipped or removed from storage during cold
weather, allow the packaged equipment to attain room temperature
before opening and exposing to warm, humid air. It is usually sufficient
to provide four to eight hours for this purpose.
CAUTION
If condensation forms on or inside the automated preparation station,
allow it to dry thoroughly before connecting it to a power source and
operating it. Failure to do so may cause equipment damage.
Note: Do not throw away the factory packaging. Keep it for possible
future use. This is one of the warranty conditions.
Inspect external packaging upon receipt for holes, tears, smashed
corners, or any other outward signs of damage from rough handling or
abuse during shipment. Inspect all items during unpacking and notify
the carrier immediately of any concealed damage.
Remove the crate cover by removing the screws marked with red circles.
There are typically eight screws holding the cover in place. Save the
screws and cover for future use.
Inside the crate there will be multiple cardboard boxes and bags
containing additional items. Remove these and set aside.
Locate the packing checklist from the shipping container, and check off
items against it. Leave accessories in the packing until you are ready to
install them on the automated prep station.
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Preparing for Installation
Once the packing checklist has been verified, remove the base unit from
the crate and set on the surface planned for operation.
WARNING
The APS-1650 base unit weighs approx. 30 kg or 66 lbs. Two
people are required to lift the unit. Always use proper form
when lifting.
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3
Installing the Automated
Prep Station
APS-1650 Automated Prep Station Operator’s Manual
Installing the APS-1650
Installing the APS-1650
The APS-1650 Automated Prep Station is designed for easy installation.
Installation consists of two parts: assembling the automated prep
station and connecting it to the host analytical instrument.
The APS-1650 can be installed with minimal effort. The only items that
will be needed are a Ball Point Allen Wrench set, which is included in
the APS-1650 kit, and a screwdriver. You can remove thumbscrews with
tools if necessary, but do not tighten them with anything other than
your fingers.
To install the automated prep station, you must complete the following
tasks. Each of these tasks will be discussed in detail later in this
chapter.
1) Removal of carriage shipping fixture.
2) Mounting the Z-Drive assembly.
3) Connect the rinse station.
4) Assemble the sample vial racks.
5) Establish external connections.
6) Connect the autosampler to the host computer.
WARNING
The APS-1650 base unit weighs approx. 30 kg or 66 lbs. Two
people are required to lift the unit. Lifting should be done with
a person situated on either side of the instrument.
Ensure the AC power is off before proceeding with installation.
Shipping Fixture Process
Depending on when the APS-1650 was shipped, there may, or may not
be a fixture securing the Y-Arm during shipment. If the unit has a
shipping fixture, it is an ‘Y’ shaped bracket holding the Y-Arm in the far
left position. Using a Philips screwdriver, remove the screw, remove the
bracket, and replace the screw. The bracket should be stored with the
packaging for future use.
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Figure 3-1
Shipping Fixture in place
Mounting the Z-Drive Assembly
The Z-Drive assembly must be attached to the autosampler arm to allow
movement and function of the sample probe. Figure 3-1 illustrates the
Z-Drive assembly components.
Attaching the Z-Drive
Autosampler Arm
Assembly
to
the
1) Carefully unpack the Z-Drive assembly.
2) Identify the four screws and the Allen Wrench.
3) Located the two mounting pins on the assembly.
4) Place the pins in the corresponding holes in the mounting
block, while holding it stable.
5) Insert the screws one at a time, while continuing to hold the
assembly stable.
6) Be careful not to tighten the screws too much.
Note: The screws are going into plastic and the plastic threads can be
easily stripped if the screw is tightened too much.
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APS-1650 Automated Prep Station Operator’s Manual
Installing the APS-1650
Figure 3-2
Mounting of Z-Drive Assembly
Installation of the Z-Drive 15-Pin Cable
1) Attach the end without the ferrite block to the 15-pin
connection port on the back of the Z-Drive assembly and
tighten screws.
2) Attach the end with the ferrite block to the 15-pin
connection port on the rear (in the center) of the unit, and
tighten the screws.
Warning: The Z-Drive 15-Pin Cable must be connected before applying
power to the unit. Connecting or disconnecting the Z-Drive cable while
power is applied WILL cause catastrophic damage to the unit and
possibly harm the user.
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APS-1650 Automated Prep Station Operator’s Manual
Installing the APS-1650
Single 3-Channel Peristaltic Pump
The APS-1650 is equipped with a 3-channel peristaltic pump on the
back side of the unit. In a typical installation one channel of the pump
is used to move rinse solution into the flowing rinse station. Gravity
drain is typical, but the additional channels can be used for a pumped
drain setup if desired.
Connecting the Rinse Station
The cabinet-mounted rinse station is located to the right of center on the
chassis. Typically, a solution from the kerosene family is used as the
rinse solution and is pumped into the rinse station by the on-board 3channel peristaltic pump.
Since the inlet of the rinse station is at the bottom of the rinse station,
the rinse solution flows from the bottom to the top of the stirrer paddle
reservoir. Up-flow rinsing is the most effective method for
decontaminating the stirrer paddle between samples. Reversing the
connections and the rinse solution flow reduces the effectiveness of the
rinse station and can cause cross-contamination and unsatisfactory
performance.
The rinse solution flows from the stirrer paddle reservoir to the drain
(rinse out) reservoir within the rinse station. The waste rinse then
drains from the rinse station by means of a gravity drain which is the
standard arrangement for draining the rinse station.
The sample probe is also rinsed within the rinse station, but the rinse
solution used to cleanse the probe is pumped from the pump module box
through the probe. The rinse solution is combined with air bubbles to
create a scrubbing effect for more efficient rinse inside the probe. The
rinse solution and air bubbles are forced through the probe into the
small opening in the rinse station which is then forced up around the
probe to cleanse the external surface prior to overflowing into the drain
(rinse out) reservoir within the rinse station.
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To connect the rinse station, complete the following steps and refer to
Figure 3-2:
Note: Portions of the tubing assembly described in steps 1-5 below may
have been completed in advance at the factory.
1) Connect the rinse solution to the on-board peristaltic pump
tubing (Figure 3-3)
a) Connect the 42 inch (107 cm) length of 1/8 inch (3.2 mm) ID
Superthane® tubing to the top inside channel of the Viton®
pump tubing.
Note: Superthane® tubing is rigid and can be hard to connect.
To aide in making good connections, slightly stretch the tubing
using needle nose pliers. Dip the tip of the connector in
isopropyl alcohol to lubricate before making the connection.
Press the tubing into the connector in one fluid motion.
b) Insert the 18 inch (46 cm) Sipper tube to the other end. The
sipper tube can now be inserted into the rinse solution
container.
2) Connect the peristaltic pump to the rinse station (Figure 3-3)
a) Connect the 42 inch (107 cm) length of 3/16 inch (4.7 mm)
Superthane® tubing to the bottom inside channel of the Viton®
pump tubing.
b) The rinse station is attached to the chassis by a bracket. It must
be removed to attach the rinse tubing. Remove the rinse station
from the bracket by removing the thumbscrew.
c)
The APS-1650 has a removable rack adapter tray. Lift the tray
out of the base and set aside.
d) Route the rinse tubing through the top hole on the left side of
the base pan to the rinse station. Connect the tubing to the
rinse in port of the rinse station. (Port Y in Figure 3-2)
e) The tubing can be trimmed to length if desired.
3) Connect the drain (rinse out) side of the rinse station to the
waste reservoir (Figure 3-3)
a) Connect the 66 inch (168 cm) length of 3/16 inch (4.7 mm)
Superthane® tubing to the drain (rinse out) channel of the rinse
station. (Port AA in Figure 3-2)
b) The waste container can be located on either side of the APS1650. The shortest distance to the waste container will produce
the best results. Route the drain tubing through the bottom hole
in the base pan nearest to the waste container. Trim the tubing
so it easily reaches the waste container, but will remain above
the fluid level. Insert the end into the waste container.
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Installing the APS-1650
c)
Attach the rinse station to the mounting bracket using the
thumb screw. Ensure the tubing is routed low in the base pan
up against the chassis.
d) Replace the rack tray ensuring the tubing is not pinched and the
tray is fully seated.
Connecting the Pump Module Box
The Pump Module Box can be positioned to the left or the right of the
base unit. When deciding on a position, keep in mind positioning of the
rinse solution container, diluent container, and electrical outlets.
Note: Portions of the tubing assembly may have been assembled in
advance at the factory.
1) Connect the air tubing (Figure 3-3)
a) Locate the peek 4-way fitting and attach it to the Z-Drive using
the two 3/32 inch allen screws and allen wrench provided. The
check valves should be pointed to the front and rear of the unit.
The top and bottom ports should not have check valves attached.
b) Connect the 54 inch length of green peek tubing to the “Air Out”
port on the Pump Module Box.
Note: The tubing should stick out past the end of the ferrule
when making the connections of the air tubing. If the air line is
flush with the ferrule air leaks will occur causing poor rinse and
an increase in carryover.
c)
Connect the other end of the peek tubing to the rear port on the
peek 4-way fitting on the Z-Drive.
2) Connect the rinse out tubing (Figure 3-3)
a) Connect the 4 inch (10 cm) length of polyurethane tubing to the
“Rinse Out” port on the Pump Module Box. Connect the other
end of the tubing to one of the top ports in the Tee-fitting.
b) Connect the 60 inch (152 cm) length of polyurethane tubing to
the other top port of the Tee-fitting. Connect the other end of
the tubing to the front port on the peek 4-way fitting on the ZDrive.
c)
3–8
Connect the 36 inch (91 cm) length of Superthane® tubing to the
bottom port of the Tee-fitting. Connect the other end to the 18
inch sipper tube. This tube can be placed in the rinse solution
container.
APS-1650 Automated Prep Station Operator’s Manual
Installing the APS-1650
3) Connect the rinse in tubing (Figure 3-3)
a) Connect the 36 inch (91 cm) length of Superthane® tubing to the
“Rinse In” port on the Pump Module Box. Connect the other end
to the ‘out’ port on the red in-line liquid filter.
b) Using a 1 inch (2.54 cm) length of Superthane® tubing, connect
the ‘in’ port on the in-line liquid filter to the 18 inch (46 cm)
sipper tube. This tube can be placed in the rinse solution.
4) Connect the diluent (Figure 3-3)
a) Connect the 36 inch (91 cm) length of Superthane® tubing to the
right port of the syringe pump valve. Connect the other end of
the tubing to the 18 inch sipper tube. This tube can be placed in
the diluent container.
b) Connect the 62 inch (158 cm) length of polyurethane tubing to
the left port of the syringe pump valve. Connect the other end of
the tubing to the the bottom port on the peek 4-way fitting on
the Z-Drive.
5) Connect the probe (Figure 3-3)
a) Connect the 8-5/8 inch (22 cm) length of polyurethane tubing to
the top port of the 4-way fitting on the Z-Drive. Connect the
other end of the tubing to the bevel tipped probe.
AA
DD
EE
GG
JJ
N
Rinse Station Drain
Tee-Fitting
In-Line Liquid Filter
Restrictor Sapphire
Check Valve (Outlet
Superthane Tubing
Table 3-1
R
S
T
X
Y
Z
4-Way Fitting
Check Valve (Inlet)
Peek Tubing
Polyurethane Tubing
Rinse Port (IN)
Viton Tubing
APS-1650 Tubing Diagram
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Installing the APS-1650
Figure 3-3
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APS-1650 Tubing Diagram
APS-1650 Automated Prep Station Operator’s Manual
Installing the APS-1650
Installation of the Paddle to the Stirring
Assembly
1) While holding the top part of the assembly in one hand, and
the paddle in the other, insert the paddle into the stirring
assembly. To remove, pull the paddle out.
Installation and Removal of the Stirring
Assembly
1) With the power off, manually push the rear block on the ZDrive assembly half of the way down.
2) Insert the stirring motor and secure with thumb screw.
3) Plug the cord into the front of the Z-Drive assembly. Do not
wrap the cord around the Z-Drive assembly.
4) To remove the stirring assembly, simply
directions for installation.
reverse the
Warning: Always power down the unit before plugging in / unplugging
the stirring motor.
Installation and Removal of the Sample Probe
1) To install the sample probe, slide the probe into the front
block on the Z-Drive and secure with the thumb screw.
When installing, make sure the bottom of the sample probe is
even with the end of the stirring paddle.
2) If the Liquid Level Detector is used, slide the sensor up the
probe and secure approximately one inch above the tip of
the probe.
Secure with the set screw. Secure the wires to
the probe with cable wraps.
Note: The level sensor block is plastic. Do not over tighten the screw
when securing to the probe.
Note: Anytime the liquid level sensor or probe has been repositioned,
the liquid level sensor requires calibration. See Calibrating the Liquid
Level Sensor later in this chapter.
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3) To remove the sample probe, simply reverse the directions
for installation.
Emptying the Drip Cup
The APS-1650 uses two drip cups; One for the stirrer and one for the
sample probe.
1) With the power off and the Z-Drive in the up position, (the
drip cup is underneath the stirrer and the sample probe), lift
up on the cup.
2) Empty the drip cup, clean it and then return it to the cup
holder.
Placing the Sample and Collection Racks
Depending upon the version of the APS-1650, the sample vial racks may
come assembled and ready for use. Some versions of sample vial racks
are shipped unassembled. However, you can easily assemble them
without using tools. Once you assemble the sample vial racks, place
them in the sample tray before proceeding with the installation.
WARNING
Before loading or unloading any sample vial racks on the
sample tray, park the sampling arm and probe in the home
position by cycling the power on and off. The home position is
the initial position at power up. Never attempt to load, unload
or reposition the sample vial rack or sample vial while the APS1650 is operating.
There are two types of racks used with the APS-1650. The Sample Rack
and the Collection Racks. The Sample Rack holds the raw samples and
is positioned to the left of the rinse station. The Collection Rack holds
the diluted samples and is position to the right of the rinse station.
1) Place the sample vial rack on the sample tray to the left of
the rinse station, aligning the holes on the sample rack to the
pegs on the sample tray.
Correctly placed sample vial racks will not move more than +/- 1mm
in either a left/right or forward/backward direction unless you lift
them.
2) Place the collection vial rack on the sample tray to the right
side of the rinse station aligning to the attachment points.
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Collection vial racks vary in models and attach in different fashions.
Some attach to pegs in the sample tray while others sit in holes on
the sample tray. Regardless of the model rack purchased, the rack
should be level and stable on the sample tray.
3) Fill the racks with the appropriate vials.
Establishing External Connections
The next step in the installation process involves connecting the APS1650 Automated Preparation Station to the power source and to a host
computer. The following sections explain how to establish these
connections.
Connecting the Automated Prep Station to the Power
Source
A voltage-specific external desktop power supply is supplied with each
APS-1650 Automated Preparation Station.
WARNING
Use only the external desktop power supply or an exact
replacement.
To connect the automated prep station to a power source, plug the
external desktop power supply cord into the power connector located on
the back panel of the autosampler. Then, plug the power supply’s power
cord into a 100-240 VAC +/-10%, 50/60Hz utility power outlet.
Connecting
the
APS-1650
Automated
Preparation Station to the Host Computer
You cannot operate the APS-1650 Automated Preparation Station until
you establish a communications interface between the autosampler and
the host computer. The APS-1650 supports the following two
communications protocols:

The USB interface is the standard configuration. A virtual COM
port is created when using the USB interface. The connection works
like a standard RS-232 serial port with the host PC software.
Device drivers for the USB interface are included on the Software
CD.

The serial (RS-232) protocol is an optional configuration. There are
two RS-232 serial ports on the APS-1650, and a serial interface kit
is shipped with the autosampler.
Either interface is acceptable for either device. Check your host
computer for available terminals when making your decision.
When interconnecting any computing devices, keep the
communications cables away from sources of electromagnetic or
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APS-1650 Automated Prep Station Operator’s Manual
Installing the APS-1650
Radio Frequency (RF) interference, such as electric motors,
transformers, fluorescent light ballasts or RF energy sources.
Establishing an RS-232 Serial
Communications Interface
The optional serial interface kit includes two interface cables equipped
with two modular port adapters each. Use the interface kit to establish a
serial communications interface with the host computer. To do so,
complete the following steps:
1) Plug one end of the cable into the host computer’s serial
(COM) port. Finger-tighten both screws of the cable adapter.
Note: If a host computer serial port with a DB9F, a DB25M or a DB25F
connector (9-pin D-submini receptacle or 25-pin D-submini plug or
receptacle) must be used, use the mating connector from the CETAC
Technologies universal port adapter kit. You can order the adapter kit
from CETAC Technologies, or purchase an adapter locally to convert the
serial port to DB9M. Do not use a “null modem” adapter.
2) Connect the other end of the cable to the APS-1650 COM1
port. Finger-tighten both screws of the cable adapter.
3) Plug one end of the second cable into the host computer’s
serial (COM) port. Finger-tighten both screws of the capable
adapter.
4) Connect the other end of the cable to the Pump Module Box
COM1 port. Finger-tighten both screws of the cable adapter.
Establishing a USB Communications
Interface
The APS-1650 Automated Preparation Station is supplied with a USB
cable. A cable may also be obtained from any computer store or
purchased separately through CETAC. Complete the following steps for
the USB interface:
1) Power up both the computer and the APS-1650.
2) Plug one end of the cable into the host computer’s USB port
and the other end to the APS-1650 USB port.
3) The computer screen should display “New Hardware Found”
on the screen. Insert the CETAC Installation CD and open
the USB drivers. Follow the instructions on the screen.
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Installing the APS-1650
4) Connect the second USB cable to the host computer and the
Pump Module Box. Power on the Pump Module Box.
Determining the COM Port being used by the
host computer
The operating system on the host computer automatically assigns a
communications port to each device.
1. Open the Device Manager
a. Right clicking on ‘My Computer’ and select ‘Manage’.
b. In the Computer Management window, select ‘Device Manager’.
c.
Scroll to the line ‘Ports (COM & LPT)’. Click on the + sign to
expand the contents.
2. Displayed is a listing of all the communications ports on the
host computer. (Figure 3-4)
3. Note these settings because they will be required to connect
with the Instruo Software to operate the APS-1650.
Figure 3-4: Communication Ports
In Figure 3-4, we can see this computer has two serial ports (COM1,
COM2) and one USB port (COM8).
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APS-1650 Automated Prep Station Operator’s Manual
Installing the APS-1650
Installing the Instruo Software
The Instruo software is designed to control the APS-1650 Automated
Prep Station operations. Follow these instructions for installation.
1) Minimum Hardware Requirements
•
Windows 2000 (Service Pack 3)/Windows XP (Service Pack 2)
•
128MB for Windows 2000, and 256MB for Windows XP
•
Video running 1024x768 with 256 colors
•
Pentium 600MHz for Windows 2000, 1GHz for Windows XP
•
2 free COM or USB ports
•
Internet Explorer 6 or higher
2) Installation
a. A software CD ships with each unit from CETAC. Insert this
CD into the host computer.
Note: If you are unable to locate the software CD, contact
CETAC Technologies Customer Service at 1-800-369-3822.
b. Locate the file on the CD named setup.exe and double click.
c.
Follow the instructions on the screen.
d. Go to Start/Programs/Instruo/Instruo Manual to open the
manual for the Instruo Software. Read it. Print a copy and
keep it with this manual for future reference.
Calibrating the Liquid Level Sensor
The Liquid Level Sensor is an IR (infrared) light sensor. The sensor
sends an IR light beam down to the sample. The light reflects off the
sample and is read by the IR sensor to determine the distance to the
liquid sample. The IR laser and detector are mounted on the back side
of the base unit. The IR light travels through two fiber optic wires to
the sensor head mounted to the probe.
If the sensor has been moved on the probe, or the probe height has
changed (or probe replaced) since the last calibration, the Liquid Level
Sensor should be re-calibrated. In addition, calibration should be
completed if the probe depth in the sample is too high or too low.
The Liquid Level Sensor cannot be used with all rack configurations. It
was designed for use with the 45 position sample rack and bottles. The
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Installing the APS-1650
Liquid Level Sensor should be turned off or removed when used with the
80 or 90 position sample racks. To turn the Liquid Level Sensor off,
refer to the “DIP Switch Usage” in Chapter 7 Trouble Shooting the
Automated Prep Station.
Note: Samples with a dull, non-reflective surface may not reflect the IR
light and could be problematic for the Liquid Level Sensor to make a
correct read. Reflective surfaces between the Liquid Level Sensor and
the sample such as the lip of the sample tube may also cause issues with
correctly reading the sample level. CETAC Technologies recommends
using sample bottles with 30mm opening with no lip at the top.
1) Verify the Liquid Level Sensor height on the probe is correct. Refer to
“Installation and Removal of the Sample Probe” earlier in this chapter.
2) Place a clear liquid sample (water works), and a clean red colored sample,
such as transmission oil in the sample rack.
3) Using the Manual Controls in the Instruo software, navigate the probe to
the clean sample. Move the probe down 2mm into the clear sample.
4) Locate the Liquid Level Detector on the rear of the unit and open the
plastic lid.
5) Set the sensitivity
a) There should be two numbers on the detector. One red number and one
green number. Press an arrow button on the detector twice. The green
light should now be flashing.
b) Using the arrow buttons, match the green number to the red number. An
exact match is difficult. Plus or minus 30 is an acceptable range.
6) Raise the probe out of the sample.
7) In the Instruo Software, mark the box “Level Sensor Enabled”
8) Add 15mm to the probe depth and tell the probe to go down.
a) The probe should stop in roughly the same position (2mm below the
surface)
b) If the probe goes too deep or too shallow, start over at step 5.
9) With the “Liquid Level Sensor” box still checked in the Instruo software,
move the probe to the clean red sample and go down 15mm below the
surface.
a) The probe should stop roughly 2-7mm into the sample.
b) If the probe goes too deep or too shallow, start over at step 5.
10) The liquid level sensor is now calibrated. In the Instruo Method, the
“Sample Probe Depth – Uptake” can be set to 135mm. The Liquid Level
Sensor will detect the sample surface and stop 2mm into each sample
regardless of the sample volume.
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4
Verifying Installation
APS-1650 Automated Preparation Station Operator’s Manual
Verifying Installation
Verifying Installation
Once installation of the APS-1650 Automated Preparation Station is
complete, it is important to verify that you have installed it correctly.
Attempting to use it before ensuring that it is installed correctly may
result in damage to the autosampler.
Verifying installation of the autosampler consists of two parts:
•
Ensuring that the communications interface between it and the host
computer is working.
•
Ensuring that the sample probe and stirring assembly function
properly.
This chapter explains how to test the above items before using the
autosampler.
Note:
The procedures given in this chapter are for use in a Windows
environment.
Testing the Interface
If the communications interface between the automated prep station
and the host computer is not established correctly, the autosampler will
not function.
Before you test the interface, ensure that the
communication port connectors are properly attached between the host
computer and the automated prep station.
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APS-1650 Automated Preparation Station Operator’s Manual
Verifying Installation
Note:
The following procedures assume that you started the Windows
operating system and the Program Manager window is showing.
To test the communications interface, complete the following steps:
1) Start the host computer and go to the main Windows screen.
2) Turn on power to the automated prep station.
3) Click the start button in the lower left corner of the Program
Manager window.
a) A selection list will appear.
4) Select rograms/Accessories/Communications/Hyperterminal®
and double-click.
a) The HyperTerminal window appears (Figure 4–1).
Figure 4–1. Example of HyperTerminal Window.
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APS-1650 Automated Preparation Station Operator’s Manual
Verifying Installation
5) Double click on the Hyperterminal® icon.
a) The Connection Description box appears (Figure 4–2).
Figure 4–2. Connection Description Box.
6) Type the name COM_test for the connection and choose an
icon from the list given, and click OK.
The phone number box appears (Figure 4-3).
4–5
APS-1650 Automated Preparation Station Operator’s Manual
Verifying Installation
Figure 4-3. Phone Number Box.
7) Select Direct to COM in the Connect Using box. Click OK.
The COM Properties box appears (Figure 4-4).
Figure 4-4. COM Properties Box.
4–6
APS-1650 Automated Preparation Station Operator’s Manual
Verifying Installation
8) Change the bits per second to 9600, set the data bits to eight,
the parity to none, the stop bits to one, the flow control to
none, and click OK.
9) Select File/Properties.
The COM_Test Properties box appears.
10) Select Settings on the COM_Test Properties box and click on
the ASCII setup button on the lower right of the box.
The ASCII setup box appears (Figure 4-5).
Figure 4-5. ASCII Setup Box.
11) In the ASCII Setup box, select the following items:
a) Echo typed characters locally.
b) Append line feeds to incoming line ends.
c)
Wrap lines that exceed terminal width.
d) Click OK.
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APS-1650 Automated Preparation Station Operator’s Manual
Verifying Installation
12) Click OK on the COM_Test Properties box.
13) Type the command “home” at the cursor in the upper left of
the main HyperTerminal screen and press Enter.
The autosampler resets, with the sample probe moving out and back
into the home position. If the autosampler does not reset, see
Chapter 7, “Troubleshooting the Automated Prep Station.”
14) Now change the COM port to the correct port used by the
Syringe Module Box, reconnect through HyperTerminal, and
type the command “ver”.
The Syringe Module Box will return a status. If nothing is returned,
see Chapter 7, “Troubleshooting the Automated Prep Station.”
Checking the Automated Prep Station
Components
The following components may be damaged during shipping or
installation: the sample probe, the peristaltic pump tubing, and the
rinse station and tubing. It is important that you check these
components for damage before you operate the automated prep station.
To do so, complete the following steps:
1) Shut down and unplug the system.
2) Visually inspect the sample probe, peristaltic pump tubing,
and rinse station and tubing for leaks or signs of damage.
If you detect a leak or other damage to an autosampler component,
you must replace it. For more information, see the appropriate
section in Chapter 6, “Maintaining the Automated Prep Station.”
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APS-1650 Automated Preparation Station Operator’s Manual
Verifying Installation
Testing the Sample Probe
The sample probe must descend into the center of each sample vial to
ensure satisfactory sample uptake. Rough handling in shipment can
disturb the autosampler’s cabinet-to-base alignment. If it is incorrectly
aligned, the sample probe will not function properly. It is therefore
important to test the sample probe before you actually run samples with
the autosampler.
Note:
Before testing the sample probe, ensure that you have installed all
system components correctly. Also, ensure that you have securely
tightened all thumbscrews and connected the communications cable
from the host computer to the COM1 port on the automated prep station.
Testing the sample probe involves observing the operation of the sample
probe. To do so, complete the following steps:
1) Turn the autosampler power switch on and verify that the
LED power indicator is on.
The LED power indicator is green in color. The indicator is located
behind the Z-Drive assembly when it is in the home position.
2) Using the Manual controls in the Instruo control software,
command the probe down 40 in the home position. In small
increments, experiment sending the probe to go deeper and
deeper until the probe goes into the port on the rinse station.
If at any point it is obvious the probe is going to hit the rinse
station instead of the port, stop and contact Customer
Support.
3) Repeat step 3 for the stirring paddle.
Note: If the autosampler alignment is not correct, contact CETAC
Technologies Customer Service and Support or an authorized
representative.
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APS-1650 Automated Preparation Station Operator’s Manual
Verifying Installation
4–10
5
Using the Automated Prep
Station
APS-1650 Automated Preparation Station Operator’s Manual
Using the Automated Prep Station
5–2
APS-1650 Automated Preparation Station Operator’s Manual
Using the Autosampler
Using the APS-1650
The APS-1650 Automated Prep Station is both reliable and easy to use.
Before using it, however, ensure that your lab environment provides
operating conditions that will prolong the life of the APS-1650. Once the
proper operating conditions are met, you can arrange the sample vial
racks and start the autosampler sequence run. When you finish using
the autosampler, you may need to flush the rinse station and flow path
before shutting the system down.
This chapter explains how to create the proper operating conditions for
using the APS-1650 Automated Prep Station. It also explains how to
arrange the sample vial racks, start and shut down the unit, and flush
the rinse station and flow path.
Establishing Optimal Operating Conditions
The APS-1650 Automated Preparation Station operates reliably even
under less than ideal conditions. It is not, however, indestructible.
Malfunction or damage can occur if specific operating conditions are not
met. Meeting these conditions requires that you create the proper lab
environment, replace autosampler components that wear out under
normal use, and purchase the appropriate supplies for use with the
automated prep station. The following sections explain how to meet
these conditions.
Note:
Damage or malfunction that results from unsatisfactory operating
conditions may constitute misuse and abuse and be excluded from
warranty coverage.
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APS-1650 Automated Preparation Station Operator’s Manual
Using the Automated Prep Station
Creating the Lab Environment
To create satisfactory operating conditions in your lab environment,
follow these guidelines:
WARNING
•
Operate the APS-1650 in a conventional lab environment where the
temperature is 50–95 °F (10–35 °C), the humidity is 20–70%
non-condensing, and the unit is not exposed to excessive flammable
or corrosive materials.
•
Avoid rough handling of the APS-1650. If possible, do not expose the
autosampler to vibration or shock.
•
Protect the autosampler from long-term exposure to condensation,
corrosive materials, solvent vapor, continual standing liquids, or
large spills into the autosampler cabinet or arm. Exposures of this
type can damage the drive mechanisms as well as the electronics.
•
Observe the same general electrostatic discharge precautions as
with any other integrated circuit electronic devices. Low humidity
environments, especially when combined with static-generating
materials, require maximum care.
Discharge static buildup and ground to the autosampler base or
cabinet before performing any maintenance. Do not touch or
short-circuit bare contacts, COM1, DILUTOR, or auxiliary ports.
•
5–4
Avoid using the APS-1650 if strong electromagnetic interference,
radio frequency interference, or radioactivity is present.
Interference fields can cause erratic operation of the unit. The APS1650 will not function properly if the level of radioactivity is above
background.
APS-1650 Automated Preparation Station Operator’s Manual
Using the Autosampler
Replacing Auto Sampler Components
The following APS-1650 components wear out under normal use and
must be replaced periodically.
•
Peristaltic pump tubing
•
Sample probe
•
Drip Cup Control Rod Springs in the Z-Drive Assembly
If you fail to replace these components when they deteriorate, the
autosampler will not function properly. For information about replacing
autosampler components, see Chapter 6, “Maintaining the APS-1650.”
Purchasing Supplies
Because the life-span of the sample vials varies, you should maintain an
adequate supply of spare vials. When you need to purchase additional
supplies, it is extremely important that you choose the appropriate sizes
and materials.
When you purchase sample and/or standards vials, make sure they meet
the following requirements:
WARNING
•
The diameter of the sample vial matches the rack size you are using.
•
The height does not exceed 125 millimeters.
•
The material is compatible with the samples you are analyzing or
the reference standards you are using. This requirement also
applies to the peristaltic pump tubing.
Use of mismatched sample vials and sample vial racks may
result in malfunctions or sample spills. Be sure your vials meet
the given requirements.
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APS-1650 Automated Preparation Station Operator’s Manual
Using the Automated Prep Station
To order additional supplies, refer to the CETAC Accessories and
Supplies Catalog for the APS-1650 Automated Preparation Station
which can be found on the installation CD or www.cetac.com.
Arranging the Sample Vial Racks
You can change the arrangement of the sample vial racks to meet your
needs. The APS-1650 accommodates one sample vial rack of 45, 80, or
90 positions each. It accommodates one sample collection rack of 80, or
90 positions each.
The automated prep station physically accepts any and all size
combinations and arrangements of sample vial racks. However, you can
use racks of mixed sizes only if the Instruo software enables you to do
so. A custom rack file may need to be created to work with the rack of
your choice.
For more information about placing sample vial racks in the sample
tray, see Chapter 3, “Installing the Autosampler.”
For more information on working with custom rack solutions, see the
Instruo Software Manual.
CAUTION
Incorrectly defining the sample rack layout can result in sample spills,
damage to the unit, and invalid analysis results.
Starting the Automated Prep Station
Once you arrange the sample vial racks and ensure that the
arrangement is correctly defined in the software, you can start the
autosampler and let it run until the sampling sequence is finished. To
do so, complete the following steps:
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APS-1650 Automated Preparation Station Operator’s Manual
Using the Autosampler
1) Ensure that the rinse station is properly connected.
For more information about proper connections, see Chapter 3,
“Installing the Autosampler.”
2) Turn the APS-1650 Automated Preparation Station power
switches on.
The green LED indicator along the autosampler X-Axis lights up
when the power is on. The green LED on the Syringe Module will
also light up when power is on.
3) Open the Instruo Software and load the desired Method and
Sequence.
Refer to the Instruo Software Manual with question on Method and
Sequence setup.
4) Purge air from the system
a) Ensure rinse and diluent uptake tubing and drain tubing are
inserted into the correct containers.
b) Using the Direct Controls in Instruo, Purge the Rinse and
Syringe Pump until all air is removed from the tubing. Refer to
the Instruo Software Manual as needed.
5) In the Instruo software, execute the sequence.
The APS-1650 runs until it reaches the end of the sampling
sequence.
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APS-1650 Automated Preparation Station Operator’s Manual
Using the Automated Prep Station
Shutting Down the Autosampler
To shut down the autosampler, complete the following steps:
1) Drain the rinse system by removing the rinse solution
uptake tubing from the rinse solution source. Using the
Direct Hardware Control in Instruo, let the peristaltic pump
run until all solution drains from the tube attached to the
rinse station outlet.
2) Using the Direct Hardware Control in Instruo, empty the
syringe pump.
3) Release the pressure shoe on the peristaltic pump.
Releasing the pressure shoe decreases wear on the pump tubing.
4) Shut down the Instruo software.
5) Turn off the APS-1650 power switch and the power switch on
the Syringe Module Box.
Flushing the Rinse Station and Flow Path
Generally, you can operate the APS-1650 without flushing the rinse
system. Under normal circumstances, you can simply drain the rinse
system prior to shutting down the autosampler. However, you need to
flush the rinse station and flow path during initial startup of the APS1650 Automated Prep Station after installation.
Flushing the rinse system during initial startup of the APS-1650
Automated Prep Station removes any contaminants that could cause
interference during sample analysis. To flush the rinse station and flow
path, complete the following steps:
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APS-1650 Automated Preparation Station Operator’s Manual
Using the Autosampler
1) Insert the rinse uptake tubing into the rinse solution or
Isopropyl alcohol.
2) Run the rinse solution through the rinse station and flow
path for 5 to 10 minutes.
Once you flush the rinse system, you can proceed with the sampling
sequence or drain the rinse system as part of the shutdown
procedure.
5–9
6
Maintaining the APS-1650
Automated Preparation Station
APS-1650 Automated Preparation System Operator’s Manual
Maintaining the Automated Prep Station
Maintaining
the
APS-1650
Automated Preparation Station
Routine maintenance of the APS-1650 consists of daily and weekly
cleaning of specific autosampler components. Routine maintenance also
includes checking APS-1650 components for leaks or other damage.
Additional periodic maintenance tasks may be required, including
replacement of the following autosampler components: peristaltic pump
tubing, sample probe, locking springs in the Z-Drive Assembly, rinse
station tubing, and sample tray.
This chapter explains how to clean the APS-1650, inspect it for leaks,
and replace damaged components.
WARNING
Discharge static buildup and ground to the autosampler base or
cabinet before performing any maintenance. Do not touch or
short-circuit bare contacts, COM1, Dilutor, or auxiliary ports.
Cleaning the Automated Prep Station
Cleaning the APS-1650 is the primary maintenance task you perform.
Failure to do so regularly causes increased wear and reduces the
automated prep station’s life.
You must clean the APS-1650 both daily and weekly to prevent damage
and extend its life. It is especially important to clean up spills and
remove contaminants, such as abrasives, from the autosampler’s moving
parts. It may also be necessary to chemically neutralize spills. The
following sections explain daily and weekly cleaning procedures.
6-3
Daily External Cleaning
Use of the APS-1650 often results in spills on autosampler components
such as the sample tray. Good maintenance requires that you clean the
autosampler daily. To do so, complete the following steps:
1) Shut down and unplug the autosampler.
For information about shutting down the Autosampler, see Chapter
5, “Using the Autosampler.”
2) Wipe the sample base, rack adapter plate, autosampler
cabinet, pump module box, and Y-arm using a towel
dampened with a lab-grade cleaning agent.
CAUTION
Do not allow the cleaning agent to come into contact with the lead
screws. Also, never lubricate either of the two lead screws.
3) Repeat step two, using a towel dampened with clean water
or Isopropyl alcohol.
This process removes any remaining contaminants.
4) Dry the sample base, rack adapter plate, autosampler
cabinet, pump module box, and Y-arm using a dry towel.
The APS-1650 must be thoroughly dry before you turn the
autosampler power on.
Weekly Cleaning
Although cleaning it daily removes spills and contaminants from most of
the automated prep station components, it is necessary to clean the
APS-1650 more thoroughly once a week. To do so, complete the
following steps:
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APS-1650 Automated Preparation System Operator’s Manual
Maintaining the Automated Prep Station
1) Shut down and unplug the system.
2) Remove the sample tray.
3) Wipe loose particles off the Y-Axis lead screw with a dry,
lint-free cloth.
The Y-Axis lead screw is a large metal screw located inside the
Autosampler arm tubing, as shown in Figure 6–1.
Figure 6–1.
Z-Drive Assembly on the Autosampler Y-Arm.
6-5
WARNING
Never lubricate the lead screws. The lead screw nuts are
compounded with a dry film lubricant. Oiling the lead screws
will cause gumming, galling, and binding of the sample probe
assembly.
4) Wipe the automated prep station exterior until it is clean,
using a towel dampened with a lab-grade cleaning agent,
followed by a towel dampened with clear water.
Pay special attention to the slider block and guide rails along the
tube of the autosampler arm.
5) Wash the rack adapter plate in a warm detergent solution.
Make sure you remove all spills and stains.
6) Rinse the rack adapter plate with water and then dry it.
Ensure that the sample tray is thoroughly dry.
7) Replace the rack adapter plate on the autosampler base.
Checking for Leaks
Several of the automated prep station components have a limited life
and will wear out under normal use: the sample probe, the peristaltic
pump tubing, and the rinse station and tubing. Standard maintenance
procedures require that you periodically check these components for
leaks. To do so, complete the following steps:
1) Run the Rinse Pump in the pump module box using the
manual controls in the Instruo software until the rinse
solution is coming out of the probe.
2) Wait 2 minutes and inspect the probe for drips.
3) Restart the Rinse Pump in the Instruo software. If there is a
delay before the rinse solution exists the probe check all
fittings for leaks.
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APS-1650 Automated Preparation System Operator’s Manual
Maintaining the Automated Prep Station
If you detect a leak or other damage to an autosampler component,
you must replace it. For more information, see the appropriate
section in this chapter.
Replacing Peristaltic Pump Tubing
Routine maintenance of the APS-1650 Automated Preparation Station
includes replacement of the peristaltic pump tubing. Because of the
operating nature of peristaltic pumps, the tubing will probably be the
most frequently replaced item on the autosampler. If you use strong
bases, acids, or solvents as rinsing agents, the tubing may break down
rapidly.
To replace the peristaltic pump tubing, complete the following steps:
1) Shut down and unplug the autosampler.
2) Release the pressure shoe on the peristaltic pump and
remove the old tubing.
Carefully pull or cut the old tubing to remove it.
3) Replace the pump tubing by pushing the new tubing onto the
mounting block fittings.
Replace the new tubing carefully. Damage can result if you apply
too much force.
4) Reconnect the pressure shoe.
Replacing the Sample Probe
You must replace the sample probe if it is leaking or shows other signs
of deterioration. To do so, complete the following steps:
1) Shut down and unplug the autosampler.
6-7
2) Remove the Liquid Level Sensor from the probe.
3) Remove the old sample probe and tubing.
Be careful not to use excessive force when removing the sample
probe. Applying too much force can result in damage to the Z-Drive
assembly.
4) Install the new sample probe.
5) Replace the Liquid Level Sensor and calibrate.
For information about installing the sample probe an Liquid Level
Sensor calibration, see Chapter 3, “Installing the Autosampler.”
Replacing the Rinse Station Tubing
If the rinse station tubing is typically exposed to deionized water as a
rinsing agent, you do not need to replace it often. However, if you use
other rinsing agents, such as acids or solvents, the tubing is likely to
deteriorate more rapidly. To replace the rinse station tubing, complete
the following steps:
1) Shut down and unplug the autosampler.
2) Disconnect the rinse solution uptake and drain tubing.
Apply only a linear force when removing the tubing to prevent the
fittings from breaking.
3) Remove the rinse station block by removing the screw from
the mounting bracket.
6) Connect the rinse solution uptake and drain tubing.
Apply only a linear force when replacing the tubing to prevent the
fittings from breaking.
6-8
7
Troubleshooting the Automated
Prep Station
APS-1650 Automated Prep Station Operator’s Manual
Troubleshooting the Automated Prep Station
Troubleshooting the APS-1650
The APS-1650 Automated Preparation Station is both easy to operate
and reliable. However, problems with it may occur. When the
autosampler does not function properly, isolate the problem to
determine if it originates in the host computer, the analytical
instrument, the RS-232 cable, or the autosampler. If you determine the
problem is in the APS-1650, check the power system, the
communications interface, or the sample probe assembly to find the
cause of the problem and resolve it.
This chapter explains how to troubleshoot APS-1650 problems. If you
cannot solve a problem using the steps given in this chapter, contact
CETAC Technologies Customer Service and Support at 1-800-369-2822.
A complete catalog of accessories and supplies is included on the
installation CD, or can be found at www.cetac.com.
Power System Problems
A possible cause of APS-1650 malfunction is a problem in the power
system. If the autosampler is not functional, there may be no power
getting to it. If this is the case, the green LED power indicator will be
off. To troubleshoot this problem, complete the following steps:
1) Check the wall outlet and see if the external power supply is
plugged in.
2) Ensure the power switch of the external power supply is
turned on.
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APS-1650 Automated Prep Station Operator’s Manual
Troubleshooting the Autosampler
Interface Problems
Operation of the APS-1650 is directed by the host computer. A
malfunction of the autosampler can indicate a problem with the RS-232
cable or with the configuration of the software on the host computer.
The following sections explain how to troubleshoot these problems.
RS-232 or USB Cable Problems
The first step in troubleshooting interface problems is to check the
RS-232 cable. To do so, complete the following steps:
1) Check the autosampler power switch to ensure it is on.
2) Check the communications cable to ensure it is plugged in to
the correct port on the autosampler.
If the cable is plugged in, ensure that it is tightened properly.
3) Check the host computer to ensure that the communications
cable is connected to the appropriate COM port.
If the cable is plugged in, ensure that it is tightened properly. For
more information about connecting the RS-232 cable, see Chapter 3,
‘‘Installing the Autosampler.’’
Software Configuration Problems
If the RS-232 cable is connected properly and the autosampler is still not
communicating with the host computer, ensure that the Instruo
software is configured correctly. To do so, complete the following steps:
1) Verify communications in Hyper Terminal.
If the wrong port or baud rate is selected, change the configuration.
For information about changing the software configuration, see
Chapter 4, ‘‘Verifying Installation.’’
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APS-1650 Automated Prep Station Operator’s Manual
Troubleshooting the Automated Prep Station
2) Run the Instruo software and ensure that the instrument is
functioning properly.
Z-Drive Assembly Problems
An APS-1650 malfunction may be caused by a problem in the Z-Drive
assembly. You can easily determine that a malfunction is related to the
Z-Drive assembly if you hear a loud chattering noise when the APS-1650
power switch is on or if the sample probe is not moving. To troubleshoot
Z-Drive assembly problems, complete the following steps:
1) Ensure that the Y-Axis slider block and Z-Drive assembly are
installed.
If the Z-Drive assembly is not installed, follow the instructions
provided in Chapter 3, ‘‘Installing the Autosampler,’’ to install it. If
the Z-Drive assembly is already installed, continue with step two.
2) Check the Y-Axis position magnet for damage.
The home position magnet is attached to the Z-Drive assembly. If
the magnet is damaged or blocked, you must replace or clean the
assembly. For information about mounting the Y-Axis slider block
on the autosampler are, see Chapter 3, ‘‘Installing the Autosampler.’’
If the home position flag is undamaged, continue with step three.
3) Ensure the sample probe block and stirrer block move freely
up and down the Z-Drive assembly.
If the assembly is binding and cannot be corrected, contact customer
service.
Note: If you cannot free the Z-Drive assembly, you will need to
replace it. See Chapter 3, ‘‘Installing the Autosampler,’’ for
information about mounting a new Z-Drive assembly. You can order
a new Z-Drive assembly from CETAC Technologies.
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APS-1650 Automated Prep Station Operator’s Manual
Troubleshooting the Autosampler
Drip Cup Problems
Should the drip cup swing out too soon, too late, or operate in any other
unusual manor, check the locking spring located at the top of the control
rod just below the Z-Drive motor assembly. Replace the spring if
broken, worn, or damaged.
1) Turn the power off and unplug the power supply.
2) Remove the drip cup.
3) Slide the probe block down to the lower end of its travel.
4) Lift up on the control rod compressing the spring.
5) Rotate the drip cup holder past its normal rotation toward
the Y-Arm.
6) Lower the control rod and replace the spring.
7) Press the control rod up compressing the spring.
8) Rotate the drip cup holder back to its original position and
release the control rod.
9) Slide the probe block up and down several times to confirm
proper operations.
10) Plug in the power supply and turn on the power.
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APS-1650 Automated Prep Station Operator’s Manual
Troubleshooting the Automated Prep Station
Dip Switch Settings
The APS-1650 Automated Preparation Station has two banks of DIP
switches located under the potentiometers on the rear of the unit. A
Philips screw driver is required to remove the panel to gain access.
The DIP Switches control various setting as outlined below. Always
power off the unit prior to making DIP Switch changes.
Small 5-DIP bank (not pictured)
1
2
3
4
5
Level Sensor Present (APS-1650)
Off
Level Sensor NOT Present (1650)
On
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APS-1650 Automated Prep Station Operator’s Manual
Troubleshooting the Autosampler
Dip switches on the large bank should be set as follows.
Large 16-DIP
1
bank
2
3 4 5 6 7 8
9
10
11
12
13
14
15
Middle Rinse
Station
Present
On
Pump Speed
Pot Enabled
On
Aux. Pump
Installed/Pot
Enabled
Off
Stirrer
Installed/Spe
ed Pot
Enabled
On
W Axis is
Installed
On
Stirrer is next
to the chassis
On
Stirrer is
away from
the chassis
Off
Enable Smart
Stirring (1st
*
Row)
Off
Enable auto
*
lift from rinse
Reset Speed
Params to
Default
7---8
16
Off
Off