POWDER GLASS GLASS PASTE

AGC Glass Powders for Electronics
POWDER GLASS
AGC Glass Pastes for Electronics
GLASS PASTE
Product Catalog
Advanced Material Division
ASAHI GLASS CO., LTD. AGC Electronics
1-5-1 Marunouchi Chiyoda-Ku, Tokyo 100-8405 Japan
URL http://www.agc.com/fritpaste/
November 2014
Product lines
The Asahi powder and paste business made their breakthrough in 1956,
with the mass production of low-melting and crystalized type glass powder used for CRT sealing.
AGC is taking up the challenge of harnessing and integrating our glass,
chemistry and ceramics technologies, exploiting our strengths in
design and analysis to expand the application of glass as a high-performance
electronic material, and moving actively into lead-free glasses.
POWDER GLASS
GLASS PREFORM
GLASS PASTE
P.2
POWDER GLASS
AGC powder glass is available in a wide range of products variants for use in applications from flat display panels, thick-film circuit boards, and Glass-Ceramic Multilayer Substrate.
From the original melt, through grinding, to the final sieving, Asahi Glass's proprietary technology is used under the strictest quality control regime.
The track record established over many years has won these products the full confidence of industrial users, particularly in terms of ease of use and fast technical service unrivalled
by competitors, and ensures that they fully meet every need.
Applications for Powder Glass Sealants
Purpose of Seal
Items Sealed
Glass-Glass
Glass-Ceramic
Glass-Metal
Ceramic-Ceramic
Glass-Glass
Glass-Ceramic
Ceramics
Metals
Frit seals
Binders
Coatings
Main Applications
PDP
Fluorescent indicator tubes
IC packages
thick-film glass paste
thick-film metal paste
Alumina substrate
The following criteria should govern your selection of Powder Glass:
●Thermal expansion coefficient
It is normally desirable to apply press to the glass after sealing, so choose
a powder glass with a thermal expansion coefficient smaller than that of the
materials being sealed by between 0 and 15×10 -7/℃.
●Sealing temperature
To form a good seal, the powder glass should properly wet the material being
sealed, so raise its temperature above the softening point of the glass.
●Seal atmosphere
In Air or nitorgen
●Chemical resistance
Powder glass consisting primarily of SiO 2 has excellent acid and water resistance.
Powder glass consisting primarily of B2O3-PbO or B2O3-ZnO has slightly lower
acid resistance.
●Particle size
Particles of powder glass for molds or paints generally pass 100~150 mesh,
while those for screen-printing generally pass 250~325 mesh.
Various types of particle distribution are available by request.
R2O ・ ・ ・ ・ ・ R can be any alkali metal (K, Na or Li)
RO ・ ・ ・ ・ ・ RO can be any alkaline earth metal (Mg, Ca, Sr or Ba)
Thermal expansion coefficient ・ ・ ・ The average ratio by which the glass expands when
heating through 1℃.
Transformation point ・ ・ ・ The temperature at which the glass structure changes, with
viscosity of approx. 1013.3 poise.
(Values are the temperature on the shoulder at the first thermal absorption region on
the DTA curve. The exception specified in the list individually.)
Softening point ・ ・ ・ The temperature at which glass deforms under its own weight, with a
viscosity of about 107.6 poise.
(Values are temperature at the peak of the second thermal absorption region on
the DTA curve. The exception specified in the list individually.)
Crystallization temperature ・ ・ ・ The temperature at which the heat of crystallization of
a crystalline glass reaches a maximum while it is being heated. (The peak temperature
for thermal dissipation on the DTA curve.)
Sealing temperature ・ ・ ・ The temperature suitable for actual operations
Average particle size ・ ・ ・ Mean particle diameter. (Permeability method)
Particle size (centre value) ・ ・ ・ Median particle diameter. (Laser diffraction method)
Sieving size ・ ・ ・ ・ ・ 100 mesh : mesh size of 149μm
150 mesh : mesh size of 105μm
200 mesh : mesh size of 74μm
250 mesh : mesh size of 63μm
325 mesh : mesh size of 44μm
P.3
POWDER GLASS
Powder Glass for Binder
Code
ASF1216
ASF1330
ASF1370
ASF1373
ASF1380
ASF1500
ASF1550
ASF102X
ASF1094
ASF1096
ASF1098
ASF1099
ASF1100
ASF1100B
ASF1109
ASF1317
ASF1560
ASF1561
ASF1620B
ASF1700
ASF1702
ASF1717
ASF1780
ASF1891
ASF1891F
ASF1898B
ASF1930
ASF1939
ASF1941B
KF9173
LS-5-300M
SK-231-300
Developing Products
1097C2
1991Y10
200GF
CB001
JP-1
K-301
K-303
K-304
K-807
K-808
K-834
K-835
K-836
TM-1
TM-5
*1 Transformation point of TMA curve.
Glass Type
PbO・SiO2
PbO・B2O3
PbO・SiO2・B2O3
PbO・SiO2
PbO・SiO2
PbO・SiO2・Al2O3・RO
PbO・B2O3・ZnO
SiO2・B2O3
Bi2O3・B2O3
Bi2O3・B2O3
Bi2O3・B2O3・ZnO
ZnO・Bi2O3・B2O3
Bi2O3・B2O3
Bi2O3・B2O3
Bi2O3・ZnO・B2O3
SiO2・RO
SiO2・ZnO・RO
SiO2・ZnO・RO
ZnO・B2O3・SiO2
SiO2・RO・ZnO
RO・SiO2・ZnO
SiO2・RO
SiO2・B2O3・RO
ZnO・B2O3・SiO2
ZnO・B2O3・SiO2
RO・B2O3・ZnO
SiO2・TiO2
RO・SiO2・B2O3
RO・SiO2・B2O3
Bi2O3・B2O3
SiO2・RO・R2O
Bi2O3・RO・B2O3
SiO2・B2O3・Bi2O3
SiO2・B2O3・R2O
SiO2・RO
SiO2・RO・Al2O3
PbO・SiO2
SiO2・B2O3・RO
SiO2・B2O3・RO
SiO2・B2O3・RO
SiO2・RO・B2O3
SiO2・RO・B2O3
B2O3・RO・ZnO
B2O3・ZnO
SiO2・RO・TiO2
SiO2・B2O3・TiO2
SiO2・TiO2
Firing Condition
Temp.-Time
Thermal
Expansion Coeff.
(℃-min)
600-10
500-15
650-15
700-15
800-15
850-15
550-15
850-60
550-10
400-15
600-10
600-10
460-30
460-30
580-5
810-10
850-15
850-10
850-15
850-15
950-15
850-10
850-15
800-10
800-10
600-10
800-15
850-15
700-15
500-10
580-20
(×10-7/℃)
63
92
51
84
62
59
47
28
79
120
54
42
113
107
65
55
73
75
55
72
119
35
52
66
63
106
112
88
90
98
106
84
650-10
600-10
750-30
900-10
865-30
490-60
490-60
770-10
800-10
800-10
800-10
69
150
95
90
40
89
129
105
73
68
82
43
94
82
97
*2 Third inflection point on DTA curve
CTE
Temp range
(℃)
Specific
Gravity
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
50-350
4.3
5.6
3.8
4.0
3.8
3.0
4.7
2.2
5.4
6.7
5.5
4.7
6.3
6.3
5.1
3.1
3.3
3.4
3.7
3.6
3.8
3.3
2.5
3.5
3.5
3.4
2.8
3.7
3.7
6.4
2.9
5.1
50-350
50-350
50-300
50-300
50-600
30-300
30-250
30-250
30-300
30-300
30-300
30-300
30-300
50-500
50-500
5.2
2.8
2.5
3.8
3.5
3.1
2.9
2.9
3.5
3.3
4.0
3.8
4.2
3.7
3.2
Viscosity Property ( DTA )
Transformation
Softening Crystallization
Point
Point
Temp.
(℃)
(℃)
(℃)
468
576
380
445
465
615
550
435*1
555
690
693
803
450
540
495 *1
762
466
526
355
405
465
441
535
475
562
380
440
510
382
520
461
537
585
730
670
780
815
640
750
892
570
656
759
680
813
890
679
807
911
677
808
846
538
783
488
587
710
495
589
707
442
526
570
660
805
620
716
591
683
*2
403
459
476
553*2
775
491
557*2
520
404
466
700
637
561
373
444
655
667
516
542
718
606
629
605
524
650
770
829
634*2
431*2
504*2
738*2
761*2
587*2
613*2
774*2
702
729
900
662
511
613
631
667
840
819
Average
Particle
(µm)
2.0
2.1
2.7
2.0
2.3
2.0
1.7
1.6
3.1
3.5
4.0
-
Particle Property
Particle Size Sieving Size
(D50)
Mesh Pass
(µm)
1.7
325
325
1.9
250
6.3
325
4.9
325
3.8
325
1.3
325
1.0
24
0.8
150
1.0
325
3.0
100
3.5
100
5.2
150
1.1
325
2.8
325
1.5
325
2.2
325
3.5
325
4.5
150
325
2.6
325
2.5
325
4.9
325
2.8
325
1.5
325
1.1
200
3.0
100
1.3
325
1.2
325
100
325
12.0
325
5.8
2.0
4.0
3.8
1.0
3.8
9.0
8.0
8.0
5.0
14.0
8.0
12.0
3.0
3.1
2.2
325
100
150
250
100
300
300
300
100
100
300
100
300
100
100
Color
After
Firing
Glass
Characteristics
Yellow-White
Gray
White
White
White
White
White
Yellow
Yellow
White
White
Brown-Yellow
Yellow
Green
White
White
White
White
Gray
White
White
White
White
Black
White
-
Vitreous
Vitreous
Vitreous
Vitreous
Vitreous
Devitrifying
Devitrifying
Vitreous
Vitreous
Devitrifying
Devitrifying
Devitrifying
Devitrifying
Devitrifying
Vitreous
Vitreous
Devitrifying
Devitrifying
Devitrifying
Devitrifying
Devitrifying
Devitrifying
Vitreous
Devitrifying
Devitrifying
Vitreous
Devitrifying
Vitreous
Vitreous
Vitreous
Devitrifying
Vitreous
White
White
White
White
White
White
White
White
White
White
White
White
White
Vitreous
Vitreous
Vitreous
Devitrifying
Vitreous
Devitrifying
Devitrifying
Vitreous
Vitreous
Vitreous
Devitrifying
Devitrifying
Devitrifying
Devitrifying
Devitrifying
P.4
POWDER GLASS
Powder Glass for Low Temperature sealing
Code
7570
7575BF
7583BF
ASF1290A4
7574
9079-150
ASF2511C
BNL115BB
FP-74
KF9173
FP-74
Developing Products
1991Y10
F1290NY01
FP-67
KFI0115
KP312
KP312E
LFP-A50Z
TNS031W
TNS062-ZB
Glass Type
Firing Condition
Temp.-Time
PbO・B2O3・Al2O3
PbO・ZnO
PbO・ZnO
PbO・B2O3
ZnO・B2O3・SiO2
SnO・P2O5
Bi2O3・ZnO
Bi2O3・ZnO
SnO・P2O5
Bi2O3・B2O3
SnO・P2O5
(℃-min)
500-5
450-60
450-60
430-10
775-30
480-10
470-10
500-10
480-10
520-20
480-10
SiO2・B2O3・R2O
PbO・B2O3
SnO・P2O5
Bi2O3・B2O3
SnO・P2O5
SnO・P2O5
SnO・P2O5
V2O5
TeO2・V2O5
600-10
430-10
480-10
470-10
430-10
430-10
460-10
430-10
380-10
Thermal
Viscosity Property ( DTA )
Particle Property
CTE
Glass
Specific Transformation Softening Crystallization Average Particle Size Sieving Size
Expansion
Temp range
Character
Gravity
Coeff.
Point
Point
Temp.
Particle
(D50)
Mesh Pass
(℃)
istics
(×10-7/℃)
(℃)
(℃)
(℃)
(µm)
(µm)
*1
84
30-300
5.4
378
447
100
6.3
Vitreous
89
6.4
320
375
3.7
100
Devitrifying
30-300
84
6.1
325
370
4.2
150
Devitrifying
30-300
105
6.3
332
394
ー
3.9
325
Vitreous
30-300
*1
37
30-500
3.6
567
10.2
100
Devitrifying
647
*1
122
30-250
3.8
13
150
Vitreous
287
344
82
30-300
6.4
351
8
100
Vitreous
400*1
*1
71
30-300
7.3
355
5.0
100
Vitreous
399
30-250
3.4
355
4.6
100
Vitreous
63
275
*1
98
30-300
6.4
403
3.5
100
Vitreous
459
30-250
3.4
355
4.6
100
Vitreous
63
275
150
78
81
105
128
70
45
105
84
50-350
30-300
30-250
30-300
30-250
30-250
30-250
30-250
30-250
2.8
5.6
3.6
7.4
3.8
3.5
3.8
3.9
4.0
404
334
280
350
280
282
270
298
270
525
405
345*1
400*1
325*1
343*1
348*1
362
325
-
-
4
3.0
10
5
6
11
1.0
11.0
100
325
150
200
150
150
300
325
Vitreous
Vitreous
Vitreous
Vitreous
Vitreous
Vitreous
Vitreous
Vitreous
Vitreous
Color
After
Firing
Major Application
White
Black
Gray
White
White
Gray
Black
Black
Black
Black
Seathed heaters
Soda-Lime Glass sealing
Ceramic sealing
Stainless sealing
AlN sealing
White
White
Black
Yellow
Gray
Black
Black
Black
Black
Metal sealing
Soda-Lime Glass sealing
Ceramic sealing
Ceramic sealing
Seathed heaters
Ceramic sealing
Soda-Lime Glass sealing
Stainless sealing
Ceramic sealing
Non-Alkali Glass sealing
*1 Third inflection point on DTA curve
y Substrate
Powder Glass for Glass-Ceramic Multilayer
Code
ASF102M
ASF102X
ASF102Y
ASF1700F
FF201
Developing Products
DL828
FF202
ZX-1
Glass Type
Firing Condition
Temp.-Time
SiO2・B2O3
SiO2・B2O3
SiO2・B2O3
SiO2・RO・ZnO
SiO2・B2O3・Al2O3
(℃-min)
850-60
850-60
850-60
850-60
900-60
SiO2・B2O3・R2O
SiO2・Al2O3・RO
SiO2・Al2O3・RO
900-60
900-60
900-60
Thermal
Viscosity Property ( DTA )
Electrical Property
CTE
Specific Transformation Softening Crystallization Dielectric Dielectric
Expansion
Measuring
Temp range
Gravity
Coeff.
Point
Point
Temp.
Constant
Loss
Condition
(℃)
-4
(×10-7/℃)
(℃)
(℃)
(℃)
ε
tanδ(X10 )
28
50-350
2.2
495 *1
790
4.0
1MHz 25℃
28
50-350
2.2
495 *1
762
4.0
1MHz 25℃
28
50-350
2.2
495 *1
775
4.0
1MHz 25℃
72
25-300
3.6
671
810
923
9.0
1MHz 25℃
50
40-750
2.6
720
840
1040
6.0
1MHz 25℃
35
89
75
25-300
30-300
25-300
2.3
3.5
2.9
712
750
861
801*2
875
961
959
4.2
6.6
6
1MHz 25℃
16GHz 25℃
Average
Particle
(µm)
-
Particle Property
Particle Size
Sieving Size
(D50)
Mesh Pass
(µm)
3.3
24
1.0
24
1.3
24
1.8
200
17
100
1.0
4.7
2.5
-
Major Application
Glass
Characteristi
cs
Multilayer Substrate
Multilayer Substrate
Multilayer Substrate
Multilayer Substrate
Multilayer Substrate
Vitreous
Vitreous
Vitreous
Devitrifying
Devitrifying
Low ε
Low ε
Low ε
Multilayer Substrate
Multilayer Substrate
Multilayer Substrate
Vitreous
Devitrifying
Devitrifying
Low ε
High CTE
Low tan δ
Feature
Low ε
*1 Transformation point of TMA curve. *2 Third inflection point on DTA curve
P.5
GLASS PASTE
AGC glass pastes consist of powder glass and the vehicle. They are widely used in the electronics industry for applications requiring extremely high precision and reliability,
such as thick-film hybrid ICs, thermal print heads, etc., in which they have an excellent track record.
Long years of experience and advanced technical know-how, from the design of recipes for the ingredients, through the melting and grinding to the mixing of the paste, and the
strictest quality control regime, are the secrets of our integrated production system.
Our continuous ongoing policy of improvement ensures that our pastes secure the widest possible use throughout the electronics industry, with improving ease of use and other
distinctive features.
Be sure to remember the following considerations when using Asahi Dielectric Glass Pastes:
●Storage locations
Avoid direct exposure to sunlight and store in a cool, well-ventilated place.
Please use within six months of receipt.
Please ask the sales person about expiry date of each pastes.
●Adjusting viscosity
Pastes have been prepared for use without further adjustment but, if necessary,
recommended thinner can be used to adjust their viscosity.
●Mixing
Mix thoroughly before use, taking particular care not to cause air bubbles.
●Application
Pastes should be applied in a well-ventilated area. Take particular care not to continue
breathing the vapor for any considerable length of time, and do not allow the paste to
remain in contact with the skin.
P.6
GLASS PASTE
AGC Overcoat Glass Paste for Hybrid IC
Code
Glass Type
SiO2・B2O3・PbO
AP5346
B2O3・ZnO・PbO
AP5550
B2O3・ZnO・PbO
AP5551
SiO2・PbO
AP5840N
Developing Products
SiO2・ZnO・Bi2O3
5033NF1
SiO2・B2O3・R2O
5102Y
SiO2・B2O3・Bi2O3
AP5094D
SiO2・B2O3・ZnO
YPT525
Bi2O3・B2O3・ZnO
YPT531E
Firing Condition
Temp.-Time
(℃-min)
510-5
550-5
550-5
550-5
Viscosity Property ( DTA )
Electrical Property
Thermal
Expansion Specific Transformation Softening Crystallization Insulation Breakdown
Gravity
Coeff.
Point
Point
Temp.
Resistance Voltage
ε
(×10-7/℃)
(℃)
(℃)
(℃)
(Ω)
(V)
10
>500
8~12
73
400
490
>10
47
455
540
>500
7~12
>1010
10
47
455
540
>500
7~12
>10
61
2.2
460
560
-
580-10
850-60
520-10
580-30
590-30
90
28
85
72
77
-
450
450
470
500
565
775
510
580
590
600
-
-
-
5~7
11~13
tanδ
(%)
<0.5
<0.5
<0.5
-
Paste Viscosity
Surface Roughness
Particle Property
Glass
Average Particle Size
Ra
Rz
η10
Viscosity
Characteristics
ratio
Particle
(D50)
(µm)
(µm)
(Pa・s) η10/η50 (μm)
(μm)
170
2.0
1.2
-
Vitreous
150
2.1
2.0
-
Devitrifying
150
2.1
2.0
-
Devitrifying
80
1.4
2.0
-
Vitreous
100
100
110
100
100
1.4
-
-
-
-
1.9
1.3
0.7
2.5
2.5
Devitrifying
Vitreous
Vitreous
Vitreous
Vitreous
Color
Paste
Green
White
Green
Green
Fired
Glass
Green
White
Green
Green
Black
White
Yellow
White
White
Black
Clear
Yellow
Clear
Clear
AGC Dielectric Crossover Paste for Hybrid IC
Code
AP5576VE
AP5577
AP5578
AP5700C
AP5701C
AGC Dielectric
Code
AP5761D
AP5762D
AP5762-10
Viscosity Property ( DTA )
Electrical Property
Thermal
Expansion Specific Transformation Softening Crystallization Insulation Breakdown
Gravity
Coeff.
Point
Point
Temp.
Resistance Voltage
ε
(℃-min)
(×10-7/℃)
(℃)
(℃)
(℃)
(Ω)
(V)
SiO2・ZnO・RO
850-10
53
670
785
830
>1000
9~14
>1012
SiO2・ZnO・RO
850-10
53
1.9
670
785
830
>1000
10~16
>1012
12
SiO2・ZnO・RO
850-10
53
1.9
670
785
830
>1000
12~17
>10
SiO2・ZnO・RO
850-10
72
680
815
890
>1000
9~14
>1012
SiO2・ZnO・RO
850-10
72
680
815
890
>1000
9~14
>1012
Paste for Alumina Substrate Glazing of Print Head
●By controlling crystalline
Viscosity Property ( DTA )
Electrical Property
Firing Condition
Thermal
Temp.-Time
Expansion Specific Transformation Softening Crystallization Insulation Breakdown
Glass Type
Gravity
Coeff.
Point
Point
Temp.
Resistance Voltage
ε
(℃-min)
(×10-7/℃)
(℃)
(℃)
(℃)
(Ω)
(V)
SiO2・B2O3・RO
1275-60
69
710
870
SiO2・RO
1270-30
65
765
925
SiO2・RO
1200-60
65
1.8
765
925
Glass Type
Firing Condition
Temp.-Time
Paste Viscosity
Surface Roughness
Particle Property
Color
Glass
Average Particle Size
η10
Ra
Rz
Viscosity
Characteristics
ratio
tanδ
Particle
(D50)
Paste
Fired
(%)
(µm)
(µm)
Glass
(Pa・s) η10/η50 (μm)
(μm)
<0.2
190
2.4
1.6
-
Devitrifying
Orange White
<0.3
190
1.7
1.6
-
Devitrifying
Blue
Blue
190
1.8
1.6
-
Devitrifying
Black
Black
<0.2
200
2.3
1.6
Partially
Orange White
<0.2
200
2.3
1.6
Partially
Blue
Blue
refraction, a smooth-surface glaze can be formed, (AP5761D, AP5762D)
Paste Viscosity
Surface Roughness
Color
Particle Property
Glass
Average Particle Size
η10
Ra
Rz
Viscosity
Characteristics Paste
ratio
tanδ
Particle
(D50)
Fired
(%)
(µm)
(µm)
Glass
(Pa・s) η10/η50 (μm)
(μm)
160
2.2
5.2
Vitreous
Orange Clear
160
1.9
5.0
Vitreous
Blue
Clear
150
1.7
5.0
Vitreous
Black
Black
AGC Overcoat Glass Paste for Print Head
Code
AP5349
AP5352B
AP5564G
AP5565H
AP5568
AP5316A
AP5317*3
AP5717*3
Developing Products
5315HT101-A5
THN24
Glass Type
Firing Condition
Temp.-Time
PbO・B2O3・SiO2
PbO・B2O3・SiO2
SiO2・B2O3・PbO
SiO2・PbO
SiO2・PbO
SiO2・B2O3・RO
SiO2・B2O3・RO
SiO2・ZnO・RO
(℃-min)
810-10
810-10
830-10
830-10
830-10
810-10
850-10
850-10
SiO2・B2O3・RO
SiO2・B2O3・RO
780-10
830-10
Viscosity Property ( DTA )
Electrical Property
Thermal
Expansion Specific Transformation Softening Crystallization Insulation Breakdown
Gravity
Coeff.
Point
Point
Temp.
Resistance Voltage
ε
(×10-7/℃)
(℃)
(℃)
(℃)
(Ω)
(V)
62
460
>1500
63
455
51
565 *1
670
58
623 *1
678 *2
59
555
55
2.3
580
720
>1500
45
2.0
580
750
35
2.2
675
800
830
68
60
1.9
2.0
625
630
780
760
-
-
>1500
>1500
-
tanδ
(%)
-
Surface Roughness
Paste Viscosity
η10
Ra
Rz
Viscosity
ratio
(Pa・s) η10/η50 (μm)
(μm)
105
2.7
<0.8
110
2.4
<0.1
100
2.6
<0.3
130
3.1
<0.3
90
2.5
<0.3
85
1.6
<1.5
90
1.8
<0.8
150
1.3
100
100
-
<0.8
<0.3
Particle Property
Color
Glass
Average Particle Size
Characteristics
Particle
(D50)
Paste
Fired
(µm)
(µm)
Glass
1.5
Vitreous
Gray
Brown
1.5
Vitreous
Black
Black
0.8
0.9
Vitreous
Orange Clear
0.7
Vitreous
Blue
Clear
0.8
Vitreous
White
Clear
1.5
Vitreous
Gray
Gray
1.5
Vitreous
Gray
Gray
2.5
Devitrifying
White
White
-
2.0
2.0
Vitreous
Vitreous
Gray
Blue
Gray
Blue
●Outstanding surface flatness, resistance to wear, and heat resistance make them ideal as over coats for various kinds of print heads, including heaters, image sensors and thermal heads.
*3 AP5317 and AP5717 are for AIN coat. (AP5317 : Top layer, AP5717 : Bottom layer)
AGC Low Tememperature sealing Glass Paste
Code
Glass Type
Firing Condition
Temp.-Time
(℃-min)
Developing Products
SiO2・B2O3・PbO
5290E
5115HT1
Bi2O3・ZnO
TNS062-Z27-TP12 TeO2・V2O5
430-10
450-10
380-10
Viscosity Property ( DTA )
Electrical Property
Thermal
Expansion Specific Transformation Softening Crystallization Insulation Breakdown
Gravity
Coeff.
Point
Point
Temp.
Resistance Voltage
ε
(×10-7/℃)
(℃)
(℃)
(℃)
(Ω)
(V)
78
75
80
3.1
3.4
2.2
340
355
270
405
415
325
-
-
-
-
tanδ
(%)
-
Paste Viscosity
Surface Roughness
Particle Property
Glass
Average Particle Size
Ra
Rz
η10
Viscosity
Characteristics
ratio
Particle
(D50)
(µm)
(µm)
(Pa・s) η10/η50 (μm)
(μm)
90
100
140
2.5
2.5
2.6
-
-
-
3.5
-
Vitreous
Vitreous
Vitreous
Color
Paste
Fired
Glass
White
Gray
Brown
White
Black
Brown
P.7