Analytical Resources, Inc. :: Price List Thank you for your interest in Analytical Resources, Inc. (ARI). Our laboratory has been providing high quality analytical data in a timely manner since 1985. During this time, we have developed outstanding reciprocal working relationships with many regional, national and international clients. ARI has enhanced these relationships by providing exceptional client service before, during and after the analysis. At ARI we believe that excellent client service is as important to our business as providing high quality data. As our valued client, you will be assigned a Project Manager (PM) who will serve as your interface with the laboratory. Your PM will assist you in setting up analytical projects to meet your objectives, confirm that the laboratory is prepared to receive your samples, keep you apprised of the performance of the laboratory during the completion of your project, and follow up to ensure that you receive high quality data. After you have received your final data report, your PM will be available to answer questions about the analyses. Please feel free to call any of the PMs listed below at any time. They will be happy to answer any questions concerning the analytical process. Ms Kelly Bottem (Client Services Manager) 206-695-6211 Mr. Mark Harris (PM) 206-695-6210 Ms. Cheronne Oreiro (PM) 206-695-6214 The following prices are based upon single analyses with standard data deliverables and turn around times. Discounts are often available based on the total number of samples and the duration of a given project. Surcharges may be applied for expedited turn-around, high-level deliverables or electronic formats. PMs will gladly provide a quote for a specific scope of work. Special R&D projects may be scheduled on a time-and-materials basis. ARI's prices include sample containers delivered to your facility within the continental US. International or expedited shipping costs are not included. Pre-arranged sample pick-up in the Seattle area may also be provided at no additional charge. Additional information about our laboratory's capabilities and experience is available in ARI's Statement of Qualifications (SOQ). You are welcome to download an SOQ from our website, http://www.arilabs.com/. We invite you to put our decades of analytical experience and innovation to work in your environmental projects. 01/11/15 06:13:12 Price List: General Information Hazardous Waste: ARI reserves the right to charge a disposal fee not to exceed $20.00 per sample. ARI also reserves the right to return any sample to the Client. All samples containing PCB concentrations in excess of 50 ppm will incur a disposal fee of $50.00 per sample due to transportation and disposal costs. Holding Times: ARI will make every attempt to meet holding times specified in the applicable methodology or in the contractual agreement, however, if samples are received at the lab more than 48 hours after collection, holding times may be in jeopardy. If that is the case, ARI will make its best effort to advise the Client of the situation and available options. ARI reserves the right to assess rush surcharges for samples received with less than 72 hours remaining in the holding time from collection. These charges may also be applied if analytical requirements for already delivered samples are not received until there is less than 72 hours left in the holding time. Hours of Operation: ARI will accept deliveries of samples at its premises Monday through Friday (except holidays) between the hours of 7:00 a.m. and 6:00 p.m. (Pacific Time). If samples are to be delivered before 7:30 am or after 6:00 p.m. on a business day, or on a Saturday, Sunday, or holiday, the Client must pre-arrange the delivery at least 24 hours in advance. Samples accepted at the premises after 3:00 p.m. on any day may be logged into the ARI LIMS data system on that day, but the turnaround time may be calculated starting the following morning at 7:30 am. In order to provide a supportive work environment, ARI reserves the right to refuse samples with short holding times around scheduled holidays. ARI will publish a list of dates surrounding scheduled holidays during which time sensitive samples will not be accepted. This list will be furnished to all clients at least 30 days in advance of the holiday period. Adherence to holding times may not be guaranteed for samples delivered within these specified holiday periods. Minimum Fee: A minimum charge is required for sample log-in and processing at a rate of seventy dollars ($70) per work order received or $25 per sample received, whichever is greater. This charge applies even if samples are placed on hold and then cancelled. Minimum sample charges will be applied to several analyses, as noted within the price list. The minimum charge will be three times the sample charge, for one, two or three samples analyzed if no other samples of the same matrix are in-house for that test. Reporting Limits: ARI's reporting limits are based on method detection limit (MDL) studies, calibration levels and demonstrated analyte response. These limits take into account sample weights or volumes, and extract or digest volumes as specified in ARI's Standard Operating Procedures (SOP). Reporting limits are matrix dependent. The sample matrix may preclude achievement of published reporting limits. ARI's analysts will endeavor to analyze samples as concentrated as possible based on the matrix. It is at the discretion of ARI to define the point at which sample overload will damage the analytical system. If insufficient sample volume is received by the laboratory to achieve published reporting limits for a specified analysis, the Project Manager (PM) will inform the Client and discuss options for reporting elevated limits or re-sampling. Sample Disposal: ARI will archive water samples for up to 90 days and soil samples for up to 90 days after submission of the final report, and frozen solids or tissues for one year from collection. After these time allotments have expired, ARI will 01/11/15 06:13:12 return the samples to the Client or dispose of the samples appropriately. ARI reserves the right to charge for storage of samples beyond the standard time allotments or for samples not analyzed. In the event that ARI is unable, after reasonable effort, to obtain removal of any contaminated or hazardous materials, the Client agrees to accept the return of such samples to its facilities for the proper disposal of same. ARI agrees that such waste will be transported in a safe and environmentally sound manner as to prevent any waste from entering the environment as a pollutant. Such costs of preparation for transport and actual costs of transfer shall be borne by the Client. Sample Holds: Samples received on hold will be billed the minimum of $25 per sample. If requested, ARI will hold samples past the sample disposal date noted above, at a rate of $10 per sample container per month until one year after sampling. Hold charges are $15 per container per month after the first year. Hold charges are in addition to any other processing or analytical fees applied to the samples. Special Services: Odd or difficult matrices that require extraordinary treatment or method development prior to analysis will be billed time and materials for development. Turnaround Time: Turnaround time (TAT) consitutes the number of working days between sample receipt before 3 pm and due date for delivery of the analytical results (COB). If the due date falls on a weekend or holiday, the TAT will extend to the following business day. ARI shall make every reasonable effort to meet any due dates quoted or acknowledged. Standard turn-around for analytical results is normally three weeks for sediments and tissues, two weeks for waters and soils, subject to the scope of work and current lab capacity. Standard Rush Charges Same Day TAT or < 24 hours (evening delivery, morning data) Call for quote not available for most parameters 1-2 Business Day TAT 100% Surcharge not available for sediments or tissues 3 Business Day TAT 75% Surcharge soils/ waters 100% for sediments or tissues 4 - 5 Business Day TAT 50% Surcharge 75% for sediments or tissues 6 - 9 Business Day TAT 25% Surcharge 50% for sediments or tissues 10- 14 Business Day TAT for sediments & Tissues 25% Surcharge Upon the request of the Client, and subject to ARI's approval, ARI may agree to use its best efforts to perform services for the Client on an expedited basis. ARI reserves the right to assess a surcharge for expedited (RUSH) services. In the event that expedited services cannot be performed and the results thereof provided in writing by the specified date, ARI will, subject to the provisions and to the extent available, provide verbal results by telephone to the Client on such specified date to fully satisfy its obligations. 01/11/15 06:13:12 Price List: Additional Terms and Conditions Acceptance, Samples: To ensure correct receipt and handling of your sample, please forward an ARI Chain-of-Custody form, or equivalent, containing at a minimum the following information: • Full name, address and phone number for invoicing purposes; • Purchase order number (if applicable); • Full name and address of the person to whom the data report is to be mailed; • Complete details of analyses required, sample identification number, time/date sample was collected, sample matrix, analyses requested, hazard identification, requested turnaround time, quote number (if applicable) and fax number. ARI will accept a sample or group of samples by signing the accompanying Chain-of-Custody record(s). Prior to ARIs acceptance of any sample, the entire risk of loss of or damage to such sample shall remain with the Client. In no event will ARI have any responsibility or liability for the action or inaction of any carrier handling shipment or delivery of samples to ARI. Acceptance, Agreement: Clients may order analytical or related services from ARI by purchase order, by telephone (followed by written confirmation from the Client), by e-mail, by fax, or by a negotiated contract. Any such order by Clients shall constitute acceptance of ARI's offer to do business with the Client under these Terms and Conditions. Client's delivery of samples to ARI shall also constitute acceptance by Client of these Terms and Conditions. Assignment: This agreement is not intended to create any rights in any third party, including any party with whom the Client has contracted, except as expressly provided herein. Changes: Any changes to this agreement must be confirmed in writing by ARI and the Client. If changes are made after the originally requested testing is initiated or has been completed, the Client must accept payment responsibility for those services. ARI is not responsible for holding times that are exceeded due to such changes initiated by Clients. Client Disclosure: The Client warrants that any sample containing any hazardous substance will be packaged, labeled, transported, and delivered in accordance with applicable laws and that the presence of any known or suspected hazardous substances be disclosed in writing, prior to or accompanying any shipment. Collection: In the event of default in payment of services rendered, the Client is responsible for reasonable collection/legal fees. Confidentiality: All sample data are confidential to the Client paying for the services. ARI will not release the data to a third party without authorization from the Client. Credit: 01/11/15 06:13:12 In the absence of an established credit arrangement and/or an authorized purchase order, all sample charges must be pre-paid prior to processing. Delivery: ARI will prepare and deliver to the Client a written report of the results of ARI's services with respect to a sample upon completion of all services ordered for that sample. For most services, the Client may designate the format and content of such report in accordance with one of ARI's standard report formats (see Data Deliverables Summary). Verbal, fax, or e-mail preliminary results may be given in advance of the final written report of results. Such preliminary results are tentative results only and are subject to change based upon ARI's Quality Assurance review procedures. ARI shall not be liable in any way for damages incurred by the Client as a result of the Client's relying on verbal, fax, or e-mail preliminary data. Discounts: Economy-of-scale discounts are available and are determined by the number of samples and the nature and scope of the requested analyses. Quotations are provided free of charge. For established Clients, discount rates are re-evaluated annually, and a new rate is applied to future invoices based upon the previous year's volume of work, type of analyses, ease of scheduling, and work continuity. For Clients with intermittent analytical needs, discounts may be extended based upon the quantity of work submitted at one time. Disputes: In the event that a dispute should arise to the performance of the services to be provided under this agreement, and should that dispute result in litigation, it is agreed that the prevailing party shall be entitled to recover all reasonable costs incurred in the defense of the claim, including staff time, court costs, attorney fees, and other claim-related expenses. Documents: The documents ARI furnishes to Client are intended for Client's exclusive reliance and internal use and not for advertising or other types of general distribution or publication. Client agrees to obtain ARI's written permission for any exception. Any unauthorized use or distribution shall be at Client's sole risk without liability to ARI. Entire Agreement: Unless superseded by a signed contract, these standard Terms and Conditions are an integral part of the agreement between ARI and Client. Further, the agreement, including these Terms, constitutes the entire agreement between ARI and Client relating to the project and any written or oral representations, assurances, commitments, or agreements by ARI not contained herein are void. Expert Services: Should ARI be requested to provide expert testimony or consulting services related to this agreement, ARI shall be compensated at the prevailing rate charged for similar services in the US. The parties shall reach written agreement as to ARI's compensation before ARI shall provide such services or testimony. Fee Schedule: Prices are subject to change without notice. Prices listed herein include one original hardcopy of the analytical report in ARI Type 1 or 2 format sent by US mail. Prices also include electronic deliverables in ARI's ARIEL format upon request. Additional charges will apply for specific QA/QC hardcopy report formats, such as EPA CLP or PSDDA QA2 data deliverables (see Type 3 and 4 in Data Deliverables section). Additional charges may apply for customized 01/11/15 06:13:12 hardcopy or electronic deliverables that differ significantly from the standard ARI formats. ARI's prices include sample containers delivered to the Client's facility within the continental US. International shipping costs are not included. ARI reserves the right to invoice for Client-specified rush delivery or special handling of sampling containers. Force Majuere: ARI shall not be responsible for non-performance or delay in work to be performed caused by Client, Client's employees, agents, or contractors, or caused by factors beyond ARI's control such as acts of governmental authorities, unanticipated physical conditions not now known, labor disputes, or natural disasters. Indemnity: The Client shall indemnify and hold harmless ARI from any and all claims, suits, judgments, damages, losses, liabilities, expenses, payments, taxes, duties, fines, and/or other costs (including but not limited to liability to other parties) arising out of (a) the presence of hazardous substances in any sample of the Client, (b) accidents occurring during shipment and delivery of any sample, (c) events or delays caused by the Client or its agents, (d) negligence by the Client in use, interpretation, or application of results provided by ARI. Tests and observations will be conducted using appropriate test procedures and laboratory protocols. If the Client requests test procedures that vary from our standard or recommended procedures, Client agrees to hold ARI harmless from all claims, damages, and expenses arising out of that direction. Inspection: The Client may inspect ARI's facilities at its premises during normal business hours. ARI may limit or deny inspection privileges if, in the reasonable judgment of ARI, such limitation or denial is necessary or advisable for reasons of health, safety, protection of ARI's competitive position and/or preservation of confidential information. Insurance: ARI represents and warrants that it and its agents, staff and consultants employed by it, is and are protected by worker's compensation insurance and that ARI has such coverage under public liability and property damage insurance policies which ARI deems to be adequate. Certificates of all such policies of insurance shall be provided to Client upon written request. Intellectual Property: Methods, procedures, innovations, discoveries, and equipment developed and employed by ARI for any specific analytical project shall remain the sole property of ARI unless otherwise agreed upon in a signed contract with Client. Law, Governing: The validity and construction of these Terms and Conditions shall be governed by the laws of Washington. In the event of any dispute relating to or concerning these Terms and Conditions, the parties hereto will submit exclusively to the jurisdiction of any court of competent jurisdiction sitting in the state of Washington, and will comply with all requirements necessary to give such court exclusive jurisdiction thereof. Liability: The liability and obligation of ARI is limited to repeating the services performed or, at the sole option of ARI, refunding in full or part fees paid by the Client for such services. Repeating the services may be subject to the Client providing at the Client's expense an additional sample, when necessary, due to expired analytical holding time or insufficient sample volume available to repeat the service. Except for the provisions specifically stated herein, ARI shall have no liability, obligation, or responsibility of any kind for any losses, costs, expenses, or damages (including 01/11/15 06:13:12 but not limited to any special, indirect, incidental, or consequential damages) for any representation or warranty of any kind with respect to ARI's services. No action, regardless of form, arising out of or brought in connection with any services provided under this agreement may be brought by the Client more than one (1) year after the performance of said services by ARI. It is expressly agreed that ARI shall have no liability to Client unless the liability arises out of the willful misconduct or gross negligence of ARI or its duly authorized employees. Notices: Client shall promptly inspect completed data packages and shall notify ARI of any defects or nonconformity within thirty (30) days of receipt. Failure to provide timely notification to ARI, or provide payment for services which Client had the opportunity to inspect, shall be considered acceptance of such services except as to latent defects which reasonable and timely inspection would not have revealed. Payment: All fees are charged or billed directly to the Client. The billing of a third party will not be accepted without a statement, signed by the Client and third party, which acknowledges and accepts payment responsibility. If Client directs ARI to invoice a third party, Client agrees to be responsible for ARI's compensation until ARI receives the third party's written acceptance of all terms of our agreement and until ARI agrees to extend credit to that party. Unless ARI's written acceptance of a billing substitution is given prior to acceptance of samples, Client agrees to be responsible for ARI's compensation even if the third party is subsequently accepted by ARI. In the event Client fails to pay ARI within sixty (60) days following the invoice date, ARI may consider the default a total breach of this agreement and ARI may, at its option, terminate all duties without liability to Client or to others. Retention of Samples and Records: After analytical results have been reported to the Client, ARI shall retain copies of the reports and all associated raw data for a period of 7 years, after which all documentation will be recycled. If the Client requests additional copies of analytical reports during the retention period, ARI reserves the right to assess additional charges for the preparation of such reports. It will be at the discretion of the laboratory Project Manager to assess these charges. Sample Delivery Group (SDG): An SDG consists of any group of twenty or fewer samples of the same matrix, designated for the same analysis, and received within a 7 day period. Scheduling: Scheduling of samples and delivery of reports as detailed in the turnaround specifications in the SOW are subject to the following conditions: a) the samples are received within the time periods originally agreed upon in the attached Schedule or Statement of Work (SOW) and the corresponding ARI quotation to Client, and b) there is no identifiable matrix interference associated with the sample(s). Services: Where applicable, ARI will use analytical methodologies that conform to US Environmental Protection Agency (EPA), state agency, American Society for Testing and Materials (ASTM), Association of Official Analytical Chemists (AOAC), Standard Methods for the Examination of Water and Wastewater, Puget Sound Estuary Protocols (PSEP), or other recognized methodologies if necessary; or appropriate due to the nature or composition of the sample or otherwise based on the sole judgment of ARI. Occasionally, project circumstances may require non-traditional analytical methodologies that are not identical to EPA, state or agency protocol. Such testing will be undertaken in a manner consistent with recognized scientific analytical procedures and good laboratory practices. Standard Operating Procedures (SOPs): 01/11/15 06:13:12 ARI performs all analytical procedures according to method-specific SOPs. These documents are available to our Clients upon verbal or written request. The Client must review and sign an agreement of non-disclosure prior to release of any SOP. All SOPs remain the property of ARI. Subcontracting: ARI will not subcontract any samples to other laboratories, for any reason, without first notifying the Client. If subcontracting is necessary, samples will be sent only to analytical laboratories that are pre-approved by ARI's Client. Suspension: ARI is aware that field or project conditions sometimes change. Client may order performance of all or any part of the services suspended at any time by written notice. ARI may refuse to resume performance of the suspended services at its discretion, and shall be compensated for services completed through receipt of the notice, and for the reasonable cost of suspending and resuming work. Use of Data: All results provided by ARI are strictly for the use of the Client and ARI is in no way responsible for use of such results by the Client or third parties. All results should be considered in their entirety and ARI is not responsible for the detachment, separation or other use of any portion of the results. Data produced by ARI are ARI's property until the bill for the analytical work is paid. Waiver: Failure by either party to enforce any of the terms in any particular instance shall neither constitute a waiver of its rights under this agreement, nor shall it constitute a continuing waiver or preclude subsequent enforcement thereof. Warranty: ARI will perform its services using that degree of care and skill ordinarily exercised under similar conditions by reputable members of ARI's profession practicing in the same or similar locality. No other warranty, expressed or implied, is or has been made by ARI. "ARI" shall mean "Analytical Resources, Inc." and its employees, servants, agents and representatives. "Captions or Descriptive Titles" of the Sections of these Terms and Conditions are solely for convenience of reference and shall not define, limit or affect in any way the provisions, terms and conditions hereof or their interpretation. "Client" refers to the person or business entity ordering the services to be performed. "Fee" shall mean the amount or sum payable to ARI by the Client for ARI's services rendered. "Hazardous Substance" shall mean any material or substance of any kind which is, or potentially is, poisonous, toxic, radioactive, explosive, flammable, or otherwise hazardous, or the handling, transport, disposition and/or disposal of which poses, or potentially poses, any hazard or risk to the environment or the safety and health of persons handling it. Premises shall mean the site of ARI s laboratories and facilities. Quotation shall mean ARI s standard form of Sales Quotation (as such form may be amended from time to time by ARI), appropriately completed, and executed by an authorized representative of ARI (whether or not executed by the Client). Receipt Date shall mean the date on which a sample is delivered and accepted by ARI. 01/11/15 06:13:12 Sample or Samples shall mean any material or substance delivered by the Client to ARI hereunder on which one or more specific tests or analytical procedures are (or are to be) performed. A single delivery of material or substance by the Client, whether or not in one or more containers, may comprise one or more samples. Terms and Conditions shall mean these Terms and Conditions and any additions or amendments agreed to in writing by ARI. Work means the specific analytical, testing, or other services to be performed by ARI as set forth in ARI s service agreement, the Clients acceptance thereof and these General Conditions. 01/11/15 06:13:12 General Organics Prices: Dioxane, Dioxin/Furans, BETX, Pesticides, Glycols, Herbicides For pricing on tissues, see our Tissues Prices section. Parameter EPA Method Technique Water/Soil Price Water Soil 1,4-Dioxane only 8270D GC/MS $180 $200 Alcohols (3 sample minimum) 8015 (Mod) GC/FID - direct injection $120 $150 Alkyl PAH 8270-SIM GC/MS-SIM $330 $350 BETX (Volatile Aromatics) 8021-M GC/PID $65 $70 BETX (Low level option) 8021-M GC/PID $75 - Chlorinated Pesticides 8081A GC/ECD $155 $165 Chlorinated Pest (MTCA B) 8081 mod GC/ECD $240 - Chlorinated Pest (~1 ng/L) 8081 mod GC/ECD $260 - Dioxin/Furans 1613/8290A HR-GC/MS $750 $750 DDTs Only (0.5 ng/L) 8082 mod GC/ECD $250 - Chlorinated Phenols 8041(Mod) GC/ECD $150 $155 F-Listed Wastes (3 sample minimum) 8015 (Mod) GC/FID - direct injection $135 $155 Glycols (3 sample minimum) 8015 (Modified) GC/FID-direct injection $115 $120 Herbicides (3 sample minimum) 8151A GC/ECD $165 $260 Non-Halogenated Volatiles 8015 (Modified) GC/FID - direct injection $100 $110 GC/MS-Selected Ion Monitoring $220 $240 OP- Pesticides (3 sample minimum) 01/11/15 06:13:12 8270-SIM General Organics Prices: PCBs, PAHs, PCP, Phenols, Phthalates Parameter EPA Method Technique Water/Soil Price Water Soil PCB Aroclors (Oils - no cleanups) 8082 GC/ECD $55 - PCB Aroclors (Wipes with cleanups) 8082 GC/ECD - $80 PCB Aroclors (1 ug/L or 30 ug/Kg) 8082 GC/ECD $110 $120 PCB Aroclors (0.1 ug/L) 8082 GC/ECD $160 - PCB Aroclors (20 ug/Kg) 8082 GC/ECD - $155 PCB Aroclors (0.01 ug/L) 8082 GC/ECD Manchester $250 - PCB Aroclors (0.01 ug/L / 4-10 ug/kg) 8082 GC/ECD - Low Level $250 $220 PCB Aroclor Confirmation by GC/MS 8270D GC/MS $120 $120 PCB Congeners (5 sample minimum) 8082 GC/ECD call for quote Pentachlorophenol (PCP) 8041A (Modified) GC/ECD $80 $85 Phenols 8270 (Modified) GC/MS $180 $185 Phenols (Chlorinated) 8041A (Modified) GC/ECD $130 $135 Phthalates 8270D (Modified) GC/MS $190 $195 Polynuclear Aromatic Hydrocarbons (PAH) (1 ug/L) 8270D (Modified) GC/MS $180 $185 Polynuclear Aromatic Hydrocarbons (PAH) (0.1 ug/L / 5 ug/kg) 8270D (Modified) GC/MS-SIM $200 $205 Polynuclear Aromatic Hydrocarbons (PAH) (0.01 ug/L) 8270D (Modified) GC/MS-SIM-Low Level $240 - Polynuclear Aromatic Hydrocarbons (PAH) 0.5 ug/kg 8270D (Modified) PAH and PCP (1 and 5 ug/L : 5 and 25 ug/kg) 8270-SIM (Modified) 01/11/15 06:13:12 GC/MS-SIM-Low Level GC/MS - SIM - $200 $250 $240 General Organics Prices: Semivolatiles, EDB/DCBP, Volatiles, TBT, Vinyl Chloride, Gases Parameter EPA Method Technique Water/Soil Price Water Soil Semivolatile Organics 8270D GC/MS $310 $330 Semivolatile Tentatively Identified Compounds (TICs) in addition to analytical cost CLP SOW OLMO4.2 GC/MS $80 $80 Semivolatiles - Isotope Dilution 1625 call for quote Tributyl Tin (Butyl Tin Species) PSEP/Krone (1988) GC/MS-SIM $275 $330 Tributyl Tin (Low Level Option) PSEP/Krone (1988) GC/MS-SIM $295 Dissolved Methane, Ethane, Ethene RSK 175 GC/FID $135 - Dissolved Methane, Ethane, Ethene, Acetylene RSK 175 GC/FID $150 - EDB/DCBP (call for availability) 8011 GC/ECD $90 - Vinyl Chloride 1,1-DCE, TCE, PCE (0.02 ppb) 8260 (modified) GC/MS-SIM $120* Volatile Aromatics (5 analytes) 8260C GC/MS $100 $110 Volatile Organics (solids include Easy Draw 5035 equipment) ** 8260C GC/MS $170 $200 Volatile Organics (0.2 to 1 ug/L) 8260C GC/MS $190 - Volatile Organics (Drinking Waters) 524.2 or 524.3 GC/MS CLP SOW OLMO4.2 GC/MS Volatile Organic Tetatively Identified Compounds (TICs) in addition to analytical cost $190 *Price for analysis when SIM analysis is concurrently analyzed by EPA Method 8260 $100.00. ** Add additional $30 for OEM Encore sampling equipment 01/11/15 06:13:12 $60 $60 Petroleum Hydrocarbon Prices Standard Methodologies Parameter EPA Method Technique Water/Soil Price Water Soil Hydrocarbon Identification (HCID) NWTPH-HCID GC/FID $50 $55 Gasoline Range Hydrocarbons + BETX (soils include 5035 Easy Draw) NWTPH-Gx / EPA 8021 GC/FID/PID $75 $95 Gasoline Range Hydrocarbons + BETX (100 ug/L and 0.08 ug/L) NWTPH-Gx/EPA 8021 (15 mL purge) GC/FID/PID $110 - Gasoline Range Hydrocarbons (soils include 5035 kit) NWTPH-G /AK101/EPA 8015M GC/FID $65 $80 Diesel Range Hydrocarbons or Extented Diesel/Oil Hydrocarbons NWTPH-Dx / AK102/AK103 GC/FID $70 $75 Diesel Range/Oil Hydrocarbons with Acid/Silica Gel Cleanup Ac/Si-NWTPH-Dx / Ac/Si-AK102/103 GC/FID $90 $95 Volatile Aromatics (BETX + MTBE soils include 5035 kit) EPA 8021 GC/PID $70 $85 Oxygenates EPA 8260 GC/MS $140 $150 Technique Price Washington Department of Ecology Interim TPH methods Parameter EPA Method Water/Soil Water Soil Volatile Petroleum Hydrocarbons (VPH) + BETX & MTBE (3 sample minimum) soils include 5035 Easy Draw Kit WDOE GC-FID $150 $175 BETX, MTBE, Naphthalene (confirmation)* WDOE / 8260 GC-MS $80 $85 Extractable Petroleum Hydrocarbons (EPH) Aromatic and Aliphatic Ranges) (3 sample minimum) WDOE GC-FID $160 $175 EPH + PAHs (3 sample minimum) WDOE / 8270 GC-FID / GC-MS $320 $325 *Confirmation analysis by GC/MS only, no VPH range reported ** Three sample minimum charge if no other samples in-house 01/11/15 06:13:12 01/11/15 06:13:12 Metals Common Group Prices: Low Level Hg, Priority Pollutants, CLP TAL List NOTE: All group prices include sample preparation. Common Group Lists receive discount off individual element pricing. Parameter EPA Method Technique Water/Soil Price Water Soil Low Level Mercury 20 ng/L (ppt) Modifed 7470 CVAA: Hg $80 - Priority Pollutant Metals - standard 200.7/6010C 245.1/245.5 7470A/7471A ICP: Ag, As, Be, Cd, Cr, Cu, Ni, Pb, Se, Sb, Tl, Zn CVAA: Hg $165 $175 Priority Pollutant Metals - low level option 200.7/6010C 200.8/6020A 245.1/245.5 7470A/7471A ICP: Ag, Be, Cd, Cr, Cu, Ni, Sb, Zn ICP/MS: As, Pb, Se, Tl CVAA: Hg $210 $220 200.7/6010C 245.1/245.5 7470A/7471A ICP: Ag, Al, As, Ba, Be, Cd, Ca, Cr, Co, Cu, Fe, Mg, Mn, Ni, Pb, K, Na, Sb, Se, Tl, V, Zn CVAA: Hg - $275 $270 $280 EPA-CLP (TAL) - soil option EPA-CLP (TAL) Metals - low level option 01/11/15 06:13:12 200.7/6010C 200.8/6020A 245.1/245.5 7470A/7471A ICP: Ag, Al, Ba, Be, Cd, Ca, Cr, Co, Cu, Fe, Mg, Mn, Ni, K, Na, Sb, V, Zn ICP/MS: As, Pb, Se, Tl CVAA: Hg Metals Common Group Prices: TCLP/SPLP, RCRA, MTCA, Hardness NOTE: All group prices include sample preparation. Common Group Lists receive discount off individual element pricing. Parameter EPA Method Technique Water/Soil Price Water Soil TCLP/SPLP Metalsincludes TCLP extraction * 1311/6010C 7470A ICP: As, Ba, Cd, Cr, Pb, Se, Ag CVAA: Hg $195 $235 RCRA metals 200.7/6010C 245.1/245.5 7470A/7471A ICP: As, Ba, Cd, Cr, Pb, Se, Ag CVAA: Hg $135 $145 MTCA metals - soil 200.7/6010C 7471A ICP: As, Cd, Cr, Pb CVAA: Hg - $105 MTCA metals - water 200.8 245.1/245.5 7470A ICP/MS: As, Cd, Cr, Pb CVAA: Hg $130 - Hardness 200.7/6010C ICP: Ca, Mg (calculation) $65.00 *See TCLP/SPLP section 01/11/15 06:13:12 Metals Pricing Per Element and Sample Preparation Metals Pricing Per Element ** ICP ICP/MS GFAA (with prep) first element or mineral (does not include prep) $35 $35 Call for availability each additional element $11 $16 - each additional mineral (Al, Fe, Ca, Mg, Na, K) $11 $26 - CVA Hg (with prep) - - $35 EPA Method Price Water/Soil Water Soil Strong Acid Sample Digestion 3000 Series $15 $25 TCLP Extraction 1311 $65 $100 SPLP Extraction 1312 $65 $100 m-WET Extraction Title 22 - $150 Clean room sample concentration for low level ICP/MS ARI $60 - Sample Filtration (.45 micron) - $20 - Sample grinding/sieving - call for quote Sample compositing - call for quote Metals Sample Preparation **EPA-CLP (TAL) Metals can also be determined and reported following CLP SOW ILMO4.0. For pricing on tissues, see our Tissues Prices section. 01/11/15 06:13:12 Wet Chemistry Prices: Alkalinity, Anion Chrom., CEC Method Identification Parameter Technique EPA SW-846 SM Price Per Sample other Water Soil 1 to 5 6 to 15 >15 1 to 5 6 to 15 >15 $22 $18 $35 $30 $25 $90 $82 $75 $150 $130 $120 Physical / Inorganics Alkalinity (Total,HCO3, CO3) soil three sample min Titrimetric (pH 4.5) 2320 B-97 $25 Titrimetric (full curve) 2320 B-97 call for quote 4110 B-00 $60 Anion Chromatography* (F,Cl,NO2, Br,NO3, PO4,SO4) Cation Exchange Capacity 1M ammonium acetate 300.0 9056A 9080 Exchangeable 1M bases (cations) ammonium acetate *Anion Chromatography pricing charged by analytical run, not by Anion. 01/11/15 06:13:12 MSA 8 &9 $55 $50 Wet Chemistry Prices: Cr+6, Chloride, Color, Conductivity Method Identification Parameter Technique EPA SW-846 SM Price Per Sample other Water Soil 1 to 5 6 to 15 >15 $55 $50 $45 1 to 5 6 to 15 >15 $65 $60 $50 $65 $60 $50 Physical / Inorganics Chromium, Hexavalent (Cr+6) Diphenylcarbazide - Readily Available Soil Phosphate extract - Soil DI water extract - Soil Alkaline digestion 7196A 3500-Cr B-01 MSA 20-4.3 3060 7196A $75 per sample, 3 sample mininum Chloride - Water Auto-ferricyanide - Soil Water extraction Color Visual comparison 4500-Cl G-97 $25 $20 $17 MSA 10-3 2120 B-01 $20 $15 $12 2510 B-97 $20 $16 $12 $40 $30 $25 $25 $20 $17 $20 $16 $12 Conductivity - Water Electrometric - Soil 1:1 extract - CaCO3 Saturation Ryznar Index Corrosivity pH 01/11/15 06:13:12 9050A MSA 10 2330 9045 $80 $70 $65 Wet Chemistry Prices: Cyanide, Fluoride, Nitrogen Method Identification Parameter Technique EPA SW-846 SM Price Per Sample other Water 1 to 5 Soil 6 to 15 >15 1 to 5 6 to 15 >15 $55 $45 $40 $55 $45 $40 $50 $45 $40 Physical / Inorganics Cyanide PBA colorimetric Note: 335.4 Mod uses manual PBA in place of automated. - Total Acid distillation 335.4 9010C 4500-CN C-99 $50 $45 $40 - Amenable Alkaline chlorination 335.4 9010C 4500-CN G-97 $65 $55 $50 - Weak Acid Dissociable (WAD) Weak acid distillation 4500-CN I $55 $45 $40 4500-F C-97 $30 $26 $23 Fluoride - Water ISE 340.2 9214 - Soil Water extractable Iron, Ferrous (Fe+2) Phenanthroline 3500-Fe B-97 $50 $45 $40 - Ammonia Auto-phenate 4500-NH3 G-97 $25 $22 $18 $40 $35 $25 - Ammonia ISE 4500-NH3 D-97 $30 $26 $22 $45 $40 $30 - Nitrite Auto-NED 4500-NO3 I-00 $25 $22 $18 $40 $35 $25 - Nitrate + Nitrite Cd-red, Auto-NED 4500-NO3 I-00 $25 $22 $18 $40 $35 $25 - Nitrate (NO2+NO3) NO2 4500-NO3 I-00 $40 $36 $32 $50 $45 $38 - Kjeldahl / Organic (TKN / Org-N) Digest, ISE 4500-Norg D-97 $40 $36 $32 $60 $55 $48 MSA 10-3 Nitrogen 01/11/15 06:13:12 350.1 351.4 Wet Chemistry Prices: Diss. Oxygen, pH, Phosphorus, Salinity Method Identification Parameter Technique EPA SW-846 SM Price Per Sample other Water Soil 1 to 5 6 to 15 >15 4500-O C $30 $26 $20 4500-H+ $18 $15 $10 1 to 5 6 to 15 >15 $25 $20 $15 $40 $35 $30 $70 $60 $55 $45 $40 $35 $45 $40 $35 $45 $40 $35 $45 $40 $35 $25 $20 $17 Physical / Inorganics Oxygen, Dissolved Winkler Azide 360.2 - Water Electrometric 150.1 - Soil 1:1 extract pH 9045 9045 MSA 12 Eh/Redox Potential - Water $30 $28 $24 - Soil Phosphorus - Soluble Reactive (ortho-P) Heteropoly blue - Total (strong acid) - Bioavailable 365.2 4500-P E $30 $28 $24 4500 P B $35 $32 $28 Alkaline extraction Horner 1987 - Soil Available Water MSA 24-5.3 Bicarb MSA 24-5.4 Dilute acid MSA 24-5.2 Dilute acid fluoride MSA 24-5.1 Salinity - Conductivity Electrometric 2520 $20 Argentometric Titrimetric 210 C call for quote 01/11/15 06:13:12 $16 $12 Wet Chemistry Prices: Solids Method Identification Parameter Technique EPA SW-846 SM Price Per Sample other Water Soil 1 to 5 6 to 15 >15 1 to 5 6 to 15 >15 Physical / Inorganics Solids * - Total (TS) Gravimetric 2540B 2540G $20 $15 $10 $20 $15 $10 - Total Volatile (TVS) Gravimetric 2540E 2540G $25 $20 $15 $25 $20 $15 - Total Suspended (TSS) Gravimetric 2540D $25 $22 $18 - Volatile Suspended (VSS) Gravimetric 2540E $35 $32 $28 - Total Dissolved (TDS) Gravimetric 2540C $25 $22 $18 - Settleable (SS) Volumetric 2540F $18 $15 $12 * Total Solids Analysis required for all solid samples with conventional parameters 01/11/15 06:13:12 Wet Chemistry Prices: Sulfate, Sulfide, Sulfite Method Identification Parameter Technique EPA SW-846 SM Price Per Sample other Water Soil 1 to 5 6 to 15 >15 $26 $22 $20 1 to 5 6 to 15 >15 $45 $40 $34 $45 $40 $34 $45 $40 $35 $45 $40 $35 Physical / Inorganics Sulfate - Automethymol blue Colorimetric 375.2 9036 4500-SO4 F - Soluble Soil Calcium phosphate MSA 28-3 DI water MSA 10-3 Sulfide - Iodometric Titrimetric 376.1 - Methylene Blue Colorimetric 376.2 - PSEP Total Distillation @ pH <3.5 - SW-846 acid soluble Distillation @ pH <1 - Acid Volatile Distillation @ EPA pH <3 1991 $50 $40 $35 - AVS with SEM* (Cd, Cu, Hg, Pb, Ni, Zn) Distillation @ EPA pH <3 1991 $195 $180 $175 Sulfite Iodometric 01/11/15 06:13:12 9034 4500-S2 F-00 $30 $26 $22 4500-S2 D-00 $30 $26 $22 9030 377.1 4500-SO3 B call for quote Wet Chemistry Prices: Turbidity, O&G, TOC, BOD, COD Conventional Organics Method Identification Parameter Technique EPA SW-846 SM Price Per Sample other Water Soil 1 to 5 6 to 15 >15 $20 $18 $14 1 to 5 6 to 15 >15 $80 $75 $65 $85 $80 $70 $50 $48 $46 $170 $160 $145 $65 $60 $55 Physical / Inorganics Turbidity Nephelometric 180.1 2130 - HEM* Gravimetric 1664 $70 $65 $60 - HEM-SGT** Gravimetric 1664 $75 $70 $65 - HEM* Gravimetric 9071B - HEM-SGT** Gravimetric 9071B - Total Organic Carbon (TOC) NDIR 415.1 - Soil Combust Plumb 1981 - Solid IC, TC >30%Carbon Combust, TC & TOC Plumb 1981 Oil & Grease Organic Carbon 9060 5310 B $40 $38 $36 Chemical Closed reflux Oxygen Demand (COD) 410.4 5220 D $35 $30 $25 Biological Winkler 5-day Oxygen Demand (BOD) 405.1 5210 $55 $50 $45 5210 $55 $50 $45 Carbonaceous BOD Inhibited 5-day - Soil Winkler 5-day * HEM - N-Hexane Extractable Materials ** HEM-SGT - N-Hexane Extractable Materials/Silica Gel Treated 01/11/15 06:13:12 Plumb 1981 Wet Chemistry Prices: Phenols, Microbiological Method Identification Parameter Technique EPA SW-846 SM Price Per Sample other Water Soil 1 to 5 6 to 15 >15 1 to 5 6 to 15 >15 Physical / Inorganics Phenols - With distillation 4-AAP Colorimetric 420.1 9065 5530 $35 $28 $22 9132 9222 B $35 $32 $30 $45 $40 $38 9222 D $35 $32 $30 $45 $40 $38 Biological Characteristics Microbiological - Total coliform Membrane filtration - Fecal coliform Membrane filtration 01/11/15 06:13:12 Geotech Prices: Index Tests Test Sample Volume Price Atterberg Limits, (liquid and plastic limits) ASTM D-4318 16 oz $85 Bulk Density, ASTM D-2937 / D-7263 core or 16oz $30 Bulk Density for Aggregates ASTM C29 core $50 Calcium Carbonate, ASTM D-4373 4 oz $30 Core Logging, (includes, bulk density, moisture content Pocket penetrometer core and Torr Vane readings, digital photos) $55 Extrusion of Shelby Tube Samples $20 NA Grain Size Analysis: - Sieve & Hydrometer Analysis, ASTM D-422/421 16 oz $95 -Sieve ONLY Analysis, ASTM D-422/ C136 16 oz $80 - #200 Wet Wash, ASTM D-1140 16 oz $35 - Large gravelly samples, sieve analysis, > 3.5Kg 32 oz* $125 - Gravel, Sand, Silt, Clay Fractions (ASTM methods) 16 oz $80 - Sieve/Pipette Apparent GS - Gravel, Sand, Silt, Clay Fractions (PSEP methods) 16 oz $100 - Sieve ASTM D-421/422 with Sedigraph X-ray analysis (fines) 2 oz $90 Particle Size Analysis: -Laser Diffraction by Beckman Coulter LS Particle Size Analyzer - PSD 250 mL $55 -Laser Diffraction by Beckman Coulter LS Particle Size Analyzer - Ecology TAPE 1L $65 Moisture Content, ASTM D-2216 4 oz $25 Organic Matter, (loss on ignition), ASTM D-2974 (440 C) 8 oz $38 Specific Gravity of Soils, ASTM D-854 8 oz $45 Textural classification (USDA) 16 oz $95 Total Porosity, Void Ratio (includes specific gravity, % moisture and density) ASTM D7263 core $90 USCS classification, ASTM D-2487 (Includes grain size and Atterberg Limits) 16 oz $190 When core is listed, an intact core tube, of any standard diameter or length is required. 01/11/15 06:13:12 Geotech Prices: Strength and Permeability Tests Test Sample Volume Price California Bearing Ratio, ASTM D-1883: - Three points with varying compactive effort 45 kg $260 core $260 Consolidation: - ASTM D-2435 Method B - Secondary Plot, per load $55 - Corps of Engineers method for very soft sediments 16 oz $420 - Swell, One-Dimensional, ASTM D-4546 core $250 - Collapse Potential, ASTM D-5333 core $250 35 kg $270 - Unconfined compression (QU); ASTM D-2166 core $50 - Unconsolidated, Undrained triaxial compression (UU); ASTM D-2850 core $90 - Consolidated, Undrained triaxial compression (CU) with pore pressure readings; ASTM D-4767 core $420 Moisture-Density Relationship: - Standard/Modified Proctor, ASTM D-698/1557 Triaxial Compressive Strength: - ASTM D-4767, three pressures, three core sections core $1200 -USBR 5750 (Modified ASTM D-4767) one core section, three pressures core $850 core $170 - Flexible Wall, ASTM D-5084 core $285 - Remolding to specified density NA $35 Saturated Hydraulic Conductivity: - Rigid Wall, ASTM D-2434 When core is listed, an intact core tube, of any standard diameter or length is required. 01/11/15 06:13:12 Geotech Prices: Treatability Testing Services Test Chemical Oxidation/Reduction Studies Price quote Stabilization/Solidification: - Mix design, batching and casting samples When core is listed, an intact core tube, of any standard diameter or length is required. 01/11/15 06:13:12 quote Geotech Prices: COE Dredge Material Testing Test Sample Volume Price Standard Elutriate <4 liters ($50 for each additional liter) $150 Modified Elutriate Test, < 4 liters ($50 for each additional liter) $150 Effluent Elutriate Test < 4 liters ($50 for each additional liter) $150 Dredge Elutriate Test (DRET) <4 liters ($50 for each additional liter) $150 Sequential Batch Leach Test <2liters, 4 cycle, Anaerobic ($100 for each additional liter) $600 Thin Column Leach Test Anaerobic, 30 PV $10,360 Column Settling Test -includes cost of monitoring parameters 5 gal/20 gal Modified ASTM consolidation test for very soft sediments Self-Weight Consolidation COE method 01/11/15 06:13:12 $1,450 $400 2 liters solids/6 liters water $280 Geotech Prices: Pore Water Extraction Pore water extraction may be performed aerobic or anaerobic, for a variety of analytes. The sediment is packed into centrifuge bottles, centrifuged, and the free water is decanted off. Additional steps include a second centrifugation or filtration step to clean up the pore water. As a rule of thumb, a 20% recovery rate is good, and the more sandy a sediment, the lower the recovery. Sample amount should be two 32-oz WMG (Wide mouth glass) if possible. Please call for a project specific quote. 01/11/15 06:13:12 Geotech Prices: Contaminant Transport Parameters Test Sample Volume Price Effective Porosity: Includes a hydraulic conductivity test: - Rigid Wall test core $220 - Flexible Wall test core $350 01/11/15 06:13:12 Geotech Prices: Miscellaneous Tests Test Sample Volume Price Miscellaneous Tests: Soil Resistivity (AASHTO T288) 8 oz $45 32 oz $40 Specific Gravity of Coarse Aggregate, ASTM C127 bucket $50 SSC -Sediment Concentration in Water ASTM D3977 32 oz $60 SSC -Sediment Concentration in Water (> 1000 mg/L) ASTM D3977 32 oz $80 AWWA C105 suite of corrosion tests Restivity, pH, Redox potential, Sulfide, moisture 32 oz $173 Specific Gravity of Liquids Crushing Rock 8 oz or less $40 Core Sawing (cutting ends off) $40 When core is listed, an intact core tube, of any standard diameter or length is required. 01/11/15 06:13:12 TCLP/SPLP/WET-m Sample Preparation Prices Parameter Method Price Per Sample Water Soil 1 to 5 6 to 15 >15 1 to 5 6 to 15 >15 Sample Preparation Bottle Extraction (18 hours) EPA 1311/1312 $65 $55 $50 $100 $80 $65 - Highly Contaminated or Multiphasic Samples EPA 1311/1312 $160 $150 $135 $220 $200 $160 Zero Headspace Extraction (ZHE) EPA 1311/1312 $90 $75 $65 $100 $85 $75 WET-m (48 hours with Nitrogen purge) CA Title 22 - - - $150 $130 $120 01/11/15 06:13:12 TCLP/SPLP Sample Analysis Prices Parameter Method Technique Price Per Sample Water 1 to 5 Soil 6 to 15 >15 1 to 5 6 to 15 >15 Sample Analysis (Requires TCLP or SPLP extraction. Extraction prices not included) *TCLP/SPLP Metals** EPA 6010 & 7470 ICP/CVAA $135 $130 $125 $135 $130 $125 *TCLP/SPLP Volatile Organics (12 analytes) EPA 8260 GC/MS $130 $120 $110 $130 $120 $110 *TCLP/SPLP Semivolatile Organics (13 analytes) EPA 8270 GC/MS $280 $260 $240 $280 $260 $240 *TCLP/SPLP Pesticides (7 analytes) EPA 8081 GC/ECD $135 $110 $95 $135 $110 $95 *TCLP/SPLP Herbicides (2 analytes) EPA 8151 GC/ECD $150 $130 $120 $150 $130 $120 Call for quote Call for quote Call for quote TCLP Diesel For target analytes not listed, water analytical pricing applied. TCLP and/or SPLP parameter list available upon request. EP Toxicity Analyses available upon request. Please call for quotation. * Required for complete Toxicity Characteristic analysis. * *Metals List: ICP: As, Ba, Cd, Cr, Pb, Se, Ag CVAA: Hg 01/11/15 06:13:12 PSDDA Analysis Prices Parameter Preparation Method Analysis Method Technique PSDDA Volatiles (8 analytes) 5030 8260C PSDDA Semivolatiles (20 to 200 ug/Kg) 3546 GPC Cleanup if needed PSDDA Pest + HCB/HCBD (including Oxychlordane and Nonachlors) PSDDA PCB (20 ppb) Butyl Tin (Butyl Tin Species) Price Per Sample 1 to 5 6 to 15 >15 GC/MS $120 $110 $100 8270D GC/MS $350 $320 $300 3546 8081A GC/ECD $195 $185 $175 3546 8082 GC/ECD $155 $135 $125 GC/MS-SIM $330 $290 $270 GC/MS-SIM $325 $315 $300 Krone 1988/PSEP Butyl Tin in sediment pore water (including porewater extraction) Resin Acids 3546 8270D GC/MS call for quote Guaiacols (PSEP list) 3546 8270D GC/MS call for quote PSDDA Total Metals ICP: Sb, As, Cd, Cr, Cu, Pb, Ni, Ag, Zn ICP/MS: Se CVAA: Hg 3050/7471 6010C/200.8 /7471A ICP/CVAA $185 $170 $160 Total Solids PSEP Gravimetric $20 $15 $10 Total Volatile Solids PSEP Gravimetric $25 $20 $15 Total Organic Carbon Plumb 1981 or 9060 Combustion $50 $45 $40 Ammonia 350.1 or SM4500-NH3 Auto-phenate $40 $35 $25 Total Sulfides PSEP Distillation $45 $40 $30 Dioxin/Furans 1613/8290A HR-GC/MS $750 $730 $690 01/11/15 06:13:12 Sediment Management Standard Analysis Prices Parameter Preparation Analysis Method Method Technique Volatiles* (Dichlorobenzenes and 1,2,4-Trichlorobenzene) 5030 8260C SMS Semivolatiles 20 to 200 ug/kg - LPAH, HPAH, Phenols, Phthalates and Misc. Extractables Dual scan SIM for problematic compounds 3546 GPC cleanup if needed Price Per Sample 1 to 5 6 to 15 >15 GC/MS $120 $110 $100 8270D full-scan and SIM dual analysis GC/MS $550 $510 $480 3546 8081A GC/ECD $135 $125 $120 3546 8082 GC/ECD $155 $135 $125 3546 8082 GC/ECD $220 $200 $180 SMS Total Metals ICP: As, Cd, Cr, Cu, Pb, Ag, Zn CVAA: Hg 3050/7471 6010C 7471A ICP/CVAA $125 $115 $95 Ammonia - 350.1 or SM4500-NH3 Auto-phenate $40 $35 $25 Total Sulfides - PSEP Distillation $45 $40 $30 - 160.3 Gravimetric $25 $20 $15 - ASTM Gravimetric $40 $38 $35 - PSEP Sieve/pipette $100 $95 $90 1613/8290A HR-GC/MS $750 $730 $690 HCB/HCBD * Only PCBs (20 ug/Kg) PCB (4 ug/kg) Total Volatile Solids Total Volatile Solids for wood wastes (Organic Matter / Loss on Ignition) Grainsize Dioxins/Furans * Semivolatiles Option 1 will meet screening levels for clean samples with high TOC. Option 1 plus Option 1a will meet both PSDDA and SMS levels. Option 2 required to meet screening levels for samples with low TOC values or contaminated samples. For samples with TOC less than 0.78% it is necessary to analyze 1,2,4-Trichlorobenzene by SW8260. For samples with TOC less that 1.7%, it is necessary to analyze HCB by 8081. 01/11/15 06:13:12 Tissues Analysis Prices Reporting limits may be restricted by lipid content. Parameter Method Technique Price Sample Prep (Filleting, Shucking, Grinding, Skinning, Sectioning, Compositing) - per organism quote Total Solids PSEP Oven dry/ Gravimetric $50 PCB Aroclors (20 ppb) -includes GPC cleanups 8082 GC/ECD $200 PCB Aroclors (4 ppb) -includes GPC cleanups 8082 GC/ECD $280 Chlorinated Pesticides 8081A GC/ECD $200 Polynuclear Aromatic Hydrocarbons (5 ug/kg) 8270D (Modified) GC/MS-SIM (including all cleanups) $250 Polynuclear Aromatic Hydrocarbons (0.5 ug/kg) 8270D (Modified) GC/MS-SIM (including all cleanups) $300 Pentachlorophenol 8041A GC/ECD (including cleanups) $160 Lipids Bligh & Dyer (Mod) Gravimetric $75 Mercury 7471A CVAA $45 01/11/15 06:13:12 Price List: Data Deliverables Summary • Several data deliverable formats are available. • ARI will make every effort to meet client needs when special deliverable requirements exist. Deliverables ARI Deliverable Type I II III IV Project Narrative x x x x Chain of Custody Documentation x x x x Data Report (includes method blank results) x x x x x x x x x QA Summary Forms Instrument Calibration Forms Raw Data x TICs for GC-MS analyses ¤ ¤ ¤ ¤ Electronic Deliverables in ARIEL format ¤ ¤ ¤ ¤ CLP_SOW Deliverables ¤ Optional A surcharge will be assessed for data deliverables as listed below Type III and IV Data Deliverables Surcharge (per SDG): GC/MS Volatile Organics 12% with a minimum of $200 per SDG GC/MS Semivolatile Organics 12% with a minimum of $200 per SDG GC Organics 15% with a minimum of $200 per SDG Metals 15% with a minimum of $200 per SDG Conventionals (SDG = Sample Delivery Group) 01/11/15 06:13:12 10% with a minimum of $50 per SDG Price List: ARI Electronic Deliverables Format (ARIEL) The following fields are provided in the ARIEL format: ARI ID ARI Sample Identification ClientID Client Sample Identification ProjID Client Project Identification Matrix Sample Matrix Rec Date of Sample Receipt at ARI Prep Date of Sample Preparation Analyzed Date of Sample Analysis Method Analytical Method Identification CAS CAS Number Compound Analyte Identification Value Analytical Value Q Data Qualifier Units Concentration Units The structure of the pipe-delimited text would be as follows: ARI ID|Client ID|ProjID|Matrix|Rec|Prep|Analyzed|Method|CAS|Compound|Value|Q|Units| 070194-MB|MethodBlank|ProjA|Sediment|||07/01/94|SW8260|79-01-6|Trichloroethene|1.0|U|ug/kg 070194-MB|MethodBlank|ProjA|Sediment|||07/01/94|SW8260|127-18-4|tetrachloroethene|1.0|U|ug/kg 070194-MB|MethodBlank|ProjA|Sediment|||07/01/94|SW8260|107060-07-0|d4-1,2-dichloroethane|100||% 070194-MB|MethodBlank|Proj A|Sediment|||07/01/94|SW8260|2037-26-5|d8-toluene|99.8||% 070194-MB|MethodBlank|ProjA|Sediment|||07/01/94|SW8260|460-00-4|bromofluorobenzene|100||% 070194-MB|MethodBlank|ProjA|Sediment|||07/01/94|SW8260|2199-69-1|d4-1,2-dichlorobenzene|98.2||% 95-99300-X445B|SampleC|ProjA|Sediment|06/30/94||07/01/94|SW8260|79-01-6|Trichloroethene|1.3|U|ug/kg 95-99300-X445B|SampleC|ProjA|Sediment|06/30/94||07/01/94|SW8260|127-18-4|tetrachloroethene|1.3|U|ug/kg The XLS (Excel) format would have data placed into separate fields as follows: ARI ID 94-17596 94-17596 94-17596 94-17596 Client Method Method Method Method 01/11/15 06:13:12 ID Proj ID Blank Site Blank Site Blank Site Blank Site Matrix Rec Prep Water 10/13/1994 Water 10/15/1994 Water 10/13/1994 Water 10/18/1994 A A A A Analyzed 10/14/1994 10/16/1994 10/14/1994 10/19/1994 Method 10/15/1994 10/17/1994 10/15/1994 10/20/1994 EPA EPA EPA EPA 160.2 350.1 353.2 365.2
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