PLASTOMETRIC TESTING OF 20MnB4 AND 30MnB4

Высокоэффективные технологические процессы в ОМД
Filippov Yulian Kirillovich, doctor of technical sciences, professor, [email protected],
Russia, Moscow, Umech,
Molodov Andrey Viktorovich, candidate of technical science, docent, kiod@mami.,
Russia, Moscow, Umech,
Zaycev Anton Gennadievich, postgraduate, [email protected], Russia, Moscow,
Umech,
Evsicov Roman Aleksandrovich, postgraduate, [email protected], Russia, Moscow,
Umech
УДК 621.77
PLASTOMETRIC TESTING OF 20MnB4 AND 30MnB4
MICROADDITION COLD UPSETTING STEELS AND C45 AND C70
HIGH-CARBON-STEELS
S. Sawicki, H. Dyja, A. Kawałek
The paper presents a method for determining the real steel work-hardening curves
based on the cylindrical specimen compression test. The subject of testing were steels with
micro-additions intended for cold upsetting (20MnB4, 30MnB4) and selected high-carbon
steels of a carbon content from 0,45 to 0,73 % (C42D – C76D). The tests were carried out
using the physical simulator of metallurgical processes GLEEBLE 3800 for the temperature
range of 700…1 200 °C and the strain rate range of 0,1…50,0s-1. Based on plastic deformation parameters recorded during the experiment, mathematical processing, that is the digital
filtration and approximation of the obtained testing results, will be performed. Then, using the
inverse method, the actual values of the coefficients of the numerical models for the rheological properties of the tested materials will be determined.
Key words: steels 20MnB4, 30MnB4, C45, C70, plastometric testing.
1. Introduction. A basis for carrying our the proper simulation and design of technological processes is the knowledge of characteristics describing
the rheological properties of steel. For plastic working processes, the basic feature characterizing material to be plastically formed is the yield stress σp. Determining the σp value of the examined steel is very important when designing
hot rolling processes [1 – 10]. The correct determination of the steel properties
in the form of stress-strain diagrams ensures the subsequent enhancement of calculation accuracy when using empirical formulas, as well as during numerical
computations.
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ТулГУ Технические науки. 2014. Вып.. 10. Ч. 2
Plastometric tests were carried out on the Gleeble 3800 simulator (Fig.
(
1). An overall view
iew of the specimen in testing and the working chamber of the
device is shown in Fig. 2.
Fig. 1.
1 Gleeble 3800 physical simulator
Fig. 2. A specimen in test: 1 – specimen, 2 – anvils, 3 – K-type
type thermocouples,
4 – tantalum or graphite with graphite grease
Coupling a PC with servomotors and sensors in the deformation chamber
enabled continuous recording
ording of examined parameters during plastometric testtes
ing. The yield stress was determined using software supporting the device. By
programming a specific range of temperatures, strains and speeds, the course of
the real rolling process can be simulated. Due to the relatively high strain rates
used during rolling in a continuous rolling mill, but not attainable in the laboralabor
tory, with the use of appropriate relationships it is possible to transpose the conco
version of plastometer test results to the conditions
conditions found in industrial practice.
The yield stress, as dependent on the rolling process parameters, was determined
by the hot compression test. The uniaxial compression test (Fig.
Fig. 3) involved
compressing cylindrical specimens between two well lubricated planes.
pla
The advantage of the uniaxial compression test at elevated temperature is
the fact that the information on the actual stress against the actual strain can be
obtained for a much wider range of strains compared to those examined in the
tensile test.
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Высокоэффективные технологические процессы в ОМД
Fig. 3. Schematic of the compression test
2. Material – testing methods. The steel properties were determined
from tests carried out at high temperatures corresponding to the real rolling conditions. The tests were conducted in a vacuum chamber at the constant temperature of the specimen being deformed. For plastometric tests, D = 10 mm and l =
12 mm cylindrical specimens were used. To minimize the effect of the friction
phenomenon (specimen “barrelling”), tantalum and graphite washers and special
graphite-based grease were put between the specimen faces and the tool surfaces. For the recording and monitoring of temperature variations, two K-type
(NiCr - NiAl) thermocouples were connected to the lateral specimen surface.
The cylindrical specimens were resistance heated using the working anvils.
For cooling, an air blow or non-aggressive liquid medium spray was
used. Thanks to employing such cooling, the material after deformation did not
have any oxide layer on its surface. To reduce the influence of occurring scale,
testing was conducted in a vacuum. The aim of the study was to establish the effect of strain, strain rate and temperature on the magnitude of yield stress in the
temperature range of hot plastic working. Chemical composition of the steels is
given in Table.
Chemical composition of the steels /wt%
Steel
Grade
C45
C70
20MnB4
30MnB4
C
Mn
Si
0,40-0,45
0,68-0,73
0,50-0,80
0,50-0,80
0,18-0,23
0,90-1,20
0,27-0,32
0,80-1,10
0,10-0,30
0,10-0,30
max.
0,30
max.
0,30
P
max.
0,035
0,035
S
max.
0,035
0,035
Cr
max.
0,20
0,15
Ni
max.
0,25
0,20
Mo
max.
0,05
0,05
Cu
max.
0,30
0,25
Al
max.
0,01
0,01
0,025
0,025
0,30
-
-
0,25
-
0,025
0,025
max.
0,30
-
-
0,25
-
The tests in the Gleeble simulator were planned so that it would be possible later to determine the yield stress function and its coefficients during hot
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rolling:
- temperature: 700, 800, 900, 1 000, 1 100 and 1 200 ºC;
- strain rate: 0,1; 1,0; 10,0; 50,0 s-1;
H
- strain: from 0 to 1,3 - ε = ln 0 .
H1
Round specimens of a diameter of 10 mm were heated at a constant heating rate up to the temperature of the upper plastic working limit, that is 1 250
°C, then austenitized at this temperature and then cooled at a constant cooling
rate down to selected temperature values, at which specimen deformation took
place.
3. Testing results. The graphs of the relationship of yield stress versus
the actual strain for a temperature of 900 and 1 100 °C and a strain rate of 0,1
and 10 s-1, respectively, are shown in Fig. 4 – 11.
From the data in Fig. 4 – 11 it can be found that the magnitude of the
yield stress of the examined steels is very strongly influenced by the strain rate
and the deformed metal temperature, for the examined range of these variables.
In the examined range of strain values (0 < ε < 1,3 ) at a temperature of 900 °C,
the highest magnitudes of yield stress σp were obtained for strains in the range
from 0,2 to 0,6 and a strain rate of 0,1 s-1 for steels 20MnB4, 30MnB4 and C45,
while the lowest stress magnitude was obtained for steel C70. With the further
increase in preset strain, the yield stress magnitude either decreased or remained
at a constant level.
300
250
Strain rate
[1/s]
Stress / MPa
200
0,1000
150
1,0000
100
10,000
0
50
0
0,0
0,3
0,6
0,9
1,2
Strain / -
Fig. 4. Strain-stress curves for the steel 20MnB4 at a temperature
of 900 °C
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Высокоэффективные технологические процессы в ОМД
250
200
Strain rate
[1/s] 0,1
100
00
0
1,0
00
0
Stress / MPa
150
50
0
0,0
0,3
0,6
Strain 0,9
/-
1,2
Fig. 5. Strain-stress curves for the steel 20MnB4 at a temperature
of 1 100 °C
250
200
Stress / MPa
150
Strain rate
[1/s] 0,1
00
0
1,0
00
0
100
50
0
0,0
0,3
0,6
Strain 0,9
/-
1,2
Fig. 6. Strain-stress curves for the steel 30MnB4 at a temperature
of 900 °C
300
250
200
Stress / MPa
Strain rate
[1/s]
150
0,
10
00
100
50
0
0,0
0,3
0,6 / - 0,9
Strain
1,2
Fig. 7. Strain-stress curves for the steel 30MnB4 at a temperature
of 1 100 °C
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Известия ТулГУ. Технические науки. 2014. Вып. 10. Ч. 2
300
250
200
Stress / MPa
Strain rate
[1/s]
150
0,
10
00
100
50
0
0,0
0,3
0,6
Strain 0,9
/-
1,2
Fig. 8. Strain-stress curves for the steel C45 at a temperature of 900 °C
250
200
Strain rate
[1/s] 0,1
100
00
0
1,0
00
0
Stress / MPa
150
50
0
0,0
0,3
0,6
Strain0,9
/-
1,2
Fig. 9. Strain-stress curves for the steel C45 at a temperature of 1 100 °C
300
250
200
Stress / MPa
Strain rate
[1/s]
150
0,
10
00
100
50
0
0,0
0,3
0,6
Strain 0,9
/-
1,2
Fig. 10. Strain-stress curves for the steel C70 at a temperature of 900 °C
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Высокоэффективные технологические процессы в ОМД
250
200
Strain rate
[1/s] 0,1
100
00
0
1,0
00
0
Stress / MPa
150
50
0
0,0
0,3
0,6
Strain 0,9
/-
1,2
Fig. 11. Strain-stress curves for the steel C70 at a temperature of 1 100 °C
For a strain rate of 10 s-1 at a temperature of 1 100 °C, the greatest values
of the σp stress were achieved for strains contained in the range from 0,2 to 0,4.
In this case, the greatest yield stress value was obtained for steel 20MnB4.
When examining the curves in Fig. 4 – 11, it can also be found that recovery
processes occur in them during deforming these steels at a small rate. In these
steels for the temperatures indicated in the Fig. 4 – 11, a distinct decrease in
yield stress is observed with increasing strain. This suggests that dynamic recrystallization occurs in the examined steels.
At a strain rate of 10 s-1 and a temperature of 900 °C, the greatest µ p
yield stress magnitudes were obtained for the actual strain contained in the range
from 0,2 to 0,8 for the examined steels. Also in this case, with the continued increase in strain, the yield stress magnitude either decreased or remained at a
constant level. With the increase in temperature, the stress magnitudes decreased, and at a temperature of 1 100 °C the highest µ p stress values were obtained for the strain lying in the range from 0,2 to 0,6.
When examining the curves in Fig. 7 – 8, we observe that during deforming these steels at a strain rate of 10 s-1, dynamic recrystallization also occurs in the steels for the temperatures indicated in the Fig. Only for steel
20MnB4 (Fig. 4) at a temperature of 900 °C is the recovery process no longer so
intensive, and the shape of the curve becomes flat after a certain yield stress
value has been attained. Whereas, from Fig. 4, a strain hardening of the material
can be noticed.
The majority of the curves for the steels investigated in the study have a
similar behaviour for the investigated range of temperatures and strain rates. The
increase in temperature would cause the magnitude of yield stress to decrease.
The increase in strain rate, on the other hand, caused an increase in the yield
stress value. It can be noticed that the yield stress magnitude is influenced by the
temperature, at which deformation takes place, as well as by the strain rate and
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the grade of the examined steel.
4. Summary
- The plastometric tests of micro-addition cold upsetting steels 20MnB4
and 30MnB4 and high-carbon steels C45 and C70 have shown that the magnitude of preset strain, temperature and strain rate have all a great effect on the
magnitudes of yield stress.Plastometric tests enable the subsequent assessment
of the structure and properties of the material after deformation under specific
conditions.
- Based on the plastic deformation parameters recorded during the experiment, the mathematical processing, that is digital filtration and approximation of the obtained test results is possible. Then, using the inverse method, the
actual values of the coefficients in the numerical models describing the
rheological properties of the tested materials will be determined.
- Entering the rheological properties of steel, obtained from plastometric
tests, to computer programs during the numerical examination of plastic working processes ensures a higher accuracy of the computed technological process
parameters to be achieved.
Acknowledgement. This scientific study was financed from the
resources of the National Research and Development Centre in the years
2013–2016 as Applied Research Project No. PBS2/A5/0/2013.
References
1. Gałkin A. M: Badania plastometryczne metali i stopów // Politechnika
Częstochowska. Series Monografie. No. 15. Wydawnictwo Politechniki
Częstochowskiej. 1990.
2. Nowakowski A., Kuźmiński M.: Badania plastometryczne stali
konstrukcyjnych w aspekcie procesu walcowania na gorąco // Wiadomości
Hutnicze 7. 1996. 243-246.
3. Henzel A., Spittel T.: Rasciet energosilovykh parametrov v
processakh obrobotki metallov davlenem // Metalurgia. Moscow. 1982, 34-66.
4. Kawalek A., Rapalska-Nowakowska J., Dyja H., Koczurkiewicz B. :
Physical and numerical modelling of heat treatment the precipitation-hardening
complex-phase steel (CP), Metalurgija 52 (2013) 1, 19 – 22.
5. Laber K., Mróz S., Sygut P., Dyja H.: Analysis of the temperature
change over the continuous ingot length on the parameters of round bar rolling
process // Metalurgija 52. 2013. 1. 39 – 42.
6. Polska Norma PN-83/H-04411: Próba spęczania metali, Polski
Komitet Normalizacji Miar i Jakości, the „Alfa” Standardization Publishers,
Warsaw 1983.
7. Knapiński M., Dyja H., Kawałek A., Frączek T., Laber K.: Analysis
110
Высокоэффективные технологические процессы в ОМД
of the microstructure evolution during thermo-mechanical treatment of the steel
plates in grade X80-X100 // Metalurgija, 52. 2013. 2. 239-242.
8. Milenin A., Młynarczyk J., Knapiński M.: Badanie krzywych
umocnienia stali ST3 w warunkach stanu cieplnego i mechanicznego
występującego podczas ciągłego odlewania // Mechanika 207. 2005. Warszawa,
100-106.
9. Pawlak S.J. Austenite stability in the high strength metastable
stainless steels // Journal of Achievements in Materials and Manufacturing
Engineering. 22. Issue 2. 2007. 91-94.
10. Šimeček P., Hajduk D. Prediction of mechanical properties of hot
rolled steel products // Journal of Achievements in Materials and Manufacturing
Engineering. 2007. V.20. P. 395-398.
Sawicki Sylwester Zdzisław, Associate Professor, Institute of Plastic Working and
Safety Engineering, [email protected], Poland, Czestochowa, Czestochowa University of
Technology, Faculty of Production Engineering and Materials Technology,
Dyja Henryk Stanisław, Professor, Director of Institute of Plastic Working and Safety Engineering, [email protected], Poland, Czestochowa, Czestochowa University of Technology, Faculty of Production Engineering and Materials Technology,
Laber Konrad Błażej, Assistant Professor, Institute of Plastic Working and Safety
Engineering, [email protected], Poland, Czestochowa, Czestochowa University of Technology, Faculty of Production Engineering and Materials Technology
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