Under the patronage of the Custodian of the Two Holy Mosques King Salman Bin Abdulaziz Al-Saud The 3rd Saudi International Conference on Advanced Materials Technology 2015 CONFERENCEMAGAZINE May 18 - 19, 2015 KACST Headquarters - Conference Hall - Building 36 King Abdullah Road - Riyadh, Saudi Arabia THEEVENT The 3rd Saudi International Conference on Advanced Materials Technology 2015 The event is held under the patronage of the Custodian of the Two Holy Mosques, King Salman bin Abdulaziz Al Saud... The 3rd Saudi International Conference on Advanced Materials Technology aims to bring together researchers, developers and end-users in the field of Advanced Materials Technology worldwide to share their novel research activities and to actively discuss emerging challenges facing the increasing demands for developing new materials with a high performance and a cost benefit. While the conference will deal with the broader areas of advanced materials technologies, it will put a special emphasis on advanced materials related to energy, water technology and transportation applications. Advanced Materials Technologies are critical for the future development of Saudi Arabia. There is potential for the Kingdom to become more efficient and competitive in many industries and aspects of life by creating materials with an extremely sophisticated and precisely tailored set of properties... The 3rd Saudi International Conference on Advanced Materials Technology 2015 1 THETRACKS The program is designed to offer a wide range of disciplines on Advanced Materials Technology including the following: TRACK 1 Lightweight Materials: In the last few years, lightweight materials with improvements in durability, energy efficiency and performance have received considerable attention in numerous sectors including aerospace, transportation, energy and biomedical technology. Lightweight materials may generally be classified into three main categories: metal alloys, composites (MMC, PMC and CMC), polymers and ceramics. While the growing demand for lightweight materials is unquestionable, there are different crucial factors in this technology need more improvements in areas such as processing cost, integrity, durability, reproducibility and safety. This session will address the state-of-the-art research activities related to this field. TRACK 2 Advanced Materials for Water and Energy Applications: Recently, water treatments and energy efficiency have been receiving more attention than ever before. It is well-known that materials developments play predominant roles in improving the sustainability of these two sectors. Developments in advanced materials related to membranes and renewable energy are just examples of this strong relationship. This session will focus on the recent materials developments targeting water and energy applications. 2 The 3rd Saudi International Conference on Advanced Materials Technology 2015 TRACK 3 Advanced Materials for Extreme Conditions: The growing demands for developing new materials that perform effectively under extreme conditions, such as aggressive chemical and radioactive environments, high temperature and stress, can be considered the driving force behind nowadays materials revolution. Developed materials for harsh conditions have to meet, also, the social demands such as safety , energy-efficiency, reliability and at the same time, with affordable cost. This session will highlight materials developments relevant to this field. TRACK 4 Advanced Materials Processing Technologies: Despite the diversity in nowadays materials, they are fundamentally having similar principles in areas such as thermodynamic stability, mass transport, phase transformation and materials structure from the atomic to microscopic level. Materials processing plays a central and critical role in defining the resulted microstructure and, consequently, the final mechanical, physical and chemical properties of the processed materials. Therefore, accurate prediction of the inprocess microstructural evolution is essential to control the resulted microstructure, to understand the relationships between processing conditions and the final microstructure and to adjust processing conditions to produce a material with the desired properties. The clear dependence of a certain material property on specific processing conditions is not only limited to the conventional materials but for the new and future materials as well. This session will address the stateof-the-art research activities in materials processing, microstructural control and performance integrity. The 3rd Saudi International Conference on Advanced Materials Technology 2015 3 Technical Committee 1. Dr. Khaled A. AlOgab - Conference Chair, KACST- KSA 2. Dr. Zuhair M. Gasem - KFUPM 3. Dr. Meslet Al Hajri - K.A.CARE 4. Engr. Ahmed A. Umair - ARAMCO 5. Dr. Abdulhakim A. Almajid - KSU 6. Dr. Hani A. Alarifi - KACST 7. Dr. Talal A. Aljohani - KACST 8. Dr. Marwan Al-Mojil - SABIC 9. Eng. Yasir A. Alfawzan - KACST 10. Eng. Abdullah S. Aleissa - KACST 4 The 3rd Saudi International Conference on Advanced Materials Technology 2015 The 3rd Saudi International Conference on Advanced Materials Technology 2015 5 DAY 1 Program 6 The 3rd Saudi International Conference on Advanced Materials Technology 2015 AMT CONFERENCE 2015 DAY1 MAY 18 MONDAY REGISTRATION 08:00 – 09:00 OPENING SESSION 09:00 – 09:30 Holy Quran Dr. Khaled A. AlOgab - Conference Chair, KACST - Saudi Arabia H.H. Dr. Turki bin Saud bin Mohammad Al-Saud - President, KACST - Saudi Arabia Keynote Speaker 1 09:30 – 10:15 Innovations in the Global Steel Industry and Contributions of Industry/University Partnerships Prof. David K. Matlock - University Emeritus Professor and the Armco Foundation Fogarty Professor in the George S. Ansell Department of Metallurgical and Materials Engineering at the Colorado School of Mines (CSM) 09:30 – 10:15 Coffee Break 10:15 – 10:30 SESSION 1.11.2 - LIGHTWEIGHT MATERIALS SESSION 10:30 – 12:00 Session Chair: Dr. Khaled A. AlOgab - Manager, National Center for Advanced Materials Technology, KACST - KSA 1.1.1 Recent Developments in the Processing of Metals with Submicrometer Grain Sizes Prof. Terence G. Langdon - Professor of Materials Science, University of Southampton, UK and Professor of Engineering Emeritus, University of Southern California - USA 10:30 – 11:00 1.1.2 Severe Plastic Deformation: An Effective Approach for Grain Refinement , Improved Strength and Enhamced Ductility Prof. Ehab El-Danaf - Professor of Materials Science and Engineering in Mechanical Engineering Department, King Saud University (KSU) - Saudi Arabia 1.1.3 Light Weight Improved Metal-Composites Reinforced with Nanoparticulate Materials Dr. Marc Leparoux - Swiss Federal Laboratories for Materials Sciences and Technology (EMPA) 11:00 – 11:30 Prayer & Lunch 12:00 – 13:30 SESSION 1.21.3 - ADVANCED MATERIALS FOR WATER AND ENERGY APPLICATIONS SESSION 11:30 – 12:00 13:30 – 14:30 Session Chair: Dr. Talal A. Aljohani - Research Assistant Professor, National Centre for Advanced Materials Technology, KACST - KSA 1.2.1 Nanomaterial Design Strategies for Capacitive Energy Storage Prof. Husam Al-Shareef - Professor of Materials Science and Engineering, King Abdullah University of Science & Technology (KAUST) - Saudi Arabia 13:30 – 14:00 1.2.2 Inorganic Membranes for Water Filtration and Desalination: Opportunities and Challenges Prof. Tahar Laoui - Professor of Materials & Manufacturing Engineering in Mechanical Engineering Dept., King Fahd University of Petroleum and Minerals (KFUPM) - Saudi Arabia 14:00 – 14:30 The 3rd Saudi International Conference on Advanced Materials Technology 2015 7 Opening Ceremony Opening Ceremony H.H. Dr. Turki bin Saud bin Mohammad Al-Saud President King Abdulaziz City for Science and Technology (KACST) - KSA Dr. Khaled A. AlOgab Conference Chair KACST – KSA Session Chairman 1.1 Dr. Khaled A. AlOgab Manager National Center for Advanced Materials Technology, King Abdulaziz City for Science and Technology (KACST) - KSA Keynote Lecture 1 Prof. David K. Matlock University Emeritus Professor and the Armco Foundation Fogarty Professor George S. Ansell Department of Metallurgical and Materials Engineering at the Colorado School of Mines (CSM) Session 1.1.1 Session 1.1.2 Session 1.1.3 Prof. Terence G. Langdon Professor of Materials Science University of Southampton, UK and Professor of Engineering Emeritus, University of Southern California - USA Prof. Ehab El-Danaf Professor Materials Science and Engineering in Mechanical Engineering Department, King Saud University (KSU) - Saudi Arabia Dr. Marc Leparoux Group Leader Nanopowder & Composites Swiss Federal Laboratories for Materials Sciences and Technology (EMPA) Session Chairman 1.2 Session 1.2.1 Session 1.2.2 Dr. Talal A. Aljohani Research Assistant Professor Electrochemistry and Materials Corrosion, National Centre for Advanced Materials Technology KACST - KSA Prof. Husam Al-Shareef Professor of Materials Science and Engineering King Abdullah University of Science & Technology (KAUST) - Saudi Arabia Prof. Tahar Laoui Professor Materials & Manufacturing Engineering in Mechanical Engineering Dept., King Fahd University of Petroleum and Minerals (KFUPM) - Saudi Arabia 8 The 3rd Saudi International Conference on Advanced Materials Technology 2015 DAY 1 MAY 18, 2015 - MONDAY Opening Session H.H. Dr. Turki bin Saud bin Mohammad Al-Saud President King Abdulaziz City for Science and Technology (KACST) - KSA BIOGRAPHY • President of King Abdulaziz City for Science and Technology (KACST) • He received his PHD in Aeronautics and Astronautics from Stanford University. • Joined King Abdulaziz City for Science and Technology (KACST) in 1997 as Director of the newly established Space Research Institute. • He became the Vice President of KACST for Research Institutes in 2004. Al-Saud serves as: • Chairman of the Scientific Council of KACST. • Chairman of the Supervisory Committee for the National Science and Technology and Innovations Plan (NSTIP). • Chairman of the Supervisory Committee for King Abdullah Initiative for Solar Water Desalination. • Chairman of the boards of several joint centers of excellence in collaboration with world’s leading universities and companies. • Chairman of the Supervisory Committee for Technology Incubators. • A member of the Regency Council of Al Faisal University, Riyadh. • A member of the Advisory Council for the School of Engineering at Stanford University. • Chairman of the Board of Directors of the Technology Development and Investment Company (TAQNIA). The 3rd Saudi International Conference on Advanced Materials Technology 2015 9 The 3rd Saudi International Conference on Advanced Materials Technology 2015 Opening Session & Session Chairman 1.1 Dr. Khaled A. AlOgab Conference Chair Manager - National Center for Advanced Materials Technology, King Abdulaziz City for Science and Technology (KACST) - KSA BIOGRAPHY Dr. AlOgab received his Bachelors (1996) in Mechanical Engineering Technology from Riyadh College of Technology. After which he joined Burydah College of Technology (BCT), Burydah, KSA, and awarded a scholarship to pursue his graduate studies. In Dec. 2000, he received his MSc in Materials Science and Engineering from Western Michigan University. In 2004, he received his PhD in Metallurgical and Materials Engineering from Colorado School of Mines. In 2005, Dr. AlOgab rejoined BCT and worked as an assistant professor. From Nov 2007 until Sept 2009, he was the Head of the Mechanical Technology Department at BCT. In Oct 2009, Dr. AlOgab joined King Abdulaziz City for Science and Technology (KACST). At KACST he served as the Deputy Director for the National Program for Aeronautical Technology, Director for the National Center for Non-De structive Testing, and, currently, he is the Manager of the National Center for Advanced Materials Technology. Dr. AlOgab has published a number of conference and journal papers. His research interests involve ferrous and nonferrous physical metallurgy and processing technology, in general, and to link the fundamentals of physical metallurgy with industrial applications. In 2009, Dr. AlOgab received the Charles Hatchett Award, presented in the Institute of Materials, Minerals and Mining (IOM3), London, UK, which is given for the best published research on the science and technology of niobium and its alloys. 10 The 3rd Saudi International Conference on Advanced Materials Technology 2015 DAY 1 MAY 18, 2015 - MONDAY Keynote Lecture 1 Prof. David K. Matlock Professor University Emeritus and the Armco Foundation Fogarty Professor in the George S. Ansell Department of Metallurgical and Materials Engineering at the Colorado School of Mines (CSM Title Presentation: Innovations in the Global Steel Industry and Contributions of Industry/ University Partnerships BIOGRAPHY Prof. Matlock received his B.S. degree in engineering science from the University of Texas at Austin (1968), and his M.S. (1970) and Ph.D. (1972) degrees in materials science and engineering from Stanford University. He is a University Emeritus Professor and the Armco Foundation Fogarty Professor in the George S. Ansell Department of Metallurgical and Materials Engineering at the Colorado School of Mines (CSM), Golden, Colorado. He joined the CSM faculty in 1972 and is involved in teaching and research, primarily related to the mechanical properties of materials. He is one of the co founders of the Advanced Steel Processing and Products Research Center, an industry-university cooperative research center established at CSM in 1984. The Center currently has 29 corporate sponsors and is recognized as one of the most successful industry/ university research centers in the world. He served as Center Director from 1993 until his retirement in May 2013. In retirement he continues to be an active participant in all Center operations. Prof. Matlock is a member of the US National Academy of Engineering, a Fellow of the American Society for Metals (ASM), a Fellow of TMS (the Minerals, Metals and Materials Society), and a Fellow of the American Welding Society (AWS). In his 43 year career at CSM his teaching and research efforts have led to multiple awards from CSM and professional societies including the American Iron and Steel Institute, Metallurgical Society of AIME, Iron and Steel Society, Association for Iron and Steel Technology, ASM International, American Welding Society, the Society of Automotive Engineers, the American Nuclear Society, and the Institute of Materials, Minerals and Mining. He has authored or co-authored over 400 technical publications, mostly related to steels. ABSTRACT: Currently new and enhanced steels are required to meet a broad range of societal needs including, as examples, more efficient transportation systems, improved and expanded energy production systems, and infrastructure development and redevelopment projects. As a result, multiple innovations in the steel industry have been realized to support the needs for economic solutions for these critical applications. This presentation will include an assessment of research innovations in the global steel industry as well as specific selected research examples chosen to illustrate the broad range of developments that have evolved recently leading to new products. While corporate research programs are important, emphasis here will be placed on industry/ university partnerships and their importance to the steel industry. Information is drawn from the research of the Advanced Steel Processing and Products Research Center, an industry/university cooperative research center currently in its 31st year of operation at the Colorado School of Mines. Specific research examples will include sheet, plate and bar steels. For example, newly developed advanced high strength sheet steels (AHSS) with excellent formability that have evolved particularly for automotive applications will be highlighted. These new high-strength steels enable vehicle weight reduction to improve fuel economy and lead to enhanced crash performance and passenger safety. As a second example, research on high-strength pipeline steels will be used to illustrate how the application of advanced analytical techniques (e.g. electron back scattered diffraction – EBSD) has provided enhanced understanding of the fundamental factors which control strength and toughness in plate steels used to fabricate high strength pipe. In addition, an assessment of future research opportunities for the steel industry will be presented. The 3rd Saudi International Conference on Advanced Materials Technology 2015 11 The 3rd Saudi International Conference on Advanced Materials Technology 2015 Session 1.1.1 Prof. Terence G. Langdon Professor Materials Science, University of Southampton, UK and Professor of Engineering Emeritus, University of Southern California - USA Title Presentation: Recent Developments in The Processing of Metals with Submicrometer Grain Sizes BIOGRAPHY Education: B.Sc., Physics, University of Bristol; Ph.D., Metallurgy, Imperial College, University of London Membership of Academies: Academy of Sciences of Bashkortostan Republic, Russia (1994); Royal Academy of Engineering, UK (2002); European Academy of Sciences (2008), Academia Europaea (2014). Academic Awards: D.Sc. in Physics, University of Bristol (1980); Henry Marion Howe Medal, ASM International (2000); Doctor honoris causa, Russian Academy of Sciences (2003); Sōmiya Award, International Union of Materials Research Societies (2005); Albert Sauveur Achievement Award, ASM International (2007); Blaise Pascal Medal, European Academy of Sciences (2008);, Lee Hsun Award, Chinese Academy of Sciences (2009); Honorary Medal “De Scientia et Humanitate Optime Meritis,” Academy of Sciences of the Czech Republic (2009); Acta Materialia Gold Medal (2012). ABSTRACT: The processing of metals with exceptionally small grain sizes has become important over the last two decades because these ultrafine-grained metals exhibit high strength and superplastic forming capabilities. This presentation describes recent developments in this important area of research. 12 The 3rd Saudi International Conference on Advanced Materials Technology 2015 DAY 1 MAY 18, 2015 - MONDAY Session 1.1.2 Prof. Ehab El-Danaf Professor Materials Science and Engineering in Mechanical Engineering Department, King Saud University (KSU) - Saudi Arabia Title Presentation: Severe Plastic Deformation: An Effective Approach for Grain Refinement, Improved Strength and Enhamced Ductility BIOGRAPHY I graduated with a Bachelor degree from Mechanical Design and Production Department from the College of Engineering, Cairo University with Distinction with honor in 1991. I finished My Master of Science degree in Computer Aided Design and Optimization of Gears in 1994 from the same Department. I then joined Drexel University in Philadelphia PA, USA in 1994 in the Department of Materials Science where I was awarded my Ph.D degree in 1998. I have received the following awards: • First rank award for Research Excellence from College of Engineering, King Saud University, 2012. • Highly Cited Author Award, 2003, THOMSON ISI. • Best Academic achievement “Harry Roger award”,1998, Drexel University. • Best Academic Achievement, 1993, from the Engineering Syndicate in Cairo, Egypt. ABSTRACT: Two basic and complementary approaches have been developed for the synthesis of ultrafine grained (UFG) materials and these are known as the ‘‘bottom-up’’ and the ‘‘top-down’’ approaches. In the ‘‘bottom-up’’ approach, UFG materials are fabricated by assembling individual atoms or by consolidating nano-particulate solids. The ‘‘top-down’’ approach is different because it is dependent upon taking a bulk solid with a relatively coarse grain size and processing the solid to produce a UFG microstructure through heavy straining or shock loading. In order to convert a coarse-grained solid into a material with ultrafine grains, it is necessary both to impose an exceptionally high strain in order to introduce a high density of dislocations and for these dislocations to subsequently rearrange to form an array of grain boundaries. The potential of improving mechanical properties by reducing the grain size to the nanostructured regime has been aggressively addressed, and is the focus of this presentation. The work, currently presented, addresses cryomilling and subsequent consolidation of aluminum alloys powders ( 99.7 Al, 6061 and 2024 AA) as one technique that represents the bottom-up approach. Of the top-down approach techniques investigated are the equal channel angular pressing (ECAP), high pressure torsion (HPT), friction stir processing (FSP), cryogenic shock loading, accumulative roll bonding (ARB) and rotary swaging (RS). The previous processing techniques were employed on a group of aluminum alloys (6082, 5083, 1050 AA) and a group of titanium alloys (CP Ti, Ti54M AND 10-2-3 Ti alloy). All of these procedures are capable of introducing large plastic straining and significant microstructural refinement in bulk crystalline solids. The results focus on documenting the evolution of mechanical properties, microstructure and texture. The 3rd Saudi International Conference on Advanced Materials Technology 2015 13 The 3rd Saudi International Conference on Advanced Materials Technology 2015 Session 1.1.3 Dr. Marc Leparoux Group Leader Nanopowder & Composites Swiss Federal Laboratories for Materials Sciences and Technology (EMPA) Title Presentation: Light Weight Improved Metal-Composites Reinforced with Nanoparticulate Materials BIOGRAPHY Marc Leparoux studied Physics and Chemistry of Materials in Rennes (France). He obtained his PhD in Applied Sciences in 1995 in Orléans (France) on the chemical vapor synthesis of Boron Nitride based interphases for SiC/SiC ceramic composites. The PhD work was performed at CNRS together with an industrial partner, the Snecma Group. He then joined the Fraunhofer Institute for Materials and Laser Technologies in Dresden (Germany) where he was in charge of the laser assisted chemical vapor deposition for coating fibers to be used in composite materials. In parallel, he developed infrared spectroscopy techniques for monitoring gas phase processes. He joined Empa in Switzerland in 2001 where he initiated the nanoparticle thermal plasma synthesis activities. He then built a unique inductively coupled thermal plasma reactor allowing the in-situ characterization of the nanoparticle synthesis. The facility has been used for producing a large variety of different materials like carbides (SiC, TiC, WC, TaC, ZrC), carbonitrides (TiCN), oxides (Al2O3) and also some metallic materials like Cu, Si, NiTi. Beside the synthesis of nanoparticles, the reactor can also be used for spheroidizing microscale particles or functionalizing powders. With these activities, Marc Leparoux is involved in a lot of large projects in Europe on batteries and composites. In 2006, he started in parallel his activities on metal matrix composite reinforced with the nanoparticles he produced. He reported among the best mechanical strengths for aluminum alloys reinforced with nanoparticulate materials. In this framework, a project together with KACST has been launched. He is leading officially the Group Nanoparticles and Nanocomposites since more than 7 years. ABSTRACT: A simple powder metallurgy approach is reported for producing metal matrix composites reinforced with nanoparticles showing outstanding mechanical strength and hardness. The metal and nano-reinforcement powders are mixed in a high energy ball mill and the resulting blends are hot compacted using a uniaxial press. High energy ball milling was indeed successful in dispersing different nanoparticulate materials into an AlMg5 alloy matrix. Carbon nanotubes (CNT) as well as Al2O3 or SiC nanoparticulate materials could be thus dispersed up to above 10 vol%. Hardness improvements by a factor of 4 - from 70 to 275 HV20 - could be achieved for the as pressed composites with 5 vol% CNT. The ultimate tensile strength (UTS) increased from 290 MPa for raw AlMg5 to 700 and 720 MPa with 1 vol% alumina nanofibers and 0.5 vol% CNT respectively. However these high strength composites dramatically suffered from low ductility. Typically 1 % of elongation at rupture could be measured in the best cases. The milling conditions like the process control agent, the milling time and the mill geometry have then been carefully investigated and their optimization allowed reaching a reasonable compromise between high strength and high ductility. For instance the composite AlMg5-0.5 vol% nanoAl2O3 (mean diameter 20 nm) shows the following mechanical properties: 500 MPa ultimate strength, 475 MPa yield strength and an elongation at rupture around 10%. A linear regression could be drawn between the strength and the strain of the composites reinforced with less than 1 vol% of alumina nanoparticles. These mechanical properties are comparable or even better than those reported for commercial available alloys for which a costly special heat or work hardening treatment is required. 14 The 3rd Saudi International Conference on Advanced Materials Technology 2015 DAY 1 MAY 18, 2015 - MONDAY Session Chairman 1.2 Dr. Talal A. Aljohani Research Assistant Professor Electrochemistry and Materials Corrosion, National Centre for Advanced Materials Technology, KACST - KSA BIOGRAPHY Dr. Talal A. Aljohani is currently a Research Assistant Professor of Electrochemistry and Materials Corrosion at the national centre for advanced materials technology, Kind Abdulaziz City for Science and Technology (KACST). In addition, he is the Co-director of the Excellence Centre for Advanced Materials and Manufacturing (CAMM), which is a collaborative research centre between the University of Cambridge and Kind Abdulaziz City for Science and Technology (KACST). He received his PhD in Electrochemistry from the University of Southampton, where he worked with Professor Brian E. Hayden to establish a protocol of High-Throughput Measurements of Corrosion Resistance of Metal Alloys synthesized based MBE methodology. His research interest focuses on high throughput electrochemical measurements, combinatorial synthesis techniques. In addition, he is interested in other electrochemistry fields including water electrolysis and photo-electrolysis, electro-catalysis, fuel cells, and corrosion. Dr. Aljohani has published several scientific articles at peer-reviewed international journals. The 3rd Saudi International Conference on Advanced Materials Technology 2015 15 The 3rd Saudi International Conference on Advanced Materials Technology 2015 Session 1.2.1 Prof. Husam Al-Shareef Professor of Materials Science and Engineering King Abdullah University of Science & Technology (KAUST) - Saudi Arabia NOT AVAILABLE Title Presentation: Nanomaterial Design Strategies for Capacitive Energy Storage BIOGRAPHY Prof. Husam Alshareef obtained his Ph.D. degree in materials science and engineering at North Carolina State University. He then spent 2 years as postdoctoral scientist at Sandia National Laboratories in Albuquerque, United States. He then embarked on a 10-year career in the semiconductor industry, holding positions at Micron Technology and Texas Instruments, Inc. There he worked on developing new materials and processes for integrated circuit fabrication. In 2009 he joined KAUST, where he initiated an active research group focusing on emerging electronics and on energy harvesting and storage. The author of more than 250 articles, he has nearly 80 patents. He has won the UNDP Undergraduate Fellowship, Seth Sprague Physics Award, North Carolina State Dean’s Fellowship, U.S. Department of Education Electronic Materials Fellowship, and the SEMATECH Corporate Excellence Award. He was associate editor for the Journal of Electronic Materials (2011-2013) and is the editorin-chief for Materials for Renewable & Sustainable Energy. He served as co-chair for the 2014 Materials Research Society (MRS) Fall Meeting, and is a senior member of IEEE. His students at KAUST have won the Dow Sustainability Award (twice), three academic excellence awards, Intel ISEF Award, and SABIC’s Plastic Electronics Innovation Award. His research has been featured in several media outlets. ABSTRACT: The talk will focus on strategies that we have been developing to improve electrode material performance in capacitive energy storage devices, including conventional pseudocapacitors, hybrid supercapacitors, and microfabricated supercapacitors. The talk will cover the development of organic and inorganic electrodes that offer both macroporosity and mesoporosity using in-situ nucleation on current collectors. The resultant morphologies of such electrodes facilitate electrolyte permeation, reduce device resistance, and provide large surface areas for faster reaction kinetics at the electrode surface, thereby increasing device capacitance. Development of negative electrode materials for the fabrication of hybrid and asymmetric capacitive devices, which work at higher voltage, will also be covered. Finally, recent development in flexible and microfabricated supercapacitors for self-powered device applications will be discussed. 16 The 3rd Saudi International Conference on Advanced Materials Technology 2015 DAY 1 MAY 18, 2015 - MONDAY Session 1.2.2 Prof. Tahar Laoui Professor Materials & Manufacturing Engineering in Mechanical Engineering Dept., King Fahd University of Petroleum and Minerals (KFUPM) - Saudi Arabia Title Presentation: Inorganic Membranes for Water Filtration and Desalination: Opportunities and Challenges BIOGRAPHY Dr Tahar Laoui is Professor of Materials & Manufacturing Engineering in Mechanical Engineering Dept. at King Fahd University of Petroleum and Minerals (KFUPM), Dhahran, Saudi Arabia. He received his PhD from the University of Washington, Seattle, USA in 1990. Keywords describing his research interests include processing of advanced materials and nanomaterials with a focus on nanocomposites and how to enhance uniform dispersion of nanoparticles within the matrix as well as to minimize grain growth for powder mixtures subjected to sintering during consolidation by using non-conventional techniques such as spark plasma sintering. For the past few years, he conducted research in joint collaboration with colleagues from Mechanical Engineering Dept. at MIT, USA, and Chemical Engineering Dept. at KFUPM on the development of inorganic and composite membranes for water treatment and water desalination by exploring techniques to synthesize and characterize the transport of water and ions through macro- and nano-structured materials such as zeolites, alumina-based ceramics, activated carbon and graphene. He is a Fellow of The Institute of Materials, Minerals and Mining, member of editorial board of Membranes journal, and served as a reviewer/member of the review committee for many journals and national/ international conferences. He has published over 120 refereed journal & conference papers. ABSTRACT: Clean water has become an important commodity to due to growing world population, increasing industrial plants, and depletion of some conventional fresh water resources such as lakes, rivers and groundwater. Therefore, water filtration/purification or water reuse and desalination have emerged as keys solutions to alleviate the water shortage problem. Among the various technologies used to produce drinkable water, membrane based technologies are increasingly adopted, in which membranes are made from polymeric materials (commercially dominant due to its maturity), ceramics and composites. However, polymeric membranes suffer from low flux, excessive fouling, and low resistance to chlorine, while inorganic/ceramic membranes offer potentially high permeate flux, high salt rejection and enhanced fouling resistance. They are particularly suitable for processes with high temperatures and harsh chemical environments due to their high thermal, chemical and mechanical stability. On the other hand, the performance of ceramic membranes is dictated by their morphology including pore size, shape, density, and distribution and surface characteristics, which are crucial to control during their fabrication. In this presentation, the opportunities offered by inorganic membranes for use in water treatment and desalination will be highlighted along with the associated challenges and difficulties. The research activities taking place at King Fahd University of Petroleum & Minerals (KFUPM) in this area, in collaboration with other universities such as Massachusetts Institute of Technology (MIT), will be discussed. It is worth mentioning that some of this research is supported by King Abdulaziz City for Science and Technology (KACST), as part of the National Science, Technology and Innovation Plan, which gratefully acknowledged. The 3rd Saudi International Conference on Advanced Materials Technology 2015 17 DAY 2 Program 18 The 3rd Saudi International Conference on Advanced Materials Technology 2015 AMT CONFERENCE 2015 DAY2 MAY 19 TUESDAY REGISTRATION 08:30 – 09:30 Keynote SESSION Speaker 2.1 2 09:30 – 10:15 Twenty Years of Innovations in Friction Stir Welding: Path Travelled and Future Opportunities Prof. Rajiv Mishra - Professor of Metallurgical Engineering, University of North Texas - USA 09:30 – 10:15 Coffee Break 10:15 – 10:30 SESSION 2.12.2 ADVANCED MATERIALS FOR EXTREME CONDITIONS SESSION 10:30 – 12:00 Session Chair: Dr. Nasser A. Alkhomashi - Director of the Nuclear Science Research Institute KACST - Saudi Arabia 2.1.1Surface Reactivity and Corrosion Mechanisms of Metals at the Nanoscale Prof. Philippe Marcus - Director of Research at CNRS (Centre National de la Recherche Scientifique) and Head of the Research Group of Physical Chemistry of Surfaces, Institut de Recherche de Chimie - Paris 10:30 – 11:00 2.1.2 Property-Performance Relationships in Heterogeneous Materials Prof. Magnus Nyden - Director of The Wark Research Institute, University of South Australia - Australia 11:00 – 11:30 2.1.3 A Novel Nano Rare Earth Material: From Corrosion Protection to Novel Biomedical Antioxidants Prof. Sudipta Seal - Director of Nanoscience Technology Center (tenure granting unit) and Advanced Materials Processing Analysis Center at UCF 11:30 – 12:00 Prayer & Lunch 12:00 – 13:30 SESSION 2.22.3 ADVANCED MATERIALS PROCESSING TECHNOLOGIES SESSION 13:30 – 15:00 Session Chair: Dr. Hamad A. Albrithen - Department of Physics and Astronomy Materials and Surface Physics College of Sciences, KSU - Saudi Arabia 2.2.1 Thermoset Based Lightweight Construction Materials Dr. Christian Dreyer - Deputy Director - Fraunhofer Research Institution for Polymeric Materials and Composites PYCO - Germany 13:30 – 14:00 2.2.2 Development of Nanostructured Composite Coatings by the HVOF Spraying Process Prof. Tahir Khan - Professor of Materials Engineering and holds the Qatar Petroleum Chair in Materials in the Department of Mechanical & Industrial Engineering, Qatar University - Qatar 14:00 – 14:30 2.2.3 Focused Beam Induced Materials Processing Prof. Patrik Hoffmann - Head of the Laboratory of Advanced Materials Processing at Empa, Swiss Federal Laboratories for Materials Sciences and Technology 14:30 – 15:00 The 3rd Saudi International Conference on Advanced Materials Technology 2015 19 Keynote Speaker 2 Prof. Rajiv Mishra Professor Metallurgical Engineering, University of North Texas - USA Session Chairman 2.1 Dr. Nasser A. Alkhomashi Director Nuclear Science Research Institute KACST - Saudi Arabia Session Chairman 2.2 Dr. Hamad A. Albrithen Department of Physics and Astronomy Materials and Surface Physics College of Sciences, KSU – Saudi Arabia Session 2.1.1 Session 2.1.2 Session 2.1.3 Prof. Philippe Marcus Director of Research CNRS (Centre National de la Recherche Scientifique) and Head of the Research Group of Physical Chemistry of Surfaces Institut de Recherche de Chimie - Paris Prof. Magnus Nyden Director The Wark Research Institute, University of South Australia Australia Prof. Sudipta Seal Director Nanoscience Technology Center (tenure granting unit) and Advanced Materials Processing Analysis Center at UCF Session 2.2.1 Session 2.2.2 Session 2.2.3 Dr. Christian Dreyer Deputy Director Fraunhofer Research Institution for Polymeric Materials and Composites PYCO - Germany 20 The 3rd Saudi International Conference on Advanced Materials Technology 2015 Prof. Tahir Khan Professor Materials Engineering and holds the Qatar Petroleum Chair in Materials in the Department of Mechanical & Industrial Engineering, Qatar University - Qatar Prof. Patrik Hoffmann Head of the Laboratory of Advanced Materials Processing at Empa Swiss Federal Laboratories for Materials Sciences and Technology DAY 2 MAY 19, 2015 - TUESDAY Session Chairman 2.1 Dr. Nasser A. Alkhomashi Director Nuclear Science Research Institute KACST - Saudi Arabia BIOGRAPHY Dr. Nasser Alkhomashi is graduated from the University of Surrey, UK. He holds an MSc degree in Radiation and Enviromental Protection while his PhD was in production of new radioisotopes using accelerators. He invloved in several research activcities related to the expermital nuclear physics in many leading nuclear facilities such as GSI in Germany, CERN in Switizland and IFIN-HH Institute in Romania. His research interests involve high research nuclear physics experiments, detector and accelerator developments. Currently, Dr. Nasser is the Director of the Nuclear Science Research Institute (NSRI), King Abdulaziz City for Science and Technology (KACST). The 3rd Saudi International Conference on Advanced Materials Technology 2015 21 The 3rd Saudi International Conference on Advanced Materials Technology 2015 Keynote Lecture 2 Prof. Rajiv Mishra Professor Metallurgical Engineering, University of North Texas - USA Title Presentation: Twenty Years of Innovations in Friction Stir Welding: Path Travelled and Future Opportunities BIOGRAPHY Rajiv S. Mishra: Dr. Mishra (Ph.D. in Metallurgy from University of Sheffield) is a Professor at University of North Texas from Sept. 2011. Before that he served as Curators’ Professor of Metallurgical Engineering in the Department of Materials Science and Engineering at the Missouri S&T. He is also the UNT Site Director of the NSF I/UCRC for Friction Stir Processing and a Fellow of ASM International. He has received a number of awards which include: the Brunton Medal for the best Ph.D. dissertation in the School of Materials from the University of Sheffield in 1988, the Young Metallurgist Award from the Indian Institute of Metals in 1993, Associate of the Indian Academy of Sciences in 1993, the Faculty Excellence Awards from the University of Missouri-Rolla (2001-2007), and co-recipient of Alexander Schwarzkopf Prize for Technological Innovation awarded to the Center for Friction Stir Processing by NSF-IUCRC Directors Association. He has authored or co-authored 266 papers in peer-reviewed journals and proceedings and is principal inventor of four U.S. patents. His current publication based h-index is 41 and his papers have been cited more than 7100 times. He has co-authored a book on friction stir welding and processing, and edited or co-edited twelve TMS conference proceedings. He is a co-author of four short books on (1) Residual Stresses in Friction Stir Welding, (2) Friction Stir Processing for Enhanced Low Temperature Formability, (3) Friction Stir Superplasticity for Unitized Structures, and (4) Friction Stir Welding of Dissimilar Alloys and Materials, published by Butterworth–Heinemann. He serves on the editorial board of Materials Science and Engineering A and Science and Technology of Welding and Joining. ABSTRACT: The invention of friction stir welding involved a strong technological pull and the initial phase involved adoption of this innovative technology for solid state joining of ‘non-weldable’ high strength aluminium alloys. Currently the spectrum of applications is quite wide. This talk will present an overview of the path of progress in the last twenty years. Illustrative examples will be presented to provide linkages between the current status and challenges for the future growth. Particular emphasis will be on high strength aluminium alloys, magnesium alloys, titanium alloys and steels. Emerging potential for dissimilar alloys and dissimilar materials will be highlighted in relationship with the fundamental metallurgical issues and mechanical approaches. Hybrid processes that decouple the heat input from material flow are being pursued to either overcome the limitations or expand the process domain. A very short overview on friction stir processing will be included to capture the potential of derivative processes. 22 The 3rd Saudi International Conference on Advanced Materials Technology 2015 DAY 2 MAY 19, 2015 - TUESDAY Session 2.1.1 Prof. Philippe Marcus Director of Research CNRS (Centre National de la Recherche Scientifique) and Head of the Research Group of Physical Chemistry of Surfaces, Institut de Recherche de Chimie - Paris Title Presentation: Surface Reactivity and Corrosion Mechanisms of Metals at the Nanoscale BIOGRAPHY Prof. Philippe Marcus is Director of Research at CNRS (Centre National de la Recherche Scientifique) and Head of the Research Group of Physical Chemistry of Surfaces of Institut de Recherche de Chimie Paris, Ecole Nationale Supérieure de Chimie de Paris, Chimie ParisTech, France. Dr. Marcus received his Ph. D. (1979) in Physical Sciences from University Pierre and Marie Curie, Paris, France. His field of research is surface chemistry, surface electrochemistry, and corrosion science, with emphasis on the understanding of the structure and properties of metal and alloy surfaces. His research interests include the growth mechanisms and structure of oxide layers on metals and alloys in gaseous and aqueous environments, adsorption of inorganic, organic and biomolecules, the mechanisms of corrosion of metals and alloys at the nanoscale, passivity, passivity breakdown and localized corrosion, initial stages of high temperature oxidation, and the applications of advanced surface analytical methods such as X-ray Photoelectron Spectroscopy, Scanning Tunnelling Microscopy and Spectroscopy, and Time-of-Flight Secondary Ions Mass Spectrometry. Dr. Marcus has published over 400 papers in scientific journals, books and conference proceedings in the areas of corrosion science, surface chemistry and electrochemistry, surface analysis and materials science, plus two books “Corrosion Mechanisms in Theory and Practice” and “Analytical Methods in Corrosion Science and Engineering”. He has given over 100 invited lectures at International Conferences. He serves or served on the editorial board of five major journals in Electrochemistry and Corrosion: Electrochimica Acta, Corrosion Science, Materials and Corrosion, Corrosion Engineering, Science, and Technology, and Corrosion Reviews. Pr. Marcus has received a number of awards and honors, including the 2005 Uhlig Award from the Electrochemical Society, the 2008 Whitney Award from NACE International, the Cavallaro Medal of the European Federation of Corrosion in 2008, the U.R. Evans Award of the UK Institute of Corrosion in 2010, the Lee Hsun Award of the Institute of Metals Research of the Chinese Academy of Sciences in 2012. He was the D.B. Robinson Distinguished Speaker of the University of Alberta, Edmonton, Canada in 2013. He is an elected Fellow of the Electrochemical Society (2005) and of the International Society of Electrochemistry (2009). ABSTRACT: The surface of materials often interacts with the environment, which may be a gas (e.g. air) or a liquid (e.g. water). This interaction can be detrimental to the material and cause its degradation by corrosion. The degradation of materials in corrosive environments leads to macroscopic manifestations, but the mechanisms must be understood at the atom or nanometer scale. In this lecture I will review various aspects related to the role of the surface structure and composition of alloys on corrosion, and the key issue of corrosion protection by surface oxide layers (passive films). The following points will be addressed: - The effect of grain boundaries and grain boundary structure on localized dissolution or passivation - The early stages of interaction of metal surfaces with water - The composition and structure of passive oxide films on metals and the role of alloying elements The data that will be presented have been obtained on different metals and alloys, including stainless steels and aluminium alloys, using advanced surface analytical techniques, X-ray photoelectron spectroscopy (XPS), time of flight secondary ion mass spectrometry (ToF-SIMS), scanning tunneling microscopy (STM), combined with electrochemical methods. The 3rd Saudi International Conference on Advanced Materials Technology 2015 23 The 3rd Saudi International Conference on Advanced Materials Technology 2015 Session 2.1.2 Prof. Magnus Nyden Director The Wark Research Institute, University of South Australia - Australia Title Presentation: Property-Performance Relationships in Heterogeneous Materials BIOGRAPHY Magnus is Swedish with an MSc from Umeå University 1995 and a PhD from Lund University in 1998 in the field of NMR diffusion in heterogeneous polymer solutions and gels. He was an assistant professor under the guidance of Prof. Krister Holmberg at the department of applied surface chemistry, Chalmers University of Technology in Gothenburg, Sweden between 1999-03 and became a professor at the same department in 2006 before moving to Australia in 2012. He is the director of The Wark Research Institute at the University of South Australia, Adelaide, South Australia. The Wark is internationally recognized for colloid & interface science in the areas of energy conversion, minerals processing and nanomedicine. Magnus’ main research interest is soft matter and in particular, heterogeneous materials of industrial importance. His research relies of crossing disciplines, in particular at the interface between chemistry, physics and mathematics. ABSTRACT: The world is constantly in pursuit of new materials and we want as far as possible source natural materials, without the need for energy intensive processing. We have developed a new mathematical framework that enables prediction of material properties even if the materials are highly heterogeneous with distributions in material properties and performance. We show proof-of-principle for polydisperse quantum dots and polymers and point to a applications of importance to the wider field of materials science. 24 The 3rd Saudi International Conference on Advanced Materials Technology 2015 DAY 2 MAY 19, 2015 - TUESDAY Session 2.1.3 Prof. Sudipta Seal Director Nanoscience Technology Center (tenure granting unit) and Advanced Materials Processing Analysis Center at UCF Title Presentation: A Novel Nano Rare Earth Material: From Corrosion Protection to Novel Biomedical Antioxidants BIOGRAPHY Professor Sudipta Seal is Distinguished Professor at the University of Central Florida. In 1997, he has joined the Advanced Materials Processing and Analysis Center (AMPAC) and Mechanical Materials Aerospace Engineering at the UCF. Professor Seal received his BS (BTech-Hons) in (1990) from Indian Institute of Technology (KGP) in Metallurgy and Materials Engineering, and MS in Metallurgy from University of Sheffield (91-92), UK, and Ph.D. from the University of Wisconsin (UWM) in Materials Engineering. After that, he joined Lawrence Berkeley National Laboratory, University of California, Berkeley and was involved in the development of Scanning transmission X-ray microscopy and spectroscopy and Scanning photoemission spectroscopy. Professor Seal is currently the Director of Nanoscience Technology Center (tenure granting unit) and Advanced Materials Processing Analysis Center at UCF and Professor of Materials Science and Engineering and holds a secondary joint appointment at UCF College of Medicine. In 2014, he is elected as an Interim Chair of the Materials Science and Engineering Department. He has also been selected to several distinguished fellowships and awards. He is the recipient of Fellow of American Society of Materials (FASM) and Fellow of the American Association of Advancement of Science (FAAAS), and fellow of other distinguished societies. He has 44 issued patents. ABSTRACT: Nanomaterials, especially rare earth oxide materials (nano to micro size particles), have been shown to effectively protect stainless steels and other alloys from high temperature degradation. However, recently we discovered the unique antioxidant properties of these rare earth oxide nanoparticles, where it protects mammalian cells against damage caused by increased reactive oxygen or nitrogen species, and has been shown to act as effective superoxide dismutase mimetic in vitro. The redox ability of rare earth oxides has been used in a wide range of applications such as three way catalysis, oxygen buffer systems, sensors and corrosion prevention. While these nanostructures have been widely used in many inorganic applications, their role in biology as catalyst is not explored fully. This presentation will provide a brief overview of the applications of these unique nanostructures in treatment of disorders caused by reactive oxygen species (ROS). It was found that the redox kinetics of regenerative oxide nanoparticles can be controlled with the type of medium and their implications in nanobiomedicine is presented. The 3rd Saudi International Conference on Advanced Materials Technology 2015 25 The 3rd Saudi International Conference on Advanced Materials Technology 2015 Session Chairman 2.2 Dr. Hamad A. Albrithen Department of Physics and Astronomy Materials and Surface Physics College of Sciences, KSU – Saudi Arabia BIOGRAPHY Hamad Albrithen received his Bachelor degree from Physics Department/ King Saud University and his PhD, in Surface and Materials Physics, from Ohio University in 2004. He joined Physics and Astronomy Department at King Saud University as an assistant professor in 2005, where he teaches and supervises undergraduate and graduate students. Beside his position at Physics and Astronomy Department he is also affiliated to King Abdullah Institute for Nanotechnology at KSU and the National Nano-center at King Abdulaziz City for Science and Technology. His scoop of research covers: 1) Nitride materials, 2) Oxide Materials, and 3) III-V Materials. He has published more than 20 papers in peer review journals and conferences and participated in several local and international conferences and workshops. Hamad Albrithen is a member of different scientific societies: 1- Saudi Physical Society 2- Materials Research Society 3- American Physical Society 26 The 3rd Saudi International Conference on Advanced Materials Technology 2015 DAY 2 MAY 19, 2015 - TUESDAY Session 2.2.1 Dr. Christian Dreyer Deputy Director Fraunhofer Research Institution for Polymeric Materials and Composites PYCO - Germany Title Presentation: Thermoset Based Lightweight Construction Materials BIOGRAPHY Dr. Christian Dreyer, born 1971 in Idar-Oberstein, Germany, obtained his Diploma degree in Chemistry from the Technical University of Kaiserslautern, Germany, in 1996 with a thesis about Triazine Containing Dendrimers. He obtained a further degree in Analytics and Spectroscopy from the University of Leipzig, Germany in 1999 before receiving his Ph.D. in Polymer Chemistry from the Brandenburg University of Technology of Cottbus, Germany in 2002, honored with the prize for the best Ph.D. thesis. From 1996-2006 he worked as a scientist at the Fraunhofer Institute for Reliability and Microintegration in Teltow. In 2002 he worked as a visiting scientist at the Clemson University, SC, USA. Dr. Dreyer joined in 2006 the automotive supplier LEONI, Nuremberg, Germany as head of the chemical laboratory of the Central Research and Development Department. Since 2011 he is Deputy Director of the Fraunhofer Research Institution for Polymeric Materials and Composites, Teltow. His research interests are development, synthesis, characterization and processing of thermosets for light weight construction and (integrated) optical applications. Dr. Dreyer is also responsible for alternative curing methods of thermosetting resins; including UV-curing, IR-Curing, E-Beam and Microwave-Technology. Christian Dreyer is author or coauthor of 75 papers and has 34 patents. ABSTRACT: Thermoset based lightweight construction materials are used in many industries due to their high (thermo) mechanical performance. However, the cross-linked structure of the thermosets, which is responsible for their good performance, is not always an advantage. Conventional recycling and repair methods are often not applicable for thermosetting polymers. The most frequently used recycling and disposal methods for thermoset composites, which are landfilling, burning or grinding into a raw powder, are not efficient. The state-of-the-art repair methods are mostly based on removing the damaged area by grinding or milling, followed by sticking new layers even if the composite is only de-laminated. In the case of a delamination, it would be more efficient to remove the dam-aged matrix without damaging the endless fibers. For this reason Fraunhofer PYCO developed a simple, efficient and quick recycling and repair method for cyanate- and cyanate-epoxide-based composites. Cyanates are formed via cyclotrimerization reaction from at least difunctional cyanate monomers, showing high glass transition temperatures, thermal sta¬bility and high me-chanical strength as well as a lot of other excellent properties. Furthermore, cyanates can react with a variety of compounds, e.g. epoxides, giving the possibility to produce polymers with tailor-made properties, for example for applica¬tions acquiring fast curing or curing at low temperatures. Regarding to the recycling process, the matrix resin can be decomposed and fibers with good properties could be regained. The recycling of cyanate esters can be done under rela¬tively mild conditions (from room temperature up to 190 °C) using a special class of agents, producing triazinecontaining structures, as well as phenols. The particular recy-cling product composition and the recycling time depend on the specific formu¬lation and on the particular recycling agent. Recycling times below 1 h are feasible. Furthermore, the decomposed matrix can be reused in the preparation of new thermo¬sets, e.g. polyurethanes, epoxides or polyacrylates with glass transition temperatures up to 130 °C. Concerning repair, the matrix could be decomposed in a well-defined area and the un-covered fibers could be impregnated with new resin. By choosing the right agent and reimpregnation resin, the mechanical performance of the repaired composite is compar-able to the performance of a new part. The 3rd Saudi International Conference on Advanced Materials Technology 2015 27 The 3rd Saudi International Conference on Advanced Materials Technology 2015 Session 2.2.2 Prof. Tahir Khan Professor Materials Engineering and holds the Qatar Petroleum Chair in Materials in the Department of Mechanical & Industrial Engineering, Qatar University - Qatar Title Presentation: Development of Nanostructured Composite Coatings by the HVOF Spraying Process BIOGRAPHY Prof. Tahir I. Khan obtained his PhD from the Department of Materials Science & Metallurgy, Cambridge University (U.K) in 1992. He is currently a Professor of Materials Engineering and holds the Qatar Petroleum Chair in Materials in the Department of Mechanical & Industrial Engineering at Qatar University. He also holds a Professorship at the University of Calgary, Canada and is an Adjunct Professor within the Faculty of Materials Science & Engineering, GIK Institute in Pakistan. He is registered as a Chartered Engineer (U.K) and Professional Engineer in Canada. In recognition to his research work he was elected Fellow of the Institute of Materials, Minerals and Mining (U.K) in 2004 and was awarded the Higher Doctorate of Science (Sc.D) by Cambridge University in 2013. ABSTRACT: The ability to deposit microstructured coatings by the High Velocity Oxy-fuel spraying process is well established in the area of thermal barrier coatings for the aerospace industry, however, the application of this technology to the oil and gas industry is relatively new. Research on the use of nanostructured materials indicates that certain properties such as strength, hardness and fracture toughness can be enhanced if a nanostructure was used in place of the microstructured material but the ability to deposit nanostructured coatings is relatively new and posses a challenge. This presentation will review the application of the HVOF coating technique and important parameters used to produce nanostructured coatings. A comparison of the wear resistant behaviour of microstructured and nanostructured coatings based on the WC-Co composition deposited on C-Mn steel substrates will be presented. 28 The 3rd Saudi International Conference on Advanced Materials Technology 2015 DAY 2 MAY 19, 2015 - TUESDAY Session 2.2.3 Prof. Patrik Hoffmann Head of Laboratory of Advanced Materials Processing at Empa Swiss Federal Laboratories for Materials Sciences and Technology Title Presentation: Focused Beam Induced Materials Processing BIOGRAPHY After studying chemistry at the University of Karlsruhe (today KIT), Germany, Professor Patrik Hoffmann started his PhD thesis at EPFL, Swiss Federal Institute of Technology Lausanne (Switzerland) in 1988 under the supervision of Prof. H. van den Bergh and Professor E. sz. Kovàts on continuous wave laser direct writing for repair technologies of microelectronic devices and completed in 1992. After a post doctoral fellowship at IBM Almaden Research Laboratories, San Jose (USA) from 1992-1993, where he worked on gas phase photodissociation processes with Excimer lasers and surface coating technologies he returned to Lausanne as group leader in the Applied Optics Laboratory headed by R. P. Salathé, at EPFL focussing on laser induced localized chemical vapour deposition processes and improving the technologies for production of near field optical probes (SNOM tips). Industrial experience in an electrochemical company was acquired from 1995 -1997 as dental section manager at Gramm Technik (Germany). From 1997 until 2009 he carried out research on Laser Micro-Processing, surface coatings, and Focused Electron Beam Induced Processing (FEBIP). Since 1997 he is teaching on the bachelor, master, and PhD level in micro-engineering and materials sciences at EPFL. In 2009 he became head of the Laboratory of Advanced Materials Processing at Empa, Swiss Federal Laboratories for Materials Sciences and Technology, continuing teaching at EPFL. He is author or co-author of more than 111 peer reviewed journal papers and inventor or co-inventor of half a dozen patents. ABSTRACT: Laser beams as well as charged particle beams (electrons, ions) entered into industrial processing for carrying out specific tasks of local energy input. From very small energy input, i.e. changing solubility of so called resists in microelectronics, through melting materials in welding processes, to high energy input in materials evaporation, or if applied in very short pulses even very rapid ablation of materials. Both, removal and deposition of materials by these local energy sources have been developed. Here we focus on generative processes, i.e. deposition of materials either from solid, liquid, or gaseous precursors for growing structures. Limitations such as processing speed, resolution, and materials quality will be presented and compared. Focused electron beam induced deposition of pure metal nanostructures to laser induced microstructures will be presented and discussed with impact on the generative processes starting from larger materials precursors such as micrometric sized powders. Focused electron beam induced etching and deposition are industrial processes for semiconductor mask repair. The electron beams have replaced Focused Ion Beams due to dramatically lower interaction with the substrate to be repaired, the very precious lithography masks. The latter are key elements for massive parallel mass production of chips in semiconductor industry and since recently also in mobile electronics industry. Laser direct writing by LCVD or by laser deposition from electrolytic metal solutions allow growing structures with relatively small growth rates, due to limited metal precursor supply. Laser welding processes on the other hand are not limited by materials supply, but still speed limited for obtaining high quality welds. These two process limitations will remain the challenges in modern direct laser melting additive manufacturing processes. Taking the case that the materials supply is sufficient, the heat management, i.e. reasonable heating rates to avoid excessive evaporation, key hole formation or conduction melting, and microstructure tailored cooling, have to be optimized in high quality high reliability laser generative processing. Productivity enhancement can only be achieved by selection or synthesis of ideal materials destinated for additive manufacturing. The 3rd Saudi International Conference on Advanced Materials Technology 2015 29 NOTE The 3rd Saudi International ConferenceMAY on 19 DAY2015 2TUESDAY Advanced Materials Technology 30 The 3rd Saudi International Conference on Advanced Materials Technology 2015 NOTE The 3rd Saudi International ConferenceMAY on 19 DAY2015 2TUESDAY Advanced Materials Technology The 3rd Saudi International Conference on Advanced Materials Technology 2015 31 THEORGANIZERS The 3rd Saudi International Conference on Advanced Materials Technology 2015 is organized under the patronage of the Custodian of the Two Holy Mosques, King Salman bin Abdulaziz Al Saud by King Abdulaziz City for Science and Technology (KACST)... National Centre for Advanced Materials Technology, (NCAMT)... The NCAMT at King Abdulaziz City for Science and Technology incubates innovative research in developing new advanced materials. The mission of NCAM is to strengthen the Kingdom’s position in the field of advanced materials technology by its contribution to meet the most prominent social and economic needs, and benefit from the natural wealth of the Kingdom such as oil and minerals. NCAMT carried out research in multi-fields including metals and alloys, ceramics, polymers, composites and hybrids, and materials processing. The strategic goals for the NCAMT are to: • Improve the contribution of advanced materials to the critical national needs and the competitiveness of KSA industries. • Enable a domestic technology-based advanced materials industries in key areas. • Raise KSA’s international position of advanced material. • Improve the Kingdom’s human resources and institutions for advanced materials R&D. King Abdulaziz City for Science & Technology (KACST)... King Abdulaziz City for Science and Technology (KACST) is both the Saudi Arabian national science agency and its national R&D laboratories. KACST plays a key role in science and technology policy making, related data collection, funding of external research, and other related services such as scientific publishing and managing the patent office. Main Responsibilities include: Proposing a national policy for the development of science and technology and relevant strategies; Supporting scientific research and technology development; Conducting applied research advising government; Fostering national innovation and technology transfer between research institutes and the industry; Fostering international cooperation in science and technology. For more information, please visit the conference website: sam15.kacst.edu.sa 32 The 3rd Saudi International Conference on Advanced Materials Technology 2015 National Center for Advanced Materials Technology PO Box 6086 Riyadh, 11442 Kingdom of Saudi Arabia Tel: +966 (11) 481 4441 Fax: +966 (11) 481 3042 sam15.kacst.edu.sa
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