Lackwerke Peters GmbH + Co KG Hooghe Weg 13, D-47906 Kempen Internet: www.peters.de E-Mail: [email protected] Telefon (0 21 52) 20 09-0 Telefax (0 21 52) 20 09-70 Ein Unternehmen der PETERS-Gruppe PTR PRELIMINARY TECHNICAL REPORT Conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ Base: polyurethane resins (PUR) • colourless, fluorescent • humidity curing conformal/permanent coating for assembled pcbs/flat packs com pl i a nt: RoH WEE S ELV E lead - f re e • free of aromatic solvents • free of heavy metals such as lead and chromium compounds, fulfils the requirements of the “lead-free regulation” (EU Vehicle End-Of-Life Directive 2000/53/EG) • excellent protection against corrosion in case of high temperatures and humidities Indices: SL = ECO = FLZ = conformal/permanent coating ecological fluorescent 1 2 3 4 5 6 7 8 9 10 LP 042809 E-2 / 0109100e.002 Contents 1. 2. 3. 4. 5. 6. 6.1 6.2 6.3 7. 7.1 General information............................. 2 Application........................................... 2 Special notes....................................... 2 Safety recommendations .................... 3 Characteristics .................................... 3 Properties ............................................ 3 General properties .............................. 3 Physical and mechanical properties ... 3 Electrical properties............................. 4 Processing........................................... 4 Adjustment of viscosity........................ 4 7.2 7.3 8. 9. 10. 11. Auxiliary products................................ 4 Coating................................................ 5 Drying/Curing ...................................... 5 Standard packaging ............................ 5 Storage................................................ 5 Further literature/ Technical publications ......................................... 6 12. Further products for the production of pcbs..................................................... 6 13. Further products for the electronics/ electrical engineering industries.......... 6 Please read this preliminary technical report, the material safety data sheet according to EEC 91/155 as well as the application information sheet AI 1/1 “Processing instructions for the conventional physically drying/oxidative curing conformal/permanent coatings of the series SL 1300 to SL 1309 N” (see also Item 7) carefully before using the product. 11 12 13 14 15 Preliminary Technical Report ELPEGUARD SL 1400 ECO-FLZ 1. General information The conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ, colourless, fluorescent is a humidity curing 1-pack conformal/permanent coating based on chemically reactive polyurethane resins (PUR). 2. Application The conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ is used as a protective and insulating lacquer; it • protects assembled pcbs even under increased climatic stress against moisture, especially against the effects of condensate, • insulates electrical equipment, connections, switch panels, terminal boards, etc. • can be soldered-through for repair purposes at soldering iron temperature and subsequently reapplied. The conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ is used to protect assembled pcbs that have to fulfil high requirements regarding quality and service life. Its resistance corresponds to that of a 2-pack conformal/permanent coating so that it offers highest climatic protection at high temperatures and high humidities (85 °C/85 % r. h., see also Item 6.2 “Physical and mechanical properties“) and also regarding its electrical properties is suitable for highest requirements and thus also for the coating of assembled pcbs or flat packs for: • • • • • high-performance electronics • • • • • the military sector 3. the automotive industry household appliances (hobby tools, washing machines and others) electronic/electrical measuring and control units electrical appliances equipped with electronic controls (industrial scales, medical appliances, industrial robots, and many more) shipbuilding and off-shore technology aerospace technology explosion-protected equipment appliances for telecommunications. Special notes The conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ is an ecologically modern product (ECO = ecological): It has a high solids content, is free of aromatic solvents and heavy metals and thus fulfils the requirements of the “lead-free regulation” (EU Vehicle End-Of-Life Directive 2000/53/EG). The conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ can be used at temperatures of -40 up to +130 °C [-40 – 266 °F] while at the lower and at the upper ends of this range the behaviour as well as the performance of the material can be negatively affected in case of some applications. Here additional pre-trials and tests are required. To complement the process parameters indicated in this preliminary technical report the Application Information sheet AI 1/1 “Processing instructions for the conventional physically drying/oxidative curing conformal/permanent coatings of the series SL 1300 to SL 1309 N“ gives further and more detailed information and notes that need to be observed to achieve an optimum processing result. In our report manual the Application Information sheet AI 1/1 is filed under Group 1. On our report manual CD as well as on our web-site application information sheets can be accessed in the “Service“ section. 2 www.peters.de Preliminary Technical Report ELPEGUARD SL 1400 ECO-FLZ 4. Safety recommendations ! Please read our material safety data sheet according to EEC 91/155 where you will find detailed specifications of safety precautions, environmental protection, waste disposal, storage, handling, transport as well as other characteristics. ! When using chemicals, the common precautions should be carefully noted. ! Please also pay attention to national guidelines or directives concerning the handling of flammable liquids as for example the German TRbF (technical regulations for flammable liquids) or European directives. 5. Characteristics Colour/appearance colourless, fluorescent Solids content EN ISO 3251 / ISO 3251 1 h, 125 °C [257 °F], 1 g weighed quantity 59 ± 2 % by weight Viscosity at 20 °C [68 °F] flow time acc. to EN ISO 2431 / ISO 2431 5 mm ISO flow cup 75 ± 7 s Viscosity at 20 °C [68 °F] flow time acc. to DIN 53 211* 4 mm DIN flow cup 55 ± 5 s Density at 20 °C [68 °F] EN ISO 2811-1 / ISO 2811-1 1.05 ± 0.05 g/cm³ * The DIN 53211 has been replaced by the international norm EN ISO 2431. However, on account of the widespread usage of the 4 mm DIN flow cup we continue indicating the viscosity acc. to DIN 53211. 6. Properties The conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ is distinguished by the following properties: 6.1 General properties • free of aromatic solvents (such as benzene, toluene, xylene and C9 aromates) • free of heavy metals such as chromium, lead, etc. • high solids content • fulfils the requirements of the “lead-free regulation” (EU Vehicle End-Of-Life Directive • • • • • • 2000/53/EG) after application a very good flow results and after curing an even, closely pored film is obtained safe coverage of component leads, for example, so that even in critical areas a high protection against corrosion is ensured on account of its fluorescent adjustment (Index FLZ) the coating can be easily controlled under UV light (black light with a UV-A impulse at 350-375 nm) exhibits the excellent resistances of a 2-pack lacquer system best climatic protection at high temperatures and humidities, therefore suitable for highest requirements high surface hardness of the dried lacquer film while exhibiting a tenacious elasticity; thus the risk of mechanical damage during further processing is considerably reduced can be soldered-through/-out at soldering iron temperature for repair purposes. • 6.2 Physical and mechanical properties Property Cold-Check Test (Thermal shock test) www.peters.de Test method 100 cycles, -40 °C up to +110 °C [-40 – 230 °F], holding time 15 min each, temperature change within 10 s Result passed (no cracks, no peeling) 3 Preliminary Technical Report ELPEGUARD SL 1400 ECO-FLZ 6.3 Electrical properties Property Test method Result Dielectric strength VDE 0303, part 21 IPC-TM-650, 2.5.6.1 Volume resistivity VDE 0303, part 30 DIN IEC 93 5 x 1015 Ohm x cm Surface resistance VDE 0303, part 30 DIN IEC 93 2 x 1014 Ohm Electro corrosion 21 d, 40 °C [104 °F], 95 % r. h., 100 V DC Moisture and insulation resistance IPC-CC-830, 3.7.1 Comparative tracking index (tracking resistance) DIN IEC 60 112, in connection with VDE 0110, part 3 70 kV/mm none 1 x 1010 Ohm class H and T CTI > 600 85/85 test; ramp like storage at high atmospheric humidity and Moisture and insulation resistance high temperature, among others 3 days at 85 °C [185 °F] and 85 % r. h. > 1 x 109 Ohm Condensation resistance based on DIN 50 017 1 x 1010 Ohm Thermal class based on DIN IEC 60 085 7. B = 130 °C [266 °F] Processing ! Read our Application Information sheet AI 1/1 “Processing instructions for the conventional physically drying/oxidative curing conformal/permanent coatings of the series ELPEGUARD SL 1300 to ELPEGUARD SL 1309 N” where you will find detailed information on processing. In our report manual this Application Information sheet is filed under group 1. On our report manual CD as well on our web-site application information sheets can be accessed in the “Service“ section. The conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ can be applied by means of automatic, selective coating units as well as by means of brushing or spraying. On account of the humidity sensitivity of the conformal/permanent coating application by means of dip coating can only be performed under dry inert gas. On account of the humidity sensitivity work tools made of stainless steel and, if necessary, teflon coated hoses are particularly recommended when processing the conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ. The conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ cures under the influence of moisture. Take measures, such as using dry inert gas, to protect the lacquer against moisture during processing. You must clean the threads of opened containers with the cleaning agent R 5804 or the thinner V 1400 ECO and then re-close the containers tightly. Partially filled containers must be filled with dry inert gas. 7.1 Adjustment of viscosity ! Adjust the processing viscosity of the conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ by means of the thinner V 1400 ECO (see also Item 3.1 of the Application Information sheet AI 1/1). 7.2 Auxiliary products ! Clean the coating equipment with the cleaning agent R 5804. Check the resistance of the material, particularly the seals. We recommend the use of seals made of Teflon®- or Viton®. We recommend the use of the cleaning agent R 5817 to clean work place and tools and the use of the cleaning agent R 5804 or the thinner V 1400 ECO to clean the threads of opened containers. 4 www.peters.de Preliminary Technical Report ELPEGUARD SL 1400 ECO-FLZ Do not use the cleaning agents to clean hands. Solvents extract the natural grease from the skin. Special technical reports on these products are available upon request. In our report manual these technical reports are filed under group 5. On our report manual CD technical data sheets can be accessed in the “Products“ section. Removal of the conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ by means of cleaning agents/ strippers for repair purposes after final curing is virtually impossible. Since aggressive cleaning agents/strippers may also dissolve the components of flat packs these products should only be used after suitable pre-trials. 7.3 Coating ! Ensure that the surface to be coated is clean, grease-free and dry. ! When processing please pay special attention to the notes under Item 4 “precleaning“ and Item 5 “coating“ of the Application Information sheet AI 1/1. When applying the lacquer by means of compressed-air spraying the safety precautions of the German Accident Prevention Regulation "Processing of Coating Materials" (VGB 23 in future BGV D 25), especially section IV Operation (§§ 17-22), and of the German Explosion Protection Regulations (BGR 104) or of corresponding national regulations must be observed. When processing the lacquer by means of spraying it is mandatory to take protection measures to avoid a formation of solvent vapour mixtures that might explode. Filter mats impregnated with lacquer and solvent residues in spraying cabins may self-ignite. Use water-irrigated spraying cabins to avoid the risk of the filter mats self-igniting. Moreover, observe the operating and maintenance instructions of the spraying cabin and filter mat manufacturers. 8. Drying/Curing After application the conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ initially dries physically (see also Item 7.1 “physical drying” of the AI 1/1) and then finally cures under reaction with atmospheric moisture. Guidelines for drying a wet film thickness of 75 µm at room temperature: Tack-dry (dust dry): 40 min Dry (tack-free): 90 min Complete takes approx. 48 to 96 hrs and depends, among others, on the component geometry, the applied lacquer layer thickness and the atmospheric humidity. On account of the atmospheric humidity required for curing oven drying of this lacquer system is not recommended. It is mandatory to ensure that enough humidity is available for curing. ! Determine the optimum parameters for oven curing by means of pre-trials. 9. Standard packaging The conformal/permanent coating ELPEGUARD SL 1400 ECO-FLZ is packed for delivery as follows: Can of 25 kg = 1 selling unit. The thinner V 1400 ECO is available in cans of 23.5 kg. Partial lots of the selling unit may be ordered, but will entail surcharges to cover repackaging costs. 10. Storage In a cool, dry place, sealed original containers can be stored for at least 6 months. For warehousing reasons, isolated cases may occur where the shelf life upon shipment is less than the shelf life indicated in this technical report. However, it is ensured that our products have at least two-thirds of their shelf life remaining when they leave our company. In accordance with EN ISO 9001, labels on containers show expiry dates. www.peters.de 5 Preliminary Technical Report ELPEGUARD SL 1400 ECO-FLZ Storage temperatures below +5 °C [41 F°] and/or in excess of +25 °C [77 °F] affect the storage stability. 11. Further literature/ Technical publications In addition to the recommendations given in this technical report, we can provide technical papers and information sheets written and compiled by members of our staff which give highly detailed information on the application and processing of our products. A list of the technical publications available can be found in TI 15/101 E (technical papers) and TI 15/100 E (technical information sheets). In our report manual all technical information sheets (TI’s) are filed under group 15. Alternatively, visit our web-site at http://www.peters.de or click on the "Service" section on our report manual CD. 12. Further products for the production of pcbs We offer a wide range of etch resists (photoimageable, UV curing, conventional curing), plating resists, solder resists (photoimageable, UV curing, conventional curing) as well as peelable solder resists, marking inks (photoimageable, UV curing, conventional curing), carbonconductive inks, via hole fillers (solely thermally curing), plugging pastes, heatsink pastes, special strippers for solder resists and further auxiliary products for screen printing (e. g. cleaning agents, thinners). Special technical reports on these products are available on request. 13. Further products for the electronics/ electrical engineering industries We boast a wide range of conformal/permanent coatings, thick film lacquers, silicone gel, casting compounds, casting resins, electro pastes, insulating lacquers, impregnating varnishes, adhesive lacquers and auxiliary products for electronics. Special technical reports are also available for these products and can be provided on request. Any questions? We would be pleased to offer you advice and assistance in solving your problems. Free samples and technical literature are available upon request. The above information as well as advice given by our Application Technology Department whether in verbal or written form or during product evaluations is provided to the best of our knowledge, but must be regarded as non-binding recommendations, also with respect to possible third-party proprietary rights. The products are exclusively intended for the applications indicated in the corresponding technical data sheets. The advisory service does not exempt you from performing your own assessments, in particular of our material safety data sheets and technical information sheets, and of our products as regards their suitability for the applications intended. The application, use and processing of our products and of the products manufactured by you based on the advice given by our Application Technology Department are beyond our control and thus entirely your responsibility. The sale of our products is effected in accordance with our current terms of sale and delivery. ATTENTION! For new products, according to preliminary technical reports, adequate practical results are not always available which would permit a comprehensive assessment of such a product. It is therefore imperative to exercise particular care in the testing of such products with regard to the application intended! Lackwerke Peters GmbH + Co KG Hooghe Weg 13, 47906 Kempen Internet: www.peters.de E-Mail: [email protected] Phone: 0049-21 52-20 09-0 Fax: 0049-21 52-20 09-70 6 www.peters.de
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