Small Sample Adapter for rheological evaluation where sample volume is limited ™

BROOKFIELD _ ACCESSORIES
Small Sample Adapter
™
for rheological evaluation where sample volume is limited
Standard Sample Chamber with
embedded temperature probe
provides direct temperature
measurement of sample
What’s Included?
1. Water Jacket
2. Locating Channel Assembly
3. Choice of one SC4 Spindle*
6.
4. Choice of one SC4 Sample Chamber*
5. Insulating Cap
6. Extension Link with Coupling Nut
5.
Storage Case (not shown)
*Specify when ordering
Optional Accessories
8.
7. Embedded RTD temperature Probe
in Chamber
8. SC4-13RD Disposable Sample
Chambers (p48)
Disposable
Sample Chamber
Requires special water jacket
9. Temperature Bath
(Requires SSA-DCU
Water Jacket)
(p33-35)
EZ-Lock Spindle Coupling
(p50)
For more info on Small Sample Adapter
Accessory Kits visit our website.
Complete system shows the DV-II+Pro
Viscometer and Small Sample Adapter
with Circulating Water Bath for
temperature control.
The Small Sample Adapter provides a defined
geometry system for accurate viscosity
measurements at precise shear rates.
Consisting of a cylindrical sample chamber
and spindle, the Small Sample Adapter is
designed to measure small sample volumes
of 2 to 16 mL, and easily attaches to all
standard Brookfield Viscometers/Rheometers.
9.
Labomat Essor
37 Bld Anatole France
F - 93287 Saint Denis Cedex
Tel.: +33 1 48 09 66 11
Fax: +33 1 48 09 98 65
E-mail : [email protected]
www.labomat.eu
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38
TEL 800-628-8139 or 508-946-6200
FAX 508-946-6262
www.brookfieldengineering.com
Labomat Essor
Vlamingstraat 4
B - 8560 Wevelgem
Tel.: +32 56 43 28 13
Fax: +32 56 43 28 14
E-mail : [email protected]
www.labomat.eu
Labomat Essor
Labomat Essor
37 Bld Anatole France
Vlamingstraat 4
F - 93287 Saint Denis Cedex
B - 8560 Wevelgem
Solutions
Tel.: +33 1 L.E
48 09
66 11
Tel.: +32 56 43 28 13
lmm
Résidence
lbn Batoua Fax:
Tel.:+32
+212
22 28
41 714
Fax: +33 1 648
09B98
65
565243
14
Place
Prince
Sidi
Mohammed
+212 52 22 42 751
E-mail : [email protected]
E-mail : Fax:
[email protected]
Belvedère
[email protected]
www.labomat.eu
www.labomat.eu
MA - 20300 Casablanca
www.labomat.eu
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3MALL3AMPLE!DAPTER6ISCOSITY2ANGESC0M0AsS
MODEL
Spi Spi
nd nd
Sam le:SSaCm le: SC
4p
4
p
Sam leSCahm -l1e8Ch -18
ple apmleb amb
She SVhoel eVro:*l er:*
uSm
ar R uam
S
ate r Re:a6te. Ce4: -61. C4-1
seLc -1 37Rm(LP 3R(P
Spi Spi (sec -1 7(m
)
nd nd ):
): )
Sam le:SSaCm le: SC1.32N 1.32N
ple 4p-l3e1 4-31
Sam SCahm Ch
p apm am
She leSVhoel lebeVro:*l ber:*
uSm
ar R uam
S
at r Re:a9t Ce4: -91. C4-1
s 30Rm 3R
Spi Spei (sec -1e.0(m
ndl ndl ): eLc -1): (LP) (P)
Sam e:SSaCm e: SC.34N .34N
4p
4
p
Sam leSCahm -l3e4Ch -34
p apm am
She leSVhoel lebeVro:*l ber:*
uSm
ar R uam
S
at r Re:a9t Ce4: -91. C4-1
s 34Rm 3R
Spi Spei (sec -1e.4(m
ndl ndl ): eLc -1): (LP) (P)
Sam e:SSaCm e: SC.28N .28N
4p
4
p
Sam leSCahm -l1e6Ch -16
p apm am
She leSVhoel lebeVro:*l ber:*
uSm
ar R uam
S
at r Re:a4t Ce4: -48. C4-8
R(P
(
s R2m
Spi Spei (sec -1e.2(m
)
ndl ndl ): eLc -1): PL)
Sam e:SSaCm e: SC.29N .29N
ple 4p-l2e5 4-25
Sam SCahm Ch
p apm am
She leSVhoel lebeVro:*l ber:*
uSm
ar R uam
S
at r Re:a1t Ce4: -11 C4-1
Spi Spei : (sec -e16:.1(smecL -163.R1m
(PL) 3R(P)
ndl ndl ):
Sam e:SSaCm e: SC .22N ): .22N
4p
4
p
Sam leSCahm -l2e1Ch -21
p apm am
She leSVhoel lebeVro:*l ber:*
uSm
ar R uam
S
at r Re:a7t Ce4: -71. C4-1
s 31Rm 3R
Spi Spei (sec -1e.1(m
ndl ndl ): eLc -1): (LP) (P)
Sam e:SSaCm e: SC.93N .93N
4p
4
p
Sam leSCahm -l2e7C(Dh -27(D
p apm a) m )
She leSVhoel lebeVro:*l ber:*
uSm
ar R uam
S
at r Re:a1t Ce4: -110 C4-1
3.R4( 3R(
Spi Spei (sec -1e0.(4sm
PL)
P)
ndl ndl ): ecL-1): m
Sam e:SSaCm e: SC.34N .34N
ple 4p-l1e5 4-15
Sam SCahm Ch
p apm am
She leSVhoel lebeVro:*l ber:*
uSm
ar R uam
S
at r Re:a3t Ce4: -37. C4-7
R(P
(
s R8m
Spi Spei (sec -1e.8(m
)
ndl ndl ): eLc -1): PL)
Sam e:SSaCm e: SC.48N .48N
ple 4p-l2e8 4-28
Sam SCahm Ch
p apm am
She leSVhoel lebeVro:*l ber:*
uSm
ar R uam
S
at r Re:a1t Ce4: -111 C4-1
3.R0( 3R(
Spi Spei (sec -1e1.(0sm
PL)
P)
ndl ndl ): ecL-1): m
Sam e:SSaCm e: SC.28N .28N
ple 4p-l2e9 4-29
Sam SCahm Ch
p apm am
She leSVhoel lebeVro:*l ber:*
uSm
ar R uam
S
at r Re:a1t Ce4: -113 C4-1
3.R5( 3R(
Spi Spei (sec -1e3.(5sm
PL)
P)
ndl ndl ): ecL-1): m
Sam e:SSaCm e: SC.25N .25N
ple 4p-l1e4 4-14
Sam SCahm Ch
p apm am
She leSVhoel lebeVro:*l ber:*
uSm
ar R uam
S
ate r Re:a2te. Ce4: -26. C4-6
R1(P R(P
(se - 1(m
L)
)
c 1) seLc -1) m
: .4 : .4
0N 0N
3MALL3AMPLE!DAPTER6ISCOSITY2ANGESC0M0AsS
LVDV-IIIU 1.2-30K
MODEL
LVDV-II+P
LVDV-IIIU
LVDV-IP
LVDV-II+P
LVDVE
LVDV-IP
LVT
LVDVE
RVDV-IIIU
LVT
RVDV-II+P
RVDV-IIIU
RVDV-IP
RVDV-II+P
RVDVE
RVDV-IP
RVT
RVDVE
HADV-IIIU
RVT
HADV-II+P
HADV-IIIU
HADV-IP
HADV-II+P
HADVE
HADV-IP
HAT
HADVE
HBDV-IIIU
HAT
HBDV-II+P
HBDV-IIIU
HBDV-IP
HBDV-II+P
HBDVE
HBDV-IP
HBT
HBDVE
12-300K 24-600K 48-1.2M
15-300K
48-1.2M
24-600K 60-1.2M
12-300K 30-600K
30-100K
60-1.2M
30-600K 120-400K
15-300K 60-200K
30-100K
120-400K
60-200K 120-400K
30-100K 60-200K
50-100K
120-400K
60-200K 200-400K
30-100K 100-200K
50-100K 100-200K 200-400K
192-4.8M
240-4.8M
192-4.8M
800-1.6M
240-4.8M
800-1.6M
800-1.6M
800-1.6M
800-1.6M
Not applicable for historical reasons. However, it is possible
use the above
spindles with
any ofHowever,
these instruments.
Notto applicable
for historical
reasons.
it is possible
Digital
Viscometers/Rheometers
will
automatically
calculate
to use the above spindles with any of these instruments.
viscosity.
Please
contact
Brookfield
or
an
authorized
dealer
Digital Viscometers/Rheometers will automatically calculate
if
you
require
information
on
viscosity
range.
viscosity. Please contact Brookfield or an authorized dealer
200-5M
500-12.5M
200-5M
800-1.6M 20-500K 100-2.5M
5-10K
if you require
information on viscosity 400-10M
range.
250-5M
500-10M
250-5M
125-2.5M
25-500K
200-5M 400-10M 625-12.5M
500-12.5M
20-500K 100-2.5M 200-5M
500-1.7M
1K-3.3M 1.25K-4.2M
500-1.7M
250-830K
50-170K
250-5M 500-10M
625-12.5M
25-500K 125-2.5M 250-5M
500-1.7M
Not applicable for historical reasons.
50-170K
1K-3.3M 1.25K-4.2M
1.25K-4.2M
500-1.7M 500-1.7M 1K-3.3M
250-830K 500-1.7M
50-170K 250-830K
500-1M
However,
it is possible
to use the
above
1K-2M 1.25K-2.5M
500-1M 500-1.7M
50-100K
Not applicable
for historical
reasons.
1K-3.3M
1.25K-4.2M
250-830K 500-1.7M
50-170K 250-500K
400-10M
spindles
with
any
of
these
instruments.
800-20M
1K-25M
400-10M
200-5M
40-1M
500-1M
However, it is possible to use the above
1K-2M 1.25K-2.5M
50-100K 250-500K 500-1M
500-10M
Digital
Viscometers/Rheometers
will
1K-20M
1.25K-25M
500-10M
250-5M
50-1M
spindles with any of these instruments.
200-5M 400-10M 400-10M 800-20M 1K-25M
40-1M
1K-3.3M 2K-6.7M 2.5K-8.3M
automatically
calculate viscosity. Please
1K-3.3M 500-10M
100-300K
Digital Viscometers/Rheometers
will
1K-20M 1.25K-25M
250-5M 500-10M
50-1M 500-1.7M
1K-3.3M
contact
Brookfield
or
an
authorized
dealer
if
1K-3.3M
500-1.7M
100-300K
automatically calculate viscosity. Please
2K-6.7M 2.5K-8.3M
2.5K-8.3M
100-300K 500-1.7M 1K-3.3M 1K-3.3M 2K-6.7M
1K-2M
you require
information
on viscositydealer
range.if
2K-4M 2.5K-8.3M
2.5K-5M
1K-2M
500-1M 1K-3.3M
100-200K
1K-3.3M
contact
Brookfield
or an authorized
2K-6.7M
100-300K 500-1.7M
1.6K-40M
3.2K-80M
4K-100M
1.6K-40M
800-20M
160-4M
1K-2M
you require information on viscosity range.
2K-4M
2.5K-5M
1K-2M
100-200K 500-1M
2K-40M
4K-80M 5K-100M
2K-40M 1.6K-40M
1K-20M 1.6K-40M
200-4M
3.2K-80M
4K-100M
160-4M 800-20M
4K-13.3M
400-1.3M
2K-40M 8K-26.7M
4K-80M 10K-33.3M
5K-100M
2K-40M
1K-20M 4K-13.3M
200-4M 2K-6.7M
4K-13.3M
8K-26.7M
4K-13.3M
2K-6.7M
400-1.3M
4K-13.3M
8K-26.7M 10K-33.3M
10K-33.3M
400-1.3M 2K-6.7M 4K-13.3M
4K-8M
8K-16M 10K-33.3M
10K-20M
4K-8M 4K-13.3M
2K-4M 4K-13.3M
400-800K
8K-26.7M
400-1.3M 2K-6.7M
1.5-30K
1.2-30K
3-10K
1.5-30K
3-10K
3-10K
5-10K
3-10K
.NJMMJPO,UIPVTBOE/31.FH4QJOEMF4$YSQN
TFDD1$FOUJQPJTFN1BtT.JMMJQBTDBMtTFDPOET
4K-8M
8K-16M 10K-20M
4K-8M
400-800K 2K-4M
HBT
N/A = Not applicable for historical reasons. However, it is possible to use any spindle/chamber combination with any torque range. Digital viscometers/rheometers will automatically calculate viscosity.
.NJMMJPO,UIPVTBOE/31.FH4QJOEMF4$YSQN
TFDD1$FOUJQPJTFN1BtT.JMMJQBTDBMtTFDPOET
* Examples
N/A
= NotSample
applicable
for historical reasons. However, it is possible to use any spindle/chamber combination
with Sample
any torque
range.with
Digital
viscometers/rheometers
will automatically calculate viscosity.
SC4-13R
Chamber
SC4-13RP
Chamber
RTD
temperature probe
* Examples Sample Chamber with RTD temperature probe and cable to viscometer/rheometer
SC4-13RPY
SC4-13R Stainless
Sample Steel
Chamber
SC4-27
Spindle
SC4-13RPY
Chamber
with
temperature
probe
and cable
to viscometer/rheometer
**
DisposableSample
chamber
available
in RTD
13R size
and requires
SC4-45YD
water
jacket
SC4-27 Stainless Steel Spindle
SC4-13RD-100 Disposable Sample Chamber available in packages of 100
SC4-13RP Disposable
Sample Chamber
SC4-27D
Spindlewith RTD temperature probe
SC4-13RD-100
Sample
available in-packages
of 100
Note:
Hastelloy Disposable
C available for
someChamber
spindles/chambers
call for details
SC4-27D Disposable Spindle
** Disposable chamber available in 13R size and requires SC4-45YD water jacket
Note: Hastelloy C available for some spindles/chambers - call for details
Removable Sample Chamber
The
design of
the Small
Sample Adapter allows the sample chamber to be easily changed
Removable
Sample
Chamber
and
cleaned
without
disturbing
set-upallows
of thethe
viscometer
or temperature
bath. changed
This
The design of the Small Samplethe
Adapter
sample chamber
to be easily
means
that
successive
measurements
can
be
made
under
identical
conditions.
and cleaned without disturbing the set-up of the viscometer or temperature bath. This
means
that successive
Temperature
Control measurements can be made under identical conditions.
The
sample chamber
Temperature
Control fits into a water jacket so that precise temperature control can be
achieved
when
the Brookfi
eld acirculating
temperature
bath istemperature
used. The stirring
The sample chamber
fits into
water jacket
so that precise
control action
can be
of
the
rotating
spindle,
plus
the
small
sample
volume,
helps
to
keep
the
temperature
achieved when the Brookfield circulating temperature bath is used. The stirring action
gradient
acrossspindle,
the sample
minimum.
Direct
readout
of to
sample
is
of
the rotating
plus to
thea small
sample
volume,
helps
keep temperature
the temperature
provided
using
sample
chambers
with
optional
embedded
RTD
sensor
connected
gradient across the sample to a minimum. Direct readout of sample temperature isto
the
DV-I Prime
and DV-II+Pro
Viscometers
and embedded
the DV-III Ultra
Rheometer.
Working
provided
using sample
chambers
with optional
RTD sensor
connected
to
temperature
range
for
the
Small
Sample
Adapter
is
from
–15°C
to
100°C.
the DV-I Prime and DV-II+Pro Viscometers and the DV-III Ultra Rheometer. Working
temperature
range for the Small Sample Adapter is from –15°C to 100°C.
Cylindrical Geometry
The
Small Sample
Adapter’s coaxial cylinder geometry provides extremely accurate
Cylindrical
Geometry
viscosity
measurements
at defi
ned shear
rates.
The Small Sample Adapter’s
coaxial
cylinder
geometry provides extremely accurate
viscosity measurements
at defiand
ned SC4-27D
shear rates.
Disposable
Sample Chambers
Spindle
Disposable
13R
chambers,
for
hard-to-clean
materials,
Disposable Sample Chambers and SC4-27D Spindle are available in a kit that comes
complete with
chambers
special-sized
water jacket
(Part No.inSSA-DCU).
Disposable
13R100
chambers,
forand
hard-to-clean
materials,
are available
a kit that comes
Additional
disposable
chambers
can
be
purchased
in
quantities
of
100
complete with 100 chambers and special-sized water jacket (Part No. SSA-DCU).
(Part
No. SC4-13RD-100).
Additional
disposable chambers can be purchased in quantities of 100
(Part No.Option
SC4-13RD-100).
EZ-Lock
Small Sample
EZ-Lock
OptionAdapter is now available with special EZ-Lock spindle coupling for use on
standard
Brookfi
eld Viscometers/Rheometers
alreadyEZ-Lock
equipped
with the
EZ-Lock
Small Sample
Adapter
is now available with special
spindle
coupling
for feature.
use on
standard Brookfield Viscometers/Rheometers already equipped with the EZ-Lock feature.
2.
2.
1.
1.
7.
4.
7.
4.
3.
3.
Water jacket allows rapid and precise
temperature
of sample
Water jacket control
allows rapid
and precise
temperature
control
of sample
Sample chamber
easily
changed - slides into
water
jacket
and
locks
in
place - slides into
Sample chamber easily changed
water
jacket and
lockstemperature
in place
Simultaneous
sample
measurement
possible
by ordering embedded
Simultaneous is
sample
temperature
temperature
probe
in
sample
chamberembedded
measurement is possible by ordering
temperature
probe inchamber
sample chamber
Optional
disposable
also available
39
Optional disposable chamber also available
39