Sample Preparation Systems High Pressure Asher System Supplies Sample Pr

Sample Preparation Systems
High Pressure Asher System Supplies
Reaction Vessel Racks
Heat trays are heating blocks for insertion of reaction
vessels into the HPA-S pressure chamber.
Reaction vessel racks are made of PVC and are
used to hold reaction vessels.
Heat Tray for 5 Vessels
Part No.
Aluminum block for insertion of five
quartz digestion vessels — 90 mL.
B0511601
Heat Tray for 6 Vessels
Aluminum block for insertion of six
(glassy carbon) digestion vessels — 20 mL.
Heat Tray for 7 Vessels
Aluminum block for insertion of seven
quartz digestion vessels — 50 mL.
Part No.
B0511523
Part No.
B0511602
Each (€)
627
Each (€)
375
Each (€)
627
Heat Tray for 14 Vessels
15 mL Reaction Vessel Rack
PVC rack for holding up to 14
15 mL reaction vessels.
Part No.
B0511526
Sample Preparation Systems
Heat Trays
Each (€)
98
20 mL Reaction Vessel Rack
PVC rack for holding up to six 20 mL
glassy carbon reaction vessels.
50 mL Reaction Vessel Rack
PVC rack for holding up to seven
50 mL (or older 30 mL) reaction vessels.
Part No.
B0511527
Part No.
B0511525
Each (€)
98
Each (€)
98
90 mL Reaction Vessel Rack
Aluminum block for insertion of
14 quartz digestion vessels — 15 mL.
Heat Tray for 21 Vessels
Aluminum block for insertion of
21 quartz digestion vessels — 15 mL.
Part No.
B0511522
Part No.
B0511603
Each (€)
604
Each (€)
710
PVC rack for holding up to five
90 mL reaction vessels.
Part No.
B0511524
Each (€)
98
Reaction Vessel Sets
Reaction vessel sets are complete and include reaction vessels,
lids, heat tray, vessel rack, and PTFE tape for vessel closure.
5 x 90 mL Quartz Reaction Vessel Set
Reaction Vessels and Lids
Used for the digestion of five samples
(maximum weight 1.5 g each) in
90 mL quartz vessels.
Part No.
B0511502
Each (€)
1980
6 x 20 mL Glassy Carbon Reaction Vessel Set
Used for the digestion of six samples
(maximum weight 0.8 g each) in
20 mL glassy carbon vessels.
Part No.
B0511505
Each (€)
3040
7 x 50 mL Quartz Reaction Vessel Set
Used for the digestion of seven samples
(maximum weight 0.8 g each) in
50 mL quartz vessels.
Part No.
15 mL Quartz
50 mL Quartz
90 mL Quartz
20 mL Glassy Carbon
B0511516
B0511514
B0511513
B0511518
Each (€) Req.Lid Part No.
76
156
196
330
16 mm B0511517
22 mm B0511515
22 mm B0511515
B0511519
Each (€)
42
69
69
70
B0511503
Each (€)
2380
14 x 15 mL Quartz Reaction Vessel Set
Used for the digestion of 14 samples
(maximum weight 0.2 g each) in
15 mL quartz vessels.
Part No.
B0511504
Each (€)
Atomic Absorption
Reaction Vessel
Part No.
2582
See page 2
4 for ordering information.
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51
Sample Preparation Systems
High Pressure Asher System Supplies
Sample Preparation Systems
Supplies
Back-up Ring for O-Ring
Special back-up ring made of
reinforced PTFE compound located
behind O-Ring B0511528.
Extraction Tool
Tool for removing heat trays from
the HPA-S pressure chamber.
Part No.
Each (€)
B0511529
Part No.
20
Each (€)
B0511512
310
O-Ring 107 x 5 FPM with FEP Coating
Special O-Ring for hermetically sealing
the high-pressure chamber safety lid.
Part No.
Each (€)
B0511528
56
PTFE Tape
Analytically pure PTFE tape for
positioning the lids on the reaction
vessels. The roll is 6.5 m.
Part No.
B0511507
Each (€)
17
Rupture Disk, DN 15
Made of corrosion-resistant Inconel® alloy with a burst
pressure of 180 bar. This allows for overpressure relief in
case of heavy explosions inside the HPA-S. Replace rupture
disk after approximately 750 cycles.
Part No.
Each (€)
B0511511
168
Support Ring, PEEK
Located behind the back-up ring (B0511529), this support
ring gives mechanical stability
Part No.
Each (€)
to the entire seal assembly.
B0511530
117
Wrapping Tool for PTFE Tape
Atomic Absorption
Tool for closing the HPA-S vessels
with their lids using PTFE tape by
applying a special wrapping technique.
52
Part No.
B0511506
Each (€)
890
Sample Preparation Systems
Multiwave
Multiwave Accessories and Supplies
Sample Preparation Systems
The Multiwave can be used with a wide variety of reaction vessels allowing the application of optimum reaction conditions
for almost every type of sample. The table below provides an overview of all the available reaction vessel assemblies.
HQ20
Characteristics
Small, high temperature vessel for analysis of
micro-samples of a few mg, for ultratrace analysis
MF100
Characteristics
Large vessel for versatile applications,
for combined organic-inorganic samples
Typical Applications
■ Pharmaceuticals
■ Biological and forensic microsamples
■ Biopolymers
Typical Applications
■ Soil, sediments
■ Ashes, slags
■ Metals, ores
■ Glass, quartz
HQ50
Characteristics
High temperature vessel for organic material,
for Hg detection, and for ultratrace analysis
LF100
Characteristics
Vessel with high over-pressure tolerance,
for high throughput of “easy” samples
Typical Applications
■ Food (high fat)
■ Plastics, Fibers
■ Oil, Grease, Coal
■ Pigments
Typical Applications
■ Water, effluent
■ Metals, alloys
■ Plant material
■ Beverages
HF50
Characteristics
For high pressure (HF) applications
of difficult organics and inorganics
Typical Applications
■ Semiconductor
■ Ceramics
■ Oxides
■ Geological material
Type*
Volume
Material
Operation
Pressure
Maximum
Pressure
Maximum
Temperature
Applicable
Rotor Type
Typical Sample
Weight
Maximum Filling
Volume
HQ20
20 mL
Quartz
75 bar
130 bar
300 ºC
6-position
10-200 mg
6 mL
HQ50
50 mL
Quartz
75 bar
130 bar
300 ºC
6-position
100-1000 mg
20 mL
B0502197
1721
HF50
50 mL
TFM
75 bar
130 bar
260 ºC
6-position
50-500 mg
20 mL
B0511677
1041
MF100
100 mL
TFM (PFA) 30 bar
70 bar
260 ºC
6-position
100-1500 mg
50 mL
B0511541
1180
LF100
100 mL
PFA
70 bar
230 ºC
12-position
100-1000 mg
50 mL
B3140380
545
Each (€)
Atomic Absorption
20 bar
Part No.
*Type definition: HQ50
Volume: 20, 50, 100 mL
Material: Q…Quartz
F…Fluorpolymer (TFM or PFA)
Pressure: H…High
M…Medium
L…Low
Multiwave – shipped prior to January 2002
See page 2
4 for ordering information.
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visit www.perkinelmer.com/supplies
53
Sample Preparation Systems
Multiwave
Sample Preparation Systems
Reaction Vessel Assemblies
Reaction vessel assemblies include a reaction vessel, screw cap and (where appropriate) liner, support vessel,
plug safety disk, base plate, and jacket.
Item
Description
HQ20
HQ50
HF50
MF100
G
Quartz vessel Q20 (20 mL)
A
Quartz vessel Q50EW (50 mL)*
O
Liner F50
J
Liner F100
■
N
Liner F100-PFA
A
P
Supporting vessel 50
M
Supporting vessel 100
Q
Supporting vessel with thread
D
Plug
F
Plug B
■
E
Safety Disk H
L
Safety Disk M
H
Seal 25, pkg. 6
K
Seal 40, pkg. 6
I
LF100
■
B0511674
643
B0511675
152
A
B0511532
102
■
B0511678
57
B0511676
230
B0511533
168
■
■
■
■
B3140382
164
■
B0502201
123
B0511539
271
B0502202
13
■
■
■
■
■
■
■
■
Vessel base plate
■
■
■
B
Bomb jacket PEEK
■
■
■
■
N/A
C
Screw cap PEEK
■
■
■
■
N/A
R
Screw cap L PEEK
■
■
■
Each (€)
549
■
■
Part No.
B0511538
■
■
B0511535
12
B0502203
135
B0511534
139
B0502204
148
B3140383
234
* B0511674 replaces former B0502198, quartz vessel, 50 mL
■ Part of respective pressure vessel type
A – possible alternative item
C
C
R
C
F
D
D
C
E
H
D
E
H
D
L
L
K
K
E
H
A
O
M
Atomic Absorption
G
P
N
J
I
I
I
B
B
Q
B
B
HQ20 High Pressure Quartz
Reaction Vessel Assembly
54
HQ50 Part No. B0502197
High Pressure Quartz
Reaction Vessel Assembly
HF50 Part No. B0511677
High Pressure TFM
Reaction Vessel Assembly
MF100 Part No. B0511541
Medium Pressure (PFA or TFM)
Reaction Vessel Assembly
LF100 Part No. B3140380
Low Pressure PFA
Reaction Vessel Assembly
Sample Preparation Systems
Multiwave
Reaction Vessel Racks
Sample Preparation Systems
PVC rack for holding up to six reaction vessels.
Description
Part No.
HQ20
HQ50 or HF50
MF100 or LF100
B0511540
B0511546
B0511546
Each (€)
154
86
86
Rotors and Rotor Assemblies
Reaction
Vessel Type
Description
Part No.
HQ20
Rotor Only
B0502196
4017
HF50
Rotor Assembly
(includes Rotor
and 6 vessels)
Reaction Vessel Assembly
Rotor Only
B0511679
7400
B0511677
B0502196
1041
4017
Rotor Assembly
(includes Rotor
and 6 vessels)
Reaction Vessel Assembly
Rotor Only
B0502195
8000
B0502197
B0502196
1721
4017
Rotor Assembly
(includes Rotor
and 6 vessels)
Reaction Vessel Assembly
Rotor Only
B0511537
9800
B0511541
B0502196
1180
4017
Rotor Assembly
(includes Rotor,
1sensor vessel, and 11
pressure vessles)
Reaction Vessel Assembly*
Reaction Vessel Assembly**
Rotor Only
B3140386
8600
B3140381
B3140380
B3140387
1410
545
2656
HQ50
MF100
LF100
Each (€)
* Sensor Vessel
** Pressure Vessel
Atomic Absorption
See page 2
4 for ordering information.
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55
Sample Preparation Systems
Multiwave 3000
Sample Preparation Systems
Multiwave 3000 Accessories
and Supplies
The Multiwave 3000
The Anton Paar Multiwave™ 3000 is a versatile and powerful
microwave sample preparation system for safe high-pressure
acid digestions of all types of organic and inorganic samples.
The Multiwave 3000 provides dramatically improved sample
capacity, a more powerful dual-magnetron design, superior
sensors requiring no cables and built-in methods. It offers
unique pressure monitoring and a multilevel safety system
that give you the performance and safety you want.
Important user benefits of the Multiwave 3000 are:
■
Reduced analysis times by fast digestion, using rapid
microwave heating and short cool-down times
■
Superior digestion quality using closed vessels and
simultaneous high pressure and high temperature
■
Time-saving, easy operation by simplified method
development and easy, intuitive software
■
Maximum safety provided by easy handling, sophisticated
sensors, and a library of tested methods
■
1400 W microwave power ensures fast heating
■
Unpulsed microwave power from 0 to 1400 W
for precise control of critical reactions
■
Reliable remote sensors for convenient operation
■
Fast, built-in cooling system to reduce total cycle time
resulting in improved productivity
■
Intuitive software for easy routine operation
and documentation
■
Large PTFE-coated cavity for rough laboratory environments
■
Proven safety system to minimize hazards from
violent reactions
■
Modular, industrial-type design offers individual
choice of configurations
Multiwave 3000
Atomic Absorption
The 16-position rotor maximizes productivity.
Rotor 8 for advanced
digestions offers simultaneous
pressure sensing in all vessels.
Multiwave is a trademark of Anton Paar, GmbH
56
Sample Preparation Systems
Multiwave 3000 Digestion Rotors
XF100
Rotor 8 Consumables and Vessels
1
Sample Preparation Systems
Pressure Vessel XF100
Complete reaction vessel for various
applications at elevated pressure
and temperature.
Part No.
Each (€)
N3142345
960
6
2
7
Specifications
Volume:
Working pressure:
Opening pressure:
Max. temperature:
1
2
3
4
5
6
7
8
9
10
11
3
100 mL
60 bar (870 psi)
120 bar (1740 psi)
260 °C
Components
Part No.
PEEK Protective Cap
Safety Disk Holder X
Safety Disk X
PEK Seal Holder
PEEK Center Ring
Syringe Connector
Venting Screw
PTFE-TFM Seal
100 mL TFM liner
H100 Ceramics Jacket
PEEK Protective Casing
N3142353
N3142350
N3142349
N3142351
N3142354
N3141022
N3141021
N3141015
N3141014
N3141019
N3142352
8
9
Each (€)
39
27
11
141
25
17
21
72
130
388
115
Pressure Vessel XQ80
Part No.
Each (€)
Complete pressure vessel for
digestions at extreme conditions.
N3142346
1310
10
5
11
XQ80
1
Specifications
Volume:
Working pressure:
Opening pressure:
Max. temperature:
4
80 mL
80 bar (1160 psi)
120 bar (1740 psi)
300 °C
6
2
7
Part No.
PEEK Protective Cap
Safety Disk Holder X
Safety Disk X
PEK Seal Holder
PEEK Center Ring
Syringe Connector
Venting Screw
PEEK Protective Casing
PTFE-TFM Seal XQ
Quartz Vessel
N3142353
N3142350
N3142349
N3142351
N3142354
N3141022
N3141021
N3142352
N3142348
N3142347
Each (€)
39
27
11
141
25
17
21
115
121
820
3
4
12
5
13
Atomic Absorption
1
2
3
4
5
6
7
11
12
13
Components
11
See page 2
4 for ordering information.
For the most current product listing,
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57
Sample Preparation Systems
Multiwave 3000 Digestion Rotors
1
3
Rotor 8 Consumables and Vessels
4
Sample Preparation Systems
Immersing Temperature Probe T-Probe for Rotor 8
5
Immersing temperature probe
for precise measurement of the
solution temperature in Rotor
8XF100 and XQ80. The sensor
head includes a gas-bulb
thermometer for monitoring
the decomposition
temperature up to 280 °C.
The sensor is hermetically
shielded by a sapphire
thermowell. Its microwavetransparent design does not
interfere with the microwave
field. The installation is very
easy and does not require any
electrical connections, cables
or hoses. Requires Immersion
Tube with either Seal XQ
(N3142410) or Seal XF
(N3142411).
2
6
7
8
Immersion Tube
with Seal XF
1
3
Part No.
Each (€)
N3142409
2190
Immersion Tube with Seal XF
Part No.
Each (€)
Assembly of a special seal holder
with seal for XF100-vessels.
N3142411
Immersion Tube with Seal XQ
Part No.
Assembly of a special seal holder
with seal for XQ80-vessels.
N3142410
980
4
5
2
Each (€)
980
9
11
22
3
4
5
6
7
8
9
7
Atomic Absorption
Immersion Tube
with Seal XQ
8
58
Components
Part No.
Safety Disk Holder X
Safety Disk X
Syringe Connector
Seal Holder X for T-Probe
Venting Screw
Seal XF*
Husk
Immersion Tube Sapphire X
Seal XQ for T-Probe
N3142350
N3142349
N3141022
N3142415
N3141021
N3141016
N3142416
N3142413
N3142412
* Also used for Rotor 16 Pressure/Temperature Sensor.
Each (€)
27
11
17
141
21
92
7
653
133
Sample Preparation Systems
Multiwave 3000 Digestion Rotors
Rotor 8 Spare Parts
Complete 8 position rotor
without reaction vessels.
1
2
1
2
3
4
5
6
7
8
9
10
Part No.
Each (€)
N3142355
6700
Components
Part No.
Each (€)
Rotor 8 Lid
Liner Extractor Bolt 8
Rotor Upper Plate (Assembled)
Fastening Screw
Thumbwheel
Insulating Bushing*
Bottom Guard
Bottom Load Ring Al Green
Tension Bar Short
Protection Hose 8
N3142364
N3142366
N3142356
N3142485
N3142363
N3142486
N3142357
N3142431
N3142430
N3142360
Sample Preparation Systems
Rotor 8 (without Vessels)
162
68
5000
99
23
18
290
1673
140
13
* Used with Black Rotor 8 upper plates shipped prior to July 2005.
Rotor 8 for Advanced Digestions
2
3
4
5
6
1
7
Atomic Absorption
8
9
10
See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies
59
Sample Preparation Systems
Multiwave 3000 Digestion Rotors
10
Rotor 16 Consumables and Vessels
Sample Preparation Systems
11
9
5
8
3
Pressure Vessel MF100 MW3000
Part No.
Complete reaction vessel for routine
and quality control applications.
N3141011
Each (€)
386
Specifications
Volume:
Working pressure:
Opening pressure:
Max. temperature:
1
100 mL
20 bar (290 psi)
70 bar (1000 psi)
200 °C
Pressure Vessel HF100 MW3000
Part No.
Complete reaction vessel for
versatile applications.
N3141012
Each (€)
660
6 7
Specifications
Pressure Vessel MF100
(N3141011) respectively
HF100 (N3141012)
Volume:
Working pressure:
Opening pressure:
Max. temperature:
100 mL
40 bar (580 psi)
70 bar (1000 psi)
240 °C
Components
Part No.
100 mL TFM Liner
M100 PEEK Vessel Jacket
PTFE-TFM Seal
Safety Disk
PEK Screw Cap
H100 Ceramics Jacket
Venting Screw
Package of 16 Venting Screws
Syringe Connector
Safety Disk Holder M&H
N3141014
N3141018
N3141015
N3141017
N3141020
N3141019
N3141021
N3142452
N3141022
N3141023
Each (€)
12
10
9
1
6
3
5
8
7
9
10
11
11
130
92
72
8
143
388
21
220
17
25
14
13
5
Pressure/Temperature Sensor Accessory
for Rotor 16
4
Pressure/Temperature
Sensor Accessory
Sensor screw cap for simultaneous
pressure and internal temperature
measurement of one MF or HF vessel.
15
Part No.
Each (€)
N3141005
3340
Pressure Sensor Accessory for Rotor 16
Sensor screw cap for pressure
measurement of one MF or HF vessel.
Atomic Absorption
10
9
14
11
5
Pressure Sensor
Accessory
60
13
3
4
12
13
14
15
Part No.
Each (€)
N3142418
2200
Components
Part No.
Seal p/T Sensor
Immersion Tube Sapphire M&H
O-Ring 38x1.5 FPM
Seal Holder for p/T Sensor
Husk
Husk Assembly Tool
N3141016
N3142013
N3142400
N3142399
N3142416
N3142456
Each (€)
92
680
2
153
7
2
Sample Preparation Systems
Multiwave 3000 Digestion Rotors
Rotor 16 Spare Parts
Sample Preparation Systems
Rotor 16 (without Vessels)
Complete 16-position rotor without
reaction vessels and sensors.
1
2
3
4
5
6
7
8
Part No.
Each (€)
N3141025
1180
Components
Part No.
Rotor 16 Body
Rotor 16 Lid
Rotor 16 Tray
Rotor Base Ring
Vessel Holder
Seal for Vessel Holder
Cheese Head Screw
Liner Extractor Bolt
N3141026
N3141027
N3141028
N3141029
N3141030
N3141031
N3142398
N3141032
2
1
Each (€)
100
72
139
158
45
17
2
68
4
7
Spare Parts for the Rotor 16
2
3
8
5
6
Atomic Absorption
Rotor 16 for routine digestions
1
Rotor 16
See page 2
4 for ordering information.
For the most current product listing,
visit www.perkinelmer.com/supplies
61
Sample Preparation Systems
Multiwave 3000 Drying and Evaporation Rotors
Sample Preparation Systems
Rotor 1 DRY Supplies
1
1
2
2
3
4
4
Each (€)
Components
Part No.
Filter Disk Borosilicate Glass
D=30 Porosity 0
Glass Tube
Desiccator Plate
O-Ring
28.24 x 2.62 Silicone
N3142000
9
N3142001
N3142002
N3142003
274
102
2
Components
Part No.
Hose Connector 8/8
Connection Hose
Hose Connector Nut
Syringe Filter
Screw Cap EVAP
Seal EVAP
Vessel Holder
Seal for Vessel Holder
Liner Extractor Bolt 16
Rotor Tray EVAP
Rotor 16 Body
Rotor Base Ring
Cheese Head Screw
Ring Weight
N3142370
N3142367
N3142371
N3142374
N3142373
N3142372
N3141030
N3141031
N3141032
N3142369
N3141026
N3141029
N3142398
N3142368
3
Rotor 8 EVAP Supplies
2
4
5
1
3
6
7
8
9
Atomic Absorption
10
11
12
13
14
62
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Each (€)
131
29
80
8
96
66
45
17
68
133
100
158
2
39