Sample Preparation Systems High Pressure Asher System Supplies Reaction Vessel Racks Heat trays are heating blocks for insertion of reaction vessels into the HPA-S pressure chamber. Reaction vessel racks are made of PVC and are used to hold reaction vessels. Heat Tray for 5 Vessels Part No. Aluminum block for insertion of five quartz digestion vessels — 90 mL. B0511601 Heat Tray for 6 Vessels Aluminum block for insertion of six (glassy carbon) digestion vessels — 20 mL. Heat Tray for 7 Vessels Aluminum block for insertion of seven quartz digestion vessels — 50 mL. Part No. B0511523 Part No. B0511602 Each (€) 627 Each (€) 375 Each (€) 627 Heat Tray for 14 Vessels 15 mL Reaction Vessel Rack PVC rack for holding up to 14 15 mL reaction vessels. Part No. B0511526 Sample Preparation Systems Heat Trays Each (€) 98 20 mL Reaction Vessel Rack PVC rack for holding up to six 20 mL glassy carbon reaction vessels. 50 mL Reaction Vessel Rack PVC rack for holding up to seven 50 mL (or older 30 mL) reaction vessels. Part No. B0511527 Part No. B0511525 Each (€) 98 Each (€) 98 90 mL Reaction Vessel Rack Aluminum block for insertion of 14 quartz digestion vessels — 15 mL. Heat Tray for 21 Vessels Aluminum block for insertion of 21 quartz digestion vessels — 15 mL. Part No. B0511522 Part No. B0511603 Each (€) 604 Each (€) 710 PVC rack for holding up to five 90 mL reaction vessels. Part No. B0511524 Each (€) 98 Reaction Vessel Sets Reaction vessel sets are complete and include reaction vessels, lids, heat tray, vessel rack, and PTFE tape for vessel closure. 5 x 90 mL Quartz Reaction Vessel Set Reaction Vessels and Lids Used for the digestion of five samples (maximum weight 1.5 g each) in 90 mL quartz vessels. Part No. B0511502 Each (€) 1980 6 x 20 mL Glassy Carbon Reaction Vessel Set Used for the digestion of six samples (maximum weight 0.8 g each) in 20 mL glassy carbon vessels. Part No. B0511505 Each (€) 3040 7 x 50 mL Quartz Reaction Vessel Set Used for the digestion of seven samples (maximum weight 0.8 g each) in 50 mL quartz vessels. Part No. 15 mL Quartz 50 mL Quartz 90 mL Quartz 20 mL Glassy Carbon B0511516 B0511514 B0511513 B0511518 Each (€) Req.Lid Part No. 76 156 196 330 16 mm B0511517 22 mm B0511515 22 mm B0511515 B0511519 Each (€) 42 69 69 70 B0511503 Each (€) 2380 14 x 15 mL Quartz Reaction Vessel Set Used for the digestion of 14 samples (maximum weight 0.2 g each) in 15 mL quartz vessels. Part No. B0511504 Each (€) Atomic Absorption Reaction Vessel Part No. 2582 See page 2 4 for ordering information. For the most current product listing, visit www.perkinelmer.com/supplies 51 Sample Preparation Systems High Pressure Asher System Supplies Sample Preparation Systems Supplies Back-up Ring for O-Ring Special back-up ring made of reinforced PTFE compound located behind O-Ring B0511528. Extraction Tool Tool for removing heat trays from the HPA-S pressure chamber. Part No. Each (€) B0511529 Part No. 20 Each (€) B0511512 310 O-Ring 107 x 5 FPM with FEP Coating Special O-Ring for hermetically sealing the high-pressure chamber safety lid. Part No. Each (€) B0511528 56 PTFE Tape Analytically pure PTFE tape for positioning the lids on the reaction vessels. The roll is 6.5 m. Part No. B0511507 Each (€) 17 Rupture Disk, DN 15 Made of corrosion-resistant Inconel® alloy with a burst pressure of 180 bar. This allows for overpressure relief in case of heavy explosions inside the HPA-S. Replace rupture disk after approximately 750 cycles. Part No. Each (€) B0511511 168 Support Ring, PEEK Located behind the back-up ring (B0511529), this support ring gives mechanical stability Part No. Each (€) to the entire seal assembly. B0511530 117 Wrapping Tool for PTFE Tape Atomic Absorption Tool for closing the HPA-S vessels with their lids using PTFE tape by applying a special wrapping technique. 52 Part No. B0511506 Each (€) 890 Sample Preparation Systems Multiwave Multiwave Accessories and Supplies Sample Preparation Systems The Multiwave can be used with a wide variety of reaction vessels allowing the application of optimum reaction conditions for almost every type of sample. The table below provides an overview of all the available reaction vessel assemblies. HQ20 Characteristics Small, high temperature vessel for analysis of micro-samples of a few mg, for ultratrace analysis MF100 Characteristics Large vessel for versatile applications, for combined organic-inorganic samples Typical Applications ■ Pharmaceuticals ■ Biological and forensic microsamples ■ Biopolymers Typical Applications ■ Soil, sediments ■ Ashes, slags ■ Metals, ores ■ Glass, quartz HQ50 Characteristics High temperature vessel for organic material, for Hg detection, and for ultratrace analysis LF100 Characteristics Vessel with high over-pressure tolerance, for high throughput of “easy” samples Typical Applications ■ Food (high fat) ■ Plastics, Fibers ■ Oil, Grease, Coal ■ Pigments Typical Applications ■ Water, effluent ■ Metals, alloys ■ Plant material ■ Beverages HF50 Characteristics For high pressure (HF) applications of difficult organics and inorganics Typical Applications ■ Semiconductor ■ Ceramics ■ Oxides ■ Geological material Type* Volume Material Operation Pressure Maximum Pressure Maximum Temperature Applicable Rotor Type Typical Sample Weight Maximum Filling Volume HQ20 20 mL Quartz 75 bar 130 bar 300 ºC 6-position 10-200 mg 6 mL HQ50 50 mL Quartz 75 bar 130 bar 300 ºC 6-position 100-1000 mg 20 mL B0502197 1721 HF50 50 mL TFM 75 bar 130 bar 260 ºC 6-position 50-500 mg 20 mL B0511677 1041 MF100 100 mL TFM (PFA) 30 bar 70 bar 260 ºC 6-position 100-1500 mg 50 mL B0511541 1180 LF100 100 mL PFA 70 bar 230 ºC 12-position 100-1000 mg 50 mL B3140380 545 Each (€) Atomic Absorption 20 bar Part No. *Type definition: HQ50 Volume: 20, 50, 100 mL Material: Q…Quartz F…Fluorpolymer (TFM or PFA) Pressure: H…High M…Medium L…Low Multiwave – shipped prior to January 2002 See page 2 4 for ordering information. For the most current product listing, visit www.perkinelmer.com/supplies 53 Sample Preparation Systems Multiwave Sample Preparation Systems Reaction Vessel Assemblies Reaction vessel assemblies include a reaction vessel, screw cap and (where appropriate) liner, support vessel, plug safety disk, base plate, and jacket. Item Description HQ20 HQ50 HF50 MF100 G Quartz vessel Q20 (20 mL) A Quartz vessel Q50EW (50 mL)* O Liner F50 J Liner F100 ■ N Liner F100-PFA A P Supporting vessel 50 M Supporting vessel 100 Q Supporting vessel with thread D Plug F Plug B ■ E Safety Disk H L Safety Disk M H Seal 25, pkg. 6 K Seal 40, pkg. 6 I LF100 ■ B0511674 643 B0511675 152 A B0511532 102 ■ B0511678 57 B0511676 230 B0511533 168 ■ ■ ■ ■ B3140382 164 ■ B0502201 123 B0511539 271 B0502202 13 ■ ■ ■ ■ ■ ■ ■ ■ Vessel base plate ■ ■ ■ B Bomb jacket PEEK ■ ■ ■ ■ N/A C Screw cap PEEK ■ ■ ■ ■ N/A R Screw cap L PEEK ■ ■ ■ Each (€) 549 ■ ■ Part No. B0511538 ■ ■ B0511535 12 B0502203 135 B0511534 139 B0502204 148 B3140383 234 * B0511674 replaces former B0502198, quartz vessel, 50 mL ■ Part of respective pressure vessel type A – possible alternative item C C R C F D D C E H D E H D L L K K E H A O M Atomic Absorption G P N J I I I B B Q B B HQ20 High Pressure Quartz Reaction Vessel Assembly 54 HQ50 Part No. B0502197 High Pressure Quartz Reaction Vessel Assembly HF50 Part No. B0511677 High Pressure TFM Reaction Vessel Assembly MF100 Part No. B0511541 Medium Pressure (PFA or TFM) Reaction Vessel Assembly LF100 Part No. B3140380 Low Pressure PFA Reaction Vessel Assembly Sample Preparation Systems Multiwave Reaction Vessel Racks Sample Preparation Systems PVC rack for holding up to six reaction vessels. Description Part No. HQ20 HQ50 or HF50 MF100 or LF100 B0511540 B0511546 B0511546 Each (€) 154 86 86 Rotors and Rotor Assemblies Reaction Vessel Type Description Part No. HQ20 Rotor Only B0502196 4017 HF50 Rotor Assembly (includes Rotor and 6 vessels) Reaction Vessel Assembly Rotor Only B0511679 7400 B0511677 B0502196 1041 4017 Rotor Assembly (includes Rotor and 6 vessels) Reaction Vessel Assembly Rotor Only B0502195 8000 B0502197 B0502196 1721 4017 Rotor Assembly (includes Rotor and 6 vessels) Reaction Vessel Assembly Rotor Only B0511537 9800 B0511541 B0502196 1180 4017 Rotor Assembly (includes Rotor, 1sensor vessel, and 11 pressure vessles) Reaction Vessel Assembly* Reaction Vessel Assembly** Rotor Only B3140386 8600 B3140381 B3140380 B3140387 1410 545 2656 HQ50 MF100 LF100 Each (€) * Sensor Vessel ** Pressure Vessel Atomic Absorption See page 2 4 for ordering information. For the most current product listing, visit www.perkinelmer.com/supplies 55 Sample Preparation Systems Multiwave 3000 Sample Preparation Systems Multiwave 3000 Accessories and Supplies The Multiwave 3000 The Anton Paar Multiwave™ 3000 is a versatile and powerful microwave sample preparation system for safe high-pressure acid digestions of all types of organic and inorganic samples. The Multiwave 3000 provides dramatically improved sample capacity, a more powerful dual-magnetron design, superior sensors requiring no cables and built-in methods. It offers unique pressure monitoring and a multilevel safety system that give you the performance and safety you want. Important user benefits of the Multiwave 3000 are: ■ Reduced analysis times by fast digestion, using rapid microwave heating and short cool-down times ■ Superior digestion quality using closed vessels and simultaneous high pressure and high temperature ■ Time-saving, easy operation by simplified method development and easy, intuitive software ■ Maximum safety provided by easy handling, sophisticated sensors, and a library of tested methods ■ 1400 W microwave power ensures fast heating ■ Unpulsed microwave power from 0 to 1400 W for precise control of critical reactions ■ Reliable remote sensors for convenient operation ■ Fast, built-in cooling system to reduce total cycle time resulting in improved productivity ■ Intuitive software for easy routine operation and documentation ■ Large PTFE-coated cavity for rough laboratory environments ■ Proven safety system to minimize hazards from violent reactions ■ Modular, industrial-type design offers individual choice of configurations Multiwave 3000 Atomic Absorption The 16-position rotor maximizes productivity. Rotor 8 for advanced digestions offers simultaneous pressure sensing in all vessels. Multiwave is a trademark of Anton Paar, GmbH 56 Sample Preparation Systems Multiwave 3000 Digestion Rotors XF100 Rotor 8 Consumables and Vessels 1 Sample Preparation Systems Pressure Vessel XF100 Complete reaction vessel for various applications at elevated pressure and temperature. Part No. Each (€) N3142345 960 6 2 7 Specifications Volume: Working pressure: Opening pressure: Max. temperature: 1 2 3 4 5 6 7 8 9 10 11 3 100 mL 60 bar (870 psi) 120 bar (1740 psi) 260 °C Components Part No. PEEK Protective Cap Safety Disk Holder X Safety Disk X PEK Seal Holder PEEK Center Ring Syringe Connector Venting Screw PTFE-TFM Seal 100 mL TFM liner H100 Ceramics Jacket PEEK Protective Casing N3142353 N3142350 N3142349 N3142351 N3142354 N3141022 N3141021 N3141015 N3141014 N3141019 N3142352 8 9 Each (€) 39 27 11 141 25 17 21 72 130 388 115 Pressure Vessel XQ80 Part No. Each (€) Complete pressure vessel for digestions at extreme conditions. N3142346 1310 10 5 11 XQ80 1 Specifications Volume: Working pressure: Opening pressure: Max. temperature: 4 80 mL 80 bar (1160 psi) 120 bar (1740 psi) 300 °C 6 2 7 Part No. PEEK Protective Cap Safety Disk Holder X Safety Disk X PEK Seal Holder PEEK Center Ring Syringe Connector Venting Screw PEEK Protective Casing PTFE-TFM Seal XQ Quartz Vessel N3142353 N3142350 N3142349 N3142351 N3142354 N3141022 N3141021 N3142352 N3142348 N3142347 Each (€) 39 27 11 141 25 17 21 115 121 820 3 4 12 5 13 Atomic Absorption 1 2 3 4 5 6 7 11 12 13 Components 11 See page 2 4 for ordering information. For the most current product listing, visit www.perkinelmer.com/supplies 57 Sample Preparation Systems Multiwave 3000 Digestion Rotors 1 3 Rotor 8 Consumables and Vessels 4 Sample Preparation Systems Immersing Temperature Probe T-Probe for Rotor 8 5 Immersing temperature probe for precise measurement of the solution temperature in Rotor 8XF100 and XQ80. The sensor head includes a gas-bulb thermometer for monitoring the decomposition temperature up to 280 °C. The sensor is hermetically shielded by a sapphire thermowell. Its microwavetransparent design does not interfere with the microwave field. The installation is very easy and does not require any electrical connections, cables or hoses. Requires Immersion Tube with either Seal XQ (N3142410) or Seal XF (N3142411). 2 6 7 8 Immersion Tube with Seal XF 1 3 Part No. Each (€) N3142409 2190 Immersion Tube with Seal XF Part No. Each (€) Assembly of a special seal holder with seal for XF100-vessels. N3142411 Immersion Tube with Seal XQ Part No. Assembly of a special seal holder with seal for XQ80-vessels. N3142410 980 4 5 2 Each (€) 980 9 11 22 3 4 5 6 7 8 9 7 Atomic Absorption Immersion Tube with Seal XQ 8 58 Components Part No. Safety Disk Holder X Safety Disk X Syringe Connector Seal Holder X for T-Probe Venting Screw Seal XF* Husk Immersion Tube Sapphire X Seal XQ for T-Probe N3142350 N3142349 N3141022 N3142415 N3141021 N3141016 N3142416 N3142413 N3142412 * Also used for Rotor 16 Pressure/Temperature Sensor. Each (€) 27 11 17 141 21 92 7 653 133 Sample Preparation Systems Multiwave 3000 Digestion Rotors Rotor 8 Spare Parts Complete 8 position rotor without reaction vessels. 1 2 1 2 3 4 5 6 7 8 9 10 Part No. Each (€) N3142355 6700 Components Part No. Each (€) Rotor 8 Lid Liner Extractor Bolt 8 Rotor Upper Plate (Assembled) Fastening Screw Thumbwheel Insulating Bushing* Bottom Guard Bottom Load Ring Al Green Tension Bar Short Protection Hose 8 N3142364 N3142366 N3142356 N3142485 N3142363 N3142486 N3142357 N3142431 N3142430 N3142360 Sample Preparation Systems Rotor 8 (without Vessels) 162 68 5000 99 23 18 290 1673 140 13 * Used with Black Rotor 8 upper plates shipped prior to July 2005. Rotor 8 for Advanced Digestions 2 3 4 5 6 1 7 Atomic Absorption 8 9 10 See page 2 4 for ordering information. For the most current product listing, visit www.perkinelmer.com/supplies 59 Sample Preparation Systems Multiwave 3000 Digestion Rotors 10 Rotor 16 Consumables and Vessels Sample Preparation Systems 11 9 5 8 3 Pressure Vessel MF100 MW3000 Part No. Complete reaction vessel for routine and quality control applications. N3141011 Each (€) 386 Specifications Volume: Working pressure: Opening pressure: Max. temperature: 1 100 mL 20 bar (290 psi) 70 bar (1000 psi) 200 °C Pressure Vessel HF100 MW3000 Part No. Complete reaction vessel for versatile applications. N3141012 Each (€) 660 6 7 Specifications Pressure Vessel MF100 (N3141011) respectively HF100 (N3141012) Volume: Working pressure: Opening pressure: Max. temperature: 100 mL 40 bar (580 psi) 70 bar (1000 psi) 240 °C Components Part No. 100 mL TFM Liner M100 PEEK Vessel Jacket PTFE-TFM Seal Safety Disk PEK Screw Cap H100 Ceramics Jacket Venting Screw Package of 16 Venting Screws Syringe Connector Safety Disk Holder M&H N3141014 N3141018 N3141015 N3141017 N3141020 N3141019 N3141021 N3142452 N3141022 N3141023 Each (€) 12 10 9 1 6 3 5 8 7 9 10 11 11 130 92 72 8 143 388 21 220 17 25 14 13 5 Pressure/Temperature Sensor Accessory for Rotor 16 4 Pressure/Temperature Sensor Accessory Sensor screw cap for simultaneous pressure and internal temperature measurement of one MF or HF vessel. 15 Part No. Each (€) N3141005 3340 Pressure Sensor Accessory for Rotor 16 Sensor screw cap for pressure measurement of one MF or HF vessel. Atomic Absorption 10 9 14 11 5 Pressure Sensor Accessory 60 13 3 4 12 13 14 15 Part No. Each (€) N3142418 2200 Components Part No. Seal p/T Sensor Immersion Tube Sapphire M&H O-Ring 38x1.5 FPM Seal Holder for p/T Sensor Husk Husk Assembly Tool N3141016 N3142013 N3142400 N3142399 N3142416 N3142456 Each (€) 92 680 2 153 7 2 Sample Preparation Systems Multiwave 3000 Digestion Rotors Rotor 16 Spare Parts Sample Preparation Systems Rotor 16 (without Vessels) Complete 16-position rotor without reaction vessels and sensors. 1 2 3 4 5 6 7 8 Part No. Each (€) N3141025 1180 Components Part No. Rotor 16 Body Rotor 16 Lid Rotor 16 Tray Rotor Base Ring Vessel Holder Seal for Vessel Holder Cheese Head Screw Liner Extractor Bolt N3141026 N3141027 N3141028 N3141029 N3141030 N3141031 N3142398 N3141032 2 1 Each (€) 100 72 139 158 45 17 2 68 4 7 Spare Parts for the Rotor 16 2 3 8 5 6 Atomic Absorption Rotor 16 for routine digestions 1 Rotor 16 See page 2 4 for ordering information. For the most current product listing, visit www.perkinelmer.com/supplies 61 Sample Preparation Systems Multiwave 3000 Drying and Evaporation Rotors Sample Preparation Systems Rotor 1 DRY Supplies 1 1 2 2 3 4 4 Each (€) Components Part No. Filter Disk Borosilicate Glass D=30 Porosity 0 Glass Tube Desiccator Plate O-Ring 28.24 x 2.62 Silicone N3142000 9 N3142001 N3142002 N3142003 274 102 2 Components Part No. Hose Connector 8/8 Connection Hose Hose Connector Nut Syringe Filter Screw Cap EVAP Seal EVAP Vessel Holder Seal for Vessel Holder Liner Extractor Bolt 16 Rotor Tray EVAP Rotor 16 Body Rotor Base Ring Cheese Head Screw Ring Weight N3142370 N3142367 N3142371 N3142374 N3142373 N3142372 N3141030 N3141031 N3141032 N3142369 N3141026 N3141029 N3142398 N3142368 3 Rotor 8 EVAP Supplies 2 4 5 1 3 6 7 8 9 Atomic Absorption 10 11 12 13 14 62 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Each (€) 131 29 80 8 96 66 45 17 68 133 100 158 2 39
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