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Sample Preparation
Product Range
::: Clear Solutions in Sample Preparation
Multiwave PRO
Master of Sample Preparation Methods
4The Multiwave PRO microwave reaction system delivers the sample
preparation solutions you need to obtain excellent trace analysis
results, even with complicated, demanding samples.
4Multiwave PRO masters high temperatures and provides
comprehensive reaction control features.
4Its wide range of accessories allows digestion, leaching, oxygen
combustion, solvent extraction, drying, evaporation, and UV
digestion with one single system.
Features
41500 Watt microwave power, unpulsed controllable
4Decomposition of up to 64 samples simultaneously
4Integrated high-performance cooling system
4Certified safety system
4Simultaneous measurement of pressure and temperature
4Infrared temperature measurement of all vessels
4Comprehensive application library
HPA–S
Unrivaled Performance
The High Pressure Asher HPA–S is the reference instrument for wet
chemical pressure decomposition. The instrument is TÜV certified
and can prepare even the most difficult samples for reliable AAS,
ICP-AES, ICP-MS and voltammetric analysis.
The HPA-S enables the maximum decomposition parameters and
the largest sample weight in hermetically sealed reaction vessels
made of quartz glass or glassy carbon. Uniform heating and exact
temperature control guarantee the highest level of reproducibility.
Features
Decomposition pressure up to 130 bar
Decomposition temperature up to 320 °C
Unlimited decomposition times
Reaction vessels
VolumeMaterial
15 ml
Quartz
50 ml
Quartz
90 ml
Quartz
20 ml
Glassy carbon
Number
14 or 21
7
5
6
Multiwave PRO
Abundantly Clear
Highest
sample throughput
Digestion rotors with up
to 64 vessels eliminate
the bottleneck in sample
preparation while being fast
and easy to operate without
compromising safety.
Simple operation and a comprehensive library of
applications make the Multiwave PRO a powerful tool for
sample preparation.
Integrated cooling
The reaction vessels can be operated at maximum operating
pressure and maximum temperature simultaneously. The
integrated vessel cooling prevents overheating and ensures a
higher sample throughput due to short cooling times.
Vessels
MG5
MF50
Liner material
Glass (PTFE seal)
PFA or PTFE-TFM
MF100
PTFE-TFM
Pressure jacket
n/a
PEEK
PEEK
Vessel volume
5 mL
50 mL
100 mL
Operation parameters
200 °C @ 20 bar (290 psi)
200 °C @ 20 bar (290 psi)
200 °C @
Max. design pressure
33 bar (479 psi)
60 bar (870 psi)
115 bar (16
Max. design temperature
310 °C
260 °C (PFA), 310 °C (TFM)
310 °C
HF resistant
No
Yes
Yes
Typical applications
Biological material
Water, effluents, sewage sludge, plant ma
sediment, US-EPA procedures, biological
Highest
decomposition quality
Operating pressures and
temperatures up to
80 bar and 300 °C result
in matrix-free solutions
without contamination or
loss of analytes, even for
samples which are difficult to
decompose or react violently.
Everything under control
Information about reaction parameters is delivered by installationfree pressure and temperature sensors from a reference vessel.
Continuous pressure monitoring of all eight sample vessels allows
for safe and precise reaction control, even with critical samples.
An external IR sensor monitors the temperature of all reaction
vessels at the base of each vessel.
HF100
XF100
XQ80
PTFE-TFM
PTFE-TFM
n/a
Ceramic
Ceramic
Quartz
100 mL
100 mL
80 mL
20 bar (290 psi)
240 °C @ 40 bar (580 psi)
260 °C @ 60 bar (870 psi)
300 °C @ 80 bar (1160 psi)
670 psi)
115 bar (1670 psi)
140 bar (2000 psi)
140 bar (2000 psi)
310 °C
310 °C
310 °C
Yes
Yes
No
Food samples, contaminated soil, metals, alloys,
geological material, glass,
quartz
Mixed waste, semiconductors, ceramics, ores,
ashes, slag, refractories
Fatty foodstuffs, plastics,
fibers, oil, fat, coal, pharmaceuticals, chemicals
M
aterial, soil,
material
Multiwave PRO
Special Applications
Microwave-assisted extraction
Extraction above the solvent's boiling point for unmatched
speed and safety.
Oxygen combustion
Microwave-induced combustion is a unique option for analysis of
halogenes or metals in combustible samples.
UV digestion
Microwave-powered UV lamps completely destroy organic matter in
liquid samples with little reagent and low analytical blanks.
Hydrolysis
Protein hydrolysis can be performed from milligram to gram scale in
less than one hour, even under inert gas atmosphere.
Evaporation
Acids or silicates are removed under clean room conditions without
changing the reaction vessel.
Drying
Samples are dried prior to digestion quickly and without bad smells.
Multiwave ECO
Routine Digestions - Simple and Quick
Multiwave ECO is a quick and convenient microwave digestion
system equipped with the lightweight Rotor 16HVT50. This rotor
has a superior design for controlled release of overpressure.
Multiwave ECO simplifies your routine handling of environmental,
food and many other samples. The low investment and operating
costs of Multiwave ECO and low costs for consumables make it a
good investment.
Benefits
4ECO heating concept - A smart microwave heating concept
that does more with less
4ECO cooling concept - The fastest cooling of all laboratory
microwaves
4Simplicity - Simplified handling of rotor and vessels
42 turns to tightness - Simple 3-part vessel concept
4Pressure-activated venting - Reliable, temperatureindependent system which handles pressure when the heat is
on - high temperatures and high sample weights
4Rotor 1DRY as an option to dry samples before digestion
4Rotor 16HVT50 for large sample weights up to 2 g organic
samples; Rotor 64MG5 for micro samples
Photos: Croce & Wir
Anton Paar® GmbH
Anton-Paar-Str. 20
A-8054 Graz
Austria - Europe
Tel: +43 (0)316 257-0
Fax: +43 (0)316 257-257
E-mail: [email protected]
Web: www.anton-paar.com
Instruments for:
Density & concentration
measurement
Rheometry & viscometry
Sample Preparation
Microwave synthesis
Colloid science
X-ray structure analysis
Refractometry
Polarimetry
Petroleum testing
High-precision temperature
measurement
Subject to change
without notice
01/13 XCAIP013EN-E