Lubricants Group Ballot Volvo T-13 Group II to Group II Base Oil Interchange Ballot to Establish Volvo T-13 Base Oil Interchange (BOI) for API Group II to API Group II Lubricants Group Members reviewed the recommendation on Volvo T-13 Group II to Group II BOI from the BOI/VGRA Task Force. The data analysis from the PC-11 Volvo T-13 Precision and BOI Test Matrix is attached to this Ballot as Appendix I. After reviewing the Volvo T-13 data the Lubricants Group agreed to ballot Volvo T-13 BOI with Group II to Group II BOI. A draft of the Volvo T-13 BOI Table is given below with the Group II to Group II read across highlighted. E.3.2.5.xxx If only one passing VolvoT-13 test is available on a given technology, Table E-xx applies. Table E-xx—VolvoT-13 Tests Required for Base Oil Interchange Base Stock in Original Test Oil Interchange Base Stock Group I Group II Group III Group IV Group V Group I Required Required Required Required Required Group II Required Not Required Required Required Required Group III Required Required Required Required Required Group IV Required Required Required Required Required Group V Required Required Required Required Required Lubricants Group Members should cast their vote using the API eBallot System. All Votes will be counted and all Comments will be reviewed and considered before the ballot results are final. Non Lubricants Group Members can comment on the ballot using the API eBallot System. All Comments will be reviewed and considered before the ballot results are final. This Ballot will be issued on June 8, 2015 and will close on July 20, 2015. All Ballots and comments must be received by the close date. If approved the Effective Date of the Change to API 1509 will be Monday June 8, 2015. Attachment 1 Attachment 1 Mack T13 Precision / BOI Matrix Data for BOI / VGRA Task Force Jim Rutherford 03/03/2015 Outcome For both • Precision analysis for IR Oxidation Peak Height at EOT, and • Precision analysis for 40° percent viscosity increase from 300 to 360 hours Technology was significant. • Technology 2 was significantly different from the other two technologies. • The other two technologies were not significantly different from each other. Base oil was not significant. © 2015 Chevron Oronite Companies. All rights reserved. 2 Available Data The LTMS dataset had 34 tests. Two were XC (aborted) and rerun from the designed matrix. Three were matrix oils run in nonmatrix stands. There was one repeat with modified filter head. The task force decided to delete three tests (testkeys 103550, 105822, and 104623) from the precision analysis based on operational anomalies leaving 29 tests for analyses. © 2015 Chevron Oronite Companies. All rights reserved. 3 Precision analysis for IR Oxidation Peak Height at EOT o The full model contains effects of technology, base oil, interaction between technology and base oil, laboratory, and stand within laboratory. o The only significant effect in the full model was technology. o The minimum RMSE model that contained technology, base oil and their interaction so that oil targets could be estimated also included laboratory which was marginally significant. o Although one test was flagged as a potential low outlier (testkey 103587), there was no reason found for deleting it. © 2015 Chevron Oronite Companies. All rights reserved. 4 “Best” Model – IR Oxidation Peak Height at 360 hours (EOT) irph Source Model DF Sum of Squares 9 35787.37311 Mean Square F Value Pr > F 3976.37479 25.87 <.0001 19 28 2920.77861 38708.15172 153.72519 R-Square Coeff Var 0.924544 11.65773 Root MSE 12.3986 irph Mean 106.3552 Source BOCode TechCode 1 2 Type III SS 37.21464 26517.64465 2 4 160.94682 1713.43768 Error Corrected Total DF TechCode*BOCode LTMSLAB TechCode BOCode TechCode BOCode LS Mean 142.7 1 1 1 2 2 3 3 2 1 2 1 2 133.5 59.7 59.2 121.1 123.6 1 1 0.837 <.0001 <.0001 0.141 0.225 Mean Square F Value Pr > F 37.21464 0.24 0.628 13258.82233 86.25 <.0001 80.47341 428.35942 0.52 0.601 2.79 0.056 1 2 2 1 2 2 3 1 3 2 0.837 <.0001 <.0001 0.141 0.225 <.0001 <.0001 1.000 0.675 <.0001 <.0001 0.858 <.0001 <.0001 1.000 <.0001 1.000 <.0001 0.675 <.0001 0.858 <.0001 © 2015 Chevron Oronite Companies. All rights reserved. <.0001 <.0001 1.000 5 “Best” Model – IR Oxidation Peak Height at 360 hours (EOT) © 2015 Chevron Oronite Companies. All rights reserved. 6 Precision analysis for 40° percent viscosity increase from 300 to 360 hours o The full model contains effects of technology, base oil, interaction between technology and base oil, laboratory, and stand within laboratory. o The only significant effect in the full model was technology. o The minimum RMSE model that contained technology, base oil and their interaction so that oil targets could be estimated also included laboratory. o Although one test was flagged as a potential high outlier (testkey 103423), there was no reason found for deleting it. © 2015 Chevron Oronite Companies. All rights reserved. 7 “Best” Model – Viscosity at 40°C percent increase from 300 to 360 hours v40pcd300to360 Source Model Error Corrected Total DF Sum of Squares 9 24822.3637 19 10231.5639 28 35053.9276 R-Square Coeff Var 0.708119 37.68694 Source BOCode TechCode TechCode*BOCode LTMSLAB DF 1 2 2 4 TechCode TechCode BOCode BOCode 86.9 1 1 77.6 1 2 25.2 2 1 23.2 2 2 68.8 3 1 87.1 3 2 Mean Square F Value Pr > F 2758.04041 5.12 0.001 538.50336 Root MSE v40pcd300to360 Mean 23.20568 61.57485 Type III SS 35.09333 15655.48953 779.60148 3405.21283 1 1 1 2 0.986 0.986 0.022 0.002 0.844 1 0.084 0.011 0.992 0.991 © 2015 Chevron Oronite Companies. All rights reserved. Mean Square F Value Pr > F 35.09333 0.07 0.801 7827.74476 14.54 1E-04 389.80074 0.72 0.498 851.30321 1.58 0.22 2 1 0.022 0.084 2 2 0.002 0.011 1 1 0.2274 0.037 0.0574 0.0062 8 3 1 0.844 0.992 0.227 0.057 0.894 3 2 1 0.991 0.037 0.006 0.894 “Best” Model – Viscosity at 40°C percent increase from 300 to 360 hours © 2015 Chevron Oronite Companies. All rights reserved. 9
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