Virgin Plum Oil ◦ ι 2 Integrity Ingredients Corporation IntegriLIPID “French” Plum Oil ◦ ι Integrity Ingredients Corporation 2 IntegriLIPID “French” Plum Oil An Oleic oil with high linoleic acid content, rich in anti-oxidant tocopherols. INCI: Prunus Domestica Seed Oil Properties: Non Greasy feel on skin Emollient Oil Anti Radical Properties (Tocopherols) Proven innocuity by in-vivo and intro tolerance tests Natural bitter almond-like fragrance (interesting when formulating hypoallergenic products without synthetic fragrances). Applications: General Skin Care Hair Care . ◦ ι Integrity Ingredients Corporation 2 TECHNICAL PROFILE SUMMARY 1. Composition: IntegriLIPID “French” Plum Oil displays the following characteristics. 1.1 General characteristics of IntegriLIPID “French” Plum Oil Criteria Aspect Flavor Color Specification Analytical Method Fluid at ambient temperature Flavor and aroma more or less intense, characteristic of bitter almond Visual Observation Golden yellow Visual Observation Tasting 1.2 Physical characteristics of IntegriLIPID “French” Plum Oil Criteria Density at 20°C Refractive Value at 20° C Cold Test Result Analytical Method 0.910 – 0.920 NF ISO 6883 1.4640 – 1.4730 NF ISO 6320 Absence of trouble after 5H30 at 0° C (filtered Oil) AOCS 11-53 2.Chemical Characteristics and Fatty Acid Profile IntegriLIPID “French” Plum Oil is rich in unsaturated fatty acids. It contains from 60% to 80% of Oleic Acid C18:1. The most prevalent triglycerides are trioleine (40% to 50% of total) and di-oleolinoleine (20% to 40% of total triglycerides). 2.1 General chemical characteristics of IntegriLIPID “French” Plum Oil Criteria . Value Analytical Method Iodine Value 90 – 120 NF ISO 3961 Saponification Value 170 - 210 NF ISO 3657 ◦ ι 2 Integrity Ingredients Corporation 2.2 Fatty acid compositions Fatty acid Chemical Symbol Average value Value Range C14 < 0.1 < 0.1 C16 C16:1 C17 C17:1 C18 < 5.0 <1 0.1 < 0.1 1.5 4-9 <1 0.1 < 0.1 0.5 – 3.0 C18:1 (Omega 9) C18:2 (Omega 6) C18:3 (Omega 3) C20 C20:1 C22 C24 68.0 23.0 0.1 0.2 0.1 < 0.1 < 0.1 60 – 80 15 - 25 <1 < 0.3 0.2 < 0.1 < 0.1 Myristic acid Palmitic acid Palmitoleic acid Margeric acid Heptadecenoic acid Stearic acid Oleic acid Linoleic acid Linolenic acid Arachidic acid Gondoic acid Behenic acid Lignoceric acid 2.2 Fatty acid group composition Fatty acid composition % Average Value Value range 7 5 – 10 70 23 < 0.1 65 – 80 15 – 25 < 0.1 Total saturated Total mono-unsaturated Total poly-unsaturated Total Isomer trans-fat Analytical method NF ISO 5508 and ISO 5509 Criteria Non saponifiable matters Value Average value 0.5 – 1% < 0.1 C16 C16:1 C17 < 5.0 <1 0.1 Palmitic acid Palmitoleic acid Margeric acid Analytical methol AFNOR NF T 60 - 25 . ◦ ι Integrity Ingredients Corporation 2 3. Sterols 3.1 Sterol composition Sterol Composition % Average Value Range Value Cholesterol 0.3 0.1 - 1 24-methylen-cholesterol Campesterol 0.6 4.5 <1 4.5 – 5 Campestanol Stigmasterol Clérosterol Beta-sitosterol Sitostanol Delta5-avenasterol Delta5, 24-stigmastadienol Delta7-avenasterol Non identified 0.3 0.7 0.9 81.5 1.5 7.5 0.6 1.2 0.1 <1 0.5 – 1 0.5 – 1 83 – 88 1-2 5–9 <1 1–2 <1 Analytical method NF ISO 6799 4. Total sterol content of IntegriLIPID “French” Plum Oil Criteria Total Sterol Content Analytical method NF ISO 6799 . Average Value Range Value 0.4 % 0.2 – 1% ◦ ι 2 Integrity Ingredients Corporation 5. Tocopherols 5.1 Tocopherol composition Tocopherol composition % Average Value Range Value Alpha-tocopherol 11 8 - 15 Beta-tocopherol Gama-tocopherol Delta-tocopherol < 0.1 84 5 < 0.1 80 - 90 3-8 Analytical methold IUPAC of ISO 9936 5.2 Tocopherol content of IntegriLIPID “French” Plum Oil Tocopherol content (ppm) Average Value Range Value Alpha-tocopherol 90 80 - 100 Beta-tocopherol Gama-tocopherol Delta-tocopherol Total <5 700 45 840 <5 600 - 750 30 – 50 700 - 900 Analytical method IUPAC 2.432 or ISO 9936 6. Oxidation and Oxidative Stability 6.1 Oxidation values Criteria Value (time of manufacturing) Peroxide value (Meq O2/kg) < 10 6.2 Oxidative Stability . Criteria Value Analytical Method Rancimat test (98° C) Peroxide value after 14 weeks at ambient temperature and under light Peroxide value after 14 weeks in cold storage at +6°C > 30 hours NF ISO 6886 < 20 Meq O2/kg AFNOR NF T 60-220 < 20 Meq O2/kg AFNOR NF T 60-220 ◦ ι Integrity Ingredients Corporation 2 6.3 Acid hydrolosis Criteria Value Oleic acidity 1% Acid value <2 7. External Contaminants 7.1 Solvents IntegriLIPID “French” Plum Oil is pressed by mechanical means. No organic solvent is in contact with the oil either during the production process or during storage. 7.2 Pesticides Type of Pesticides Value Organo-chlorine (19 components tested) Not detected Organo-phosphate (16 components tested) Not detected 7.3 Other external contaminants Criteria Water Impurities Soap Iron Copper . Value Analytical Method < 0.2 % NF ISO 662 < 0.05 % < 0.005 % < 5 ppm < 0.4 ppm NF ISO 663 AFNOR NF T60-217 NF ISO 8294 NF ISO 8294 ◦ ι Integrity Ingredients Corporation 2 8. Raw Material Origin & Safety Only kernels from non genetically modified plums grown in the South-West of France are used. The kernels are collected then washed and carefully dried under controlled atmosphere (60° C maximum) to prevent any microbial propagation before processing. The kernels are then crushed mechanically (no solvent is used). IntegriLIPID “French” Plum Oil offers the following guarantees: . All solid particles and non lipolhiles components (sugar, proteins, shell) are eliminated during the different processing steps. IntegriLIPID “French” Plum Oil contains less than 0.2% of water IntegriLIPID “French” Plum Oil contains less than 0.05% of solid impurities IntegriLIPID “French” Plum Oil is stocked, protected from air, light and heat in non humid containers Technical analysis confirmed the absence of such contaminants as Coliforms (at 30° C), Solmonels, E. coli or Aerobic Mesophilic Germs ◦ ι 2 Integrity Ingredients Corporation ADDENDUM 1 Presence of allergenic agents Allergenic Agents Content Unit 2-benzylidene heptanal <1 Amylcinnamyl alcohol Benzyl alcohol <1 94 mg/Kg mg/Kg mg/Kg Benzyl salicylate Cynnamyl alcohol Cinnamaldehyde Citral Coumarin Eugenol Geraniol 7-hydroxycitronellal Lyral <1 <1 9 <1 <1 <1 <1 <1 <1 <1 mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg <1 <1 <1 <1 <1 <1 <1 <1 <1 mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg <1 <1 mg/Kg mg/Kg mg/Kg mg/Kg Isoeugenol Alcohol 4-methoxybenzyl Benzyl benzoate Benzyl cinnamate Citronellol Farnesol Hexylcinnamaldehyde Lilial D-limonene Linalol Oct-2-enoate methyl Cetone Alpha Evernia prunastri Evernia furfuracea . Not detected Not detected ◦ ι 2 Integrity Ingredients Corporation Midwest Office Northwest Office Contact: Nathan Reighard Email: nreighard@ integrityingredientscorp.com Phone (803)743-8989 Fax (310)782-0283 East Coast Office Coming Soon….. Contact: Connie Wightman Email: cwightman@ integrityingredientscorp.com Phone (951)867-1584 Fax (310)782-0283 West Coast Office Contacts: South East Office South Central Office Melody Howell Email: mhowell@ Contact: Sandy Bush Sonata Technologies LLC Email: integrityingredientscorp.com Maria Reighard Email: mreighard@ Contact: Joy Roederer PhD [email protected] Phone (951)553-4175 Fax (310)782-0283 Email: [email protected] Phone (214)674-0026 integrityingredientscorp.com Contact: Larry Murphy Email: [email protected] Phone (972)369-4538 Fax (310)782-0283 ι South East Office South Central Office Phone (310)782-0282 Fax (310)782-0283 Contact: Rodney Grau Email: [email protected] Phone (602)350-6723 Fax (310)782-0283 For Technical and Sales Support contact: Lee Paler David Howell Technical and Regulatory Sales and Marketing Phone (310)782-0282 Email: [email protected] Phone (951)867-0329 Email: [email protected] Integrity Ingredients Corporation * P.O. Box 5040 * Playa del Rey, CA 90296 Phone (310)782-0282 * Fax (310)782-0283 * Toll Free (877)765-0282 email [email protected] * Web www.integrityingredientscorp.com .
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