Microelectronic Engineering 70 (2003) 102–108 www.elsevier.com / locate / mee Performance-enhanced Fabry–Perot microcavity structure with a novel non-planar diaphragm a, a a a b W.J. Wang *, R.M. Lin , T.T. Sun , D.G. Guo , Y. Ren a Centre for Mechanics of Micro-Systems, School of Mechanical & Production Engineering, Nanyang Technological University, 50 Nanyang Avenue, Singapore, 639798, Singapore b Tissue Engineering Lab, School of Mechanical & Production Engineering, Nanyang Technological University, 50 Nanyang Avenue, Singapore, 639798, Singapore Received 31 March 2003; received in revised form 7 May 2003; accepted 27 May 2003 Abstract A new Fabry–Perot (FP) microcavity structure with a novel, single and deeply corrugated diaphragm (SDCD) is presented for use as a pressure-sensing element. Both the zero-pressure offset due to the non-planar diaphragm structure and the signal averaging effect caused by the non-planar deflection of the diaphragm in response to an external pressure load are studied. The FP microcavity was fabricated on a single-chip using both surface and bulk micromachining techniques. The theoretical analyses as well as the measurements have shown that the signal-averaging effect can substantially be reduced for the proposed FP microcavity pressure sensor by using the flatness-enhancing diaphragm structure. 2003 Elsevier B.V. All rights reserved. Keywords: Fabry–Perot; Pressure sensor; Corrugated diaphragm 1. Introduction Optical metrology offers particular advantages in remote sensing and has been suggested as a valuable alternative to commercially available piezoresistive and capacitive sensing techniques for devices operable in harsh environments where electronics cannot operate. Of the various optical sensing techniques available, Fabry–Perot (FP) interferometery shows considerable promise in terms of high sensitivity, versatility and immunity to environmental noise. An *Corresponding author. Tel.: 165-790-4051; fax: 165-7911975. E-mail address: [email protected] (W.J. Wang). FP interferometer is an optical element consisting of two partially reflecting, low-loss, parallel mirrors separated by a gap. Since the reflectance or transmittance of the FP cavity is a function of both the gap spacing and the wavelength, the FP cavity can be realized as a sensor of either parameter. Microelectromechanical systems (MEMS) technology is effective for manufacturing of these sensors since considerable flexibility in choosing measurand response ranges, bandwidth and sensitivity can be achieved with the small and precise size of sensing elements. FP microcavity based sensors, such as pressure sensors, temperature sensors and chemical sensors [1–4] have been fabricated using micromachining techniques. Recent advances in 0167-9317 / 03 / $ – see front matter 2003 Elsevier B.V. All rights reserved. doi:10.1016 / S0167-9317(03)00399-X W. J. Wang et al. / Microelectronic Engineering 70 (2003) 102–108 silicon micromachining techniques have made optical sensing devices more feasible for commercialization by reducing sizes and improving performance and manufacturability. One of the major obstacles to commercialization of the micromachined FP cavity pressure sensors is the degradation of device performance arising from non-planar deflection of an edge-clamped diaphragm / mirror when subjected to an external pressure load. Two alternative techniques have been proposed to date to address the issue [4]. One technique towards minimizing the non-planarity of the deflecting mirror is to maximize the area ratio of the moving mirror to the stationary one. Another alternative flatness-enhancing technique is to form corrugations in the deflecting diaphragm. Unfortunately, due to the restrictions stemming from either the configurations of the FP microcavity or the process technology, the effect on enhancing the flatness of the diaphragm is significantly limited to date. It has been well established from our previous studies that compared to the conventional flat diaphragm and shallowly corrugated diaphragm of comparable size and thickness, significantly higher sensitivity can be achieved with the single deeply corrugated diaphragm (SDCD) by both partly releasing the initial stress and reducing the mechanical stiffness of the diaphragm simultaneously [5]. In this study, the SDCD structure will be extended into the development of a novel FP microcavity. Both analysis and finite element model (FEM) simulation have shown that the flatness-enhancing effect can be achieved with the SDCD structure, and therefore the signal averaging effect can substantially be reduced for the SDCD FP microcavity pressure sensor. 2. Design and simulation of the proposed FP microcavity The proposed FP microcavity sensing element, as shown in Fig. 1, consists of three major components: a SDCD structure consists of flexible suspending sidewalls and a flat bottom-region that serves as the moving mirror; a bottom diaphragm that serves as the stationary mirror; and an air gap between the moving and stationary mirrors of the FP microcavity. The FP microcavity pressure-sensing element is 103 Fig. 1. Three-dimensional schematic with cross-section (a); and bottom-side view (b) of the proposed SDCD FP microcavity pressure-sensing element. expected to operate at wavelengths greater than 1.15 mm, where the silicon substrate is highly transparent. The unique feature of this design is that it employs the flexible suspending sidewalls serving as the stress concentrator and buffer for the moving mirror to enhance the flatness of the diaphragm in response to external pressure load, where its whole sensing area is at the bottom of the corrugation. While similar optical characteristics may be achieved for the FP microcavity with conventional flat diaphragm provided that the diaphragm is large enough compared with optical beam size, the proposed SDCD FP 104 W. J. Wang et al. / Microelectronic Engineering 70 (2003) 102–108 microcavity offers significant advantage in terms of small size and dense arrays. The SDCD structure consists of a 0.5-mm-thick low-stress silicon nitride (Si x N y ) layer sandwiched between two 0.5-mm-thick polysilicon cladding layers. The thickness of each layer in the composite diaphragm was chosen mainly to satisfy the mechanical constraints such as low tensile residual stress and suitable mechanical compliance with the size of the flat bottom-region of the SDCD structure being chosen as 200 mm. The stationary mirror comprises also three layers of polysilicon, Si x N y and silicon substrate. The 200nm-thick Si x N y and 350-nm-thick polysilicon layers are used to fine-tune the total reflectance of the FP microcavity. It should be mentioned that finesse is a measure of the sharpness of the transmission peaks. From the sensing elements perspective, the use of mirrors possessing moderately low reflectance, r, i.e., a low finesse FP cavity, is more suitable since the total reflectance of the FP cavity would become broad and almost sinusoidal in shape for moderately small r, values while larger r values will cause the reflectance to have a sharp peak and little variation over the air gap variation of interest, and too small an r value will cause the reflectance vary in a small range over the air gap variation. The initial air gap (i.e., a gap at an applied pressure load of zero) of the FP microcavity was selected as 1.6 mm to obtain a linear response over the desired pressure range and to minimize the measurement tolerance arising from the layer thickness variation induced by the fabrication process. FP microcavity with a large gap (for example, .5 mm) has a multi-cycle operation and thus relies on fringe counting techniques for the determination of the measurand [6]. Short-gap FP microcavity has a spectral width comparable to a single fringe so that any shifts of the resonance peak can directly be related to the magnitude of the parameter of interest. Short-gap type FP microcavity is, therefore, used in this study because of its compatibility with a simpler detection scheme as opposed to the cumbersome and ambiguous fringe counting circuits associated with a large-gap FP microcavity. The signal averaging effect is referred to as a pressure-dependent degradation of optical response which arises because the negative intensity values can cancel out with the positive values due to the sinusoidal nature of the optical response reflected from or transmitted through a FP microcavity, leading to an averaged optical response from different positions of the non-uniformly deflected diaphragm. For this reason, the actually detected optical response may be lower than the expected value from the FP microcativity with an idealized piston-like diaphragm, and the degradation increases with increasing the degree of the curvature of a deflecting diaphragm in a FP microcavity. To simulate the actual optical response, the shape of the deflected diaphragm should first be determined. FEM was employed to simulate the shape of the proposed SDCD structure. For comparison, the conventional flat diaphragm was also involved in the simulation. We simulated both the square flat diaphragm of 2003200 mm 2 in area and 1.5 mm in thickness, as well as the SDCD of identical bottom area and thickness with a corrugation depth of 40 mm. The pre-stressed diaphragms were modeled using a threedimensional shell element (element Shell 63 in ANSYS 5.6). The initial stress was induced in the diaphragms by using the equivalent cooling temperature method as proposed by Zhang and Wise [7]. Fig. 2 shows the comparison of the FEM simulated deflections along the moving mirror between the conventional flat diaphragm and the SDCD structure under a l-kPa pressure load, in which the point at 0 mm corresponds to the center of the mirror having the maxmal deflection, and the deflection at each point is normalized with respect to the maximal Fig. 2. The deflection along movable mirror for an applied pressure of 1 kPa, in which the point at 0 mm corresponds to the center of the moving mirror, and the deflection at each point is normalized with respect to the maximal deflection at the center of the mirror. W. J. Wang et al. / Microelectronic Engineering 70 (2003) 102–108 deflection at the center of the mirror. It is evident from Fig. 2 that the degree of flatness of the moving mirror subjected to external pressure load has substantially been enhanced by the SDCD when compared to the conventional flat diaphragm. Since the variation in the amount of deflection over the moving mirror can be reduced by the suspending sidewalls, we propose that the pressure-dependent degradation of the optical response (i.e., the signal averaging effect), can be significantly reduced for the FP microcavity based pressure sensor. Following the determination of the shape of the deflecting diaphragm, the weighted average response was calculated from [8] O f R( g) ? A( g) g R avg 5 ]]]]] A( g) O (1) where R( g) is the reflectance of the FP microcavity at gap g and A( g) is the area with gap g. The reflectance of the FP microcavity of a given gap distance was calculated using the characteristic matrix method [9]: S h0 B 2 C R 5 ]]] h0 B 2 C DS D h0 B 2 C * ]]] h0 B 2 C (2) where * denotes complex conjugate, and B q 3 4 1P 3 3 4 C 5 i 51 cos(ko n i z i ) j ] sin(ko n i z i ) hi jhi sin(ko n i z i ) cos(ko n i z i ) 42 1 hm (3) where hm and h0 are the admittance of the environment outside the FP microcavity and of the medium from which the light comes, respectively; k 0 5 2p /l; n i and z i are the refractive index and thickness of the ith layer, respectively. Fig. 3 shows the simulated reflectance as a function of mechanical displacement at the center of the diaphragm for FP microcavity with the conventional flat diaphragm and the proposed SDCD structure with a corrugation depth of 40 mm in comparison with an idealized piston-like diaphragm. It can be seen from Fig. 3 that compared with the idealized piston-like diaphragm, degradation is present in the 105 Fig. 3. Evaluation of signal averaging effect of the FP microcavity with a conventional flat diaphragm and the proposed SDCD structure in comparison with an idealized piston-like diaphragm. reflectance of the FP microcavity with the actual bowed flat diaphragm. It is evident that the reflectance of the FP microcavity with the flat diaphragm does not have a period of one half the illumination wavelength of 1310 nm, demonstrating the signal averaging effect caused by the non-uniform deflection of the deflected diaphragm. However, it can clearly be seen that using the SDCD structure as the moving mirror of the FP microcavity can substantially reduce the signal averaging effect. The substantial reduction in the signal averaging effect is believed to be attributed to the flexible suspending sidewalls that act as a stress concentrator and buffer for the moving mirror (i.e., the flat-bottomed region of the SDCD structure), partly change their own shapes rather than the one of the entire diaphragm when absorbing the external pressure load, thereby enhancing the degree of flatness of the moving mirror in response to an applied pressure load. On the other hand, simulations performed using FEM have shown that the SDCD structures having internal stress exhibit a central deflection under zero applied pressure (i.e., a zero-pressure offset). This phenomenon is not observed in conventional flat diaphragm structures having internal stress, which remain flat under zero applied pressure. It should be pointed out that the zero-pressure offset is different from buckling, which occurs only in case of compressive stress and only if the compressive stress has exceeded a critical value [10]. The direction and shape of a buckled diaphragm cannot be exactly predicted. However, the zero-pressure offset direc- 106 W. J. Wang et al. / Microelectronic Engineering 70 (2003) 102–108 Fig. 4. FEM simulated zero-pressure offset versus corrugation depth for different initial stress. tion and magnitude of the non-planar diaphragm can, in principle, be predicted if the dimensions and the stress are known [10]. It has been established that the offset direction of the SDCD structure is dependent on whether the initial stress is compressive or tensile, while the offset magnitude is a function of diaphragm stress level and diaphragm geometry [5]. Fig. 4 shows the magnitude of zero-pressure offset of the diaphragm versus the initial stress. It can be seen from Fig. 4 that the higher the internal stress level, the larger the zero-pressure offset. An interesting phenomenon is that, for a specific initial stress level, a larger zero-pressure offset is observed at the extremes of the corrugation depth range with a minimum value in mid range. This is because the four sidewalls at a smaller corrugation depth are more rigid as compared to those of a larger corrugation depth. Thus, the relaxation of the diaphragm structure is more difficult when it is being released. For a large corrugation depth, however, the SDCD structure has become more flexible, which makes it more vulnerable at high initial stress. As for the offset direction, the observed zero-pressure deflections were in the direction of bending down from the substrate for the low tensile stress composite diaphragms in this study, which is consistent with the FEM simulation results. 3. Fabrication and characterizations As shown in Fig. 5, the proposed FP sensing Fig. 5. Process flow of the proposed FP microcavity. element is fabricated using both surface and bulk micromachining techniques. The process starts with a double-sided polished n-type silicon (100) wafer upon which a masking layer of silicon nitride, as shown in Fig. 5a, was formed by low-pressure chemical vapor deposition (LPCVD). After the masking layer was patterned on the front-side of the wafer, a deep cavity was etched with 40% aqueous KOH at 60 8C (50-mm thick silicon was remained) (Fig. 5b). The masking layer of silicon nitride was then removed using hot H 3 PO 4 . Low-stress silicon nitride and polysilicon were then formed by LPCVD successively, followed by deposition of phosphosilicate glass (PSG) of 1.6 mm serving as the sacrificial layer. A reflow of the PSG was carried out at a temperature of 850 8C for 1 h to eliminate the effect W. J. Wang et al. / Microelectronic Engineering 70 (2003) 102–108 of stress concentration at sharp corners. A trilayer of 0.5 mm of polysilicon, 0.5 mm of low-stress silicon nitride, and again 0.5 mm of polysilicon, were deposited successively by LPCVD. The resultant tensile residual stresses of the stacked layers of the diaphragms were measured as 70 MPa. The stress of the film at every process stage was obtained by measuring a dummy wafer using a curvature-based film-stress meter. The polysilicon / Si x N y / polysilicon sandwich, the sacrificial PSG layer, as well as the polysilicon and the low-stress silicon nitride layers at the back-side of the wafer were then removed, followed by the creation of access holes using deep reactive ion etching with photoresist as its masking layer (Fig. 5c). The diaphragm was then released in the 40% HF solution (Fig. 5d). Sequential replacement of acetone and methanol was carefully processed to protect the diaphragm from sticking. Fig. 6 shows the SEM micrograph of the fabricated SDCD FP microcavity. The wavelength-dependent transmittance of the FP microcavity was measured without any external pressure load. The measurements combined with the simulated results are shown in Fig. 7. Included in the simulation is the variation of the refractive index of each film as a function of wavelength, using the data from [11]. The zero-pressure offset of approximately 40 nm responsible for the phase shift of the optical response is considered, as well. It can be seen from Fig. 7 that reasonable agreement was obtained Fig. 6. SEM micrograph of the fabricated FP microcavity; (a) the top view and (b) the bottom-corner region. 107 Fig. 7. Simulated and measured transmittance of the FP microcavity versus wavelength; solid line: simulated response; dotted line: measured response. between the measured and simulated transmittance, indicating the layer thickness and indices of refraction used in the calculation were correct, and the structure proposed in this study is feasible to be realized as a pressure sensor. An applied pressure deflects the diaphragms and changes the optical path length of the cavity, which is sensed by the change in the intensity of the light reflected from the FP microcavity. Since there are access holes in the bottom diaphragm, when a pressure differential exists, it is actually the top diaphragm that is deflected. The prototype pressure sensor has been tested under static pressure. The experimental setup is sketched in Fig. 8. As shown in Fig. 8, a laser was routed to the one end of the input ports of the 232 coupler. The reflected light was measured from the other end of input ports. One end of output ports is connected to the FP microcavity. Fig. 8. Schematic view of the optical measurement set-up. 108 W. J. Wang et al. / Microelectronic Engineering 70 (2003) 102–108 a novel SDCD structure as a moving mirror has been designed, fabricated and characterized. The device performances were evaluated by both theoretical analysis and measurements. Results show that the signal averaging effect was substantially reduced for the SDCD FP pressure sensor by the flatness-enhancing diaphragm structure. The initial testing of the FP microcavity has shown encouraging results. Since the proposed FP microcavity is significantly miniaturized, they will find applications to advantage small size and dense arrays, which play an important role in medical applications. Fig. 9. Simulated and measured reflectance as a function of differential pressure. Fig. 9 shows the simulated and measured optical reflectance of the SDCD FP pressure sensor. In the simulation of the proposed SDCD FP pressure sensor, the residual stress of 70 Mpa is assumed to be present in the SDCD with corrugation depth of 40 mm, according to the previous measurements. Both zero-pressure offset and signal averaging effect were included in the simulation. It can be seen from Fig. 9 that the experiments show good consistence with the calculations. The maximum sensitivity is obtained over the pressures ranging from about 10 to 25 psi at the wavelength l 5 1310nm, which can be tailored to a particular range of pressures according to the specific requirements of applications by tuning the laser wavelength. It is noticed from Fig. 9 that at wavelength l 5 1320nm, the response curve shifts along the horizontal axis of Fig. 9, resulting in the maximum sensitivity over the pressures ranging from 12 to 27 psi. The validity of the extracted deflection distance from the reflectance plot in Fig. 9 is evaluated by comparing with the measured deflection distance. The measured deflection distance of the SDCD mirror, 0.63 mm, is comparable with the one peak-to-peak period of the reflectance, 0.655 mm, demonstrating the SDCD FP microcavity is promising in realization as a pressure sensor. 4. Conclusions In this work, a new FP microcavity structure with References [1] Y. Kim, D.P. Neikirk, Micromachined Fabry–Perot cavity pressure transducer, IEEE Photonics Technol. Lett. 7 (12) (1995) 1471–1473. [2] D.C. Abeysinghe, S. Dasgupta, J.T. Boyd, H.E. Jackson, A novel MEMS pressure sensor fabricated on an optical fiber, IEEE Photonics Technol. Lett. 13 (9) (2001) 993–995. [3] J. Han, Fabry–Perot cavity chemical sensors by silicon micromachining techniques, Appl. Phys. Lett. 74 (3) (1999) 445–447. [4] J. Han, J.Y. Kim, T.S. Kim, J.S. Kim, Performance of Fabry–Perot microcavity structures with corrugated diaphragms, Sensor. Actuat. A79 (2000) 162–172. [5] W.J. Wang, R.M. Lin, Study of single deeply corrugated diaphragm for high sensitivity microphones, J. 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