Glass Thermometers: A Degree of History E ver since the early 1600s, when Galileo invented the first crude instrument, called a thermoscope, to show changes in temperature, the thermometer has evolved to become a crucial instrument for determining temperature in a multitude of laboratory and industrial applications. The earliest thermometers, considered a curiosity by many people, were used for medical and meteorological purposes and shared basic features. All were glass tubes open at one end, partially filled with air, set in a basin of water and graduated with primitive notches or dials. It wasn't until 50 years later that the first closed-glass liquid thermometer was developed in Italy by Leopoldo, Cardinal dei Medici, a co-founder of the Academia de Cimento. Known as Florentine thermometers, they were graduated into 50, 100 or 300 degrees and roughly standardized by the heat of the sun and the cold of ice water, and filled with distilled colored wine. Mercury and water thermometers were also tried by the Florentines but their expansion was too small. This problem was later overcome by making thermometers with finer bores, thereby increasing their sensitivity. By the middle of the eighteenth century, mercury thermometers had superseded all others because of their more uniform expansion. Today the glass thermometer is available in a variety of calibrations, immersion styles, versions, lengths, divisions and backings and in °F and °C versions with columns filled with mercury or safety liquid. Lodged as a staple in laboratories and industries worldwide, the glass thermometer is an enduring symbol for the advancement of knowledge. MEGA introduces its new line of glass thermometers for laboratory and industrial applications. Accurate, economical instruments, glass thermometers measure the temperature of many fluid types–liquid or gas. OMEGA offers precision ASTM-designated thermometers in accordance with strict performance specifications. Immersion Styles O Care and Use of Glass Thermometers Glass thermometers must be handled with care. Avoid tapping a glass thermometer against a hard surface to prevent small fractures, which could affect accuracy. A glass thermometer should never be subjected to extreme temperature changes. For example, removing a glass thermometer from a boiling water bath and immediately immersing it in an ice bath may cause the thermometer to break or the liquid filling to separate. With proper care, a glass thermometer can be a useful instrument for years. Column Separation Occasionally, a thermometer arrives with a separation of the mercury column due to rough handling in transit. A column will reunite if: 1) the bulb is cooled in brine/ice solution, or 2) the bulb is cooled in an alcohol/dry ice solution, or 3) the separation is slowly heated into the expansion chamber. A total immersion thermometer is designed to indicate temperatures correctly when the bulb and the entire liquid column are immersed in the substance being measured. A minimal length of the thermometer must be visible. A partial immersion thermometer has a line around it indicating maximum immersion depth. For maximum accuracy, select the proper thermometer. A total immersion style offers the best accuracy when used properly. A partial immersion style is appropriate for use when immersion depth is limited. When used correctly, either type will yield reliable results. A total immersion thermometer can be used accurately at partial immersion if the following correction is applied: (T-t) 0.000089°F x N (T-t) 0.00016°C x N T = temperature of the bath t = average temperature of stem N = number of degrees emergent CAUTION Mercury sealed in a thermometer is not dangerous. However, if the thermometer is broken, the mercury metal or vapor may be hazardous to health or materials. Parts of a Glass Thermometer Bulb – reservoir for the thermometric liquid. Stem – glass capillary tube through which the mercury or organic liquid fluctuates with changes in temperature. Scale – the scale is graduated in degrees, fractions or multiples of degrees. Contraction Chamber– an enlarged capillary bore which serves to reduce a long length of capillary, or prevent contraction of the entire liquid column into the bulb. Expansion Chamber– an enlargement of the capillary bore at the top of the thermometer to prevent buildup of excessive pressures in gas-filled thermometers. Partial Immersion Style Immersion Line Bulb Stem Scale Total Immersion Style E-3 Glass Thermometer Options Any encapsulation will increase lag time, but OMEGA® encapsulation does not affect the accuracy of even precision thermometers. Price for Teflon encapsulation ranges from $9. NIST Calibration Available for ASTM and Precision Styles An optional factory certificate is available that will show the corrections of a thermometer stated to one-tenth of one scale division as tested against our National Institute of Standards and Technology (NIST) certified thermometers, and will reference the NIST test number involved. You may specify the test points to be taken. The charge is $70 per test point. Thermometers may be calibrated over the temperature range of -112 to 572°F (-80 to 300°C). To Order: Add suffix "-E" to model number and the appropriate amount to price of thermometer: to 6" length, $9; 6-12" length, $11; 13 to 18" length, $13; 19 to 24" length $16. Ordering Example: GT-6452W-E is a 6" total immersion style, white back, mercury-filled laboratory thermometer, 30 to 125°F range ($17) with optional Teflon® encapsulation ($9). Total price = $17 + 9 = $26. ASTM Thermometers Page E-5 to 12 Meets Accuracy Tolerance and Dimensional Specifications for American Society of Testing Materials (ASTM) Ordering Example: ASTM-44F-NC (68°F, 70°F) is a 12" total immersion style, kinematic viscosity thermometer, 66.5 to 71.5°F range ($90), calibrated at 68°F and 70°F ($70 per point, or $140).Total price = $90 + 70 +70 = $230. CERTIFICATE OF CONFORMANCE E Contents To Order: Add the suffix "-NC" to the model number and $70 per calibration point to the price of the thermometer. Indicate the calibration point(s) in parentheses following the part number. Certificate of Conformance Available for ASTM, Laboratory and Precision Styles Laboratory Thermometers A factory Certificate of Conformance will show accuracy tolerance of a specific type of liquid-in-glass thermometer according to NBS Monograph 150, state conformance to it as tested against our NIST-certified thermometers, and reference the NIST number involved. The charge is $40 per thermometer. To Order: Add suffix "-CC" to model number and $40 to the price of the thermometer. E-13 to 18 White Back, Yellow Back, Red Magnified Mercury and Red Safety Liquid-Filled Precision °F & °C Thermometers E-19 to 22 Yellow Back and Red Magnified Mercury Make for Superior Visibility Ordering Example: GT-1544Y-CC is a total immersion style, yellow back, precision thermometer, -2 to 52°C range ($35) with optional factory Certificate of Conformance ($40). Total price = $35 + 40 = $75. Low Cost Thermometers TEFLON® E-23 to 24 Economical, General Purpose, Ideal For Frequent Purchases Teflon Encapsulation Available for Laboratory and Precision Styles ® Laboratory and precision style OMEGA® thermometers may be ordered encapsulated in transparent PFA Teflon® for use wherever freedom from contamination must be assured. The entire thermometer is sealed permanently in a coating which permits use in corrosive chemicals or acids up to 435°F (225°C) and prevents contamination if breakage does occur. Accessories Clip-on Magnifier, Handheld Lens, Protective Metal Sheath and Mercury Spill Kit Expansion Chamber E-4 E-25
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