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Product Specifications
Thermo Scientific
Sample Collection and
Preparation Tools for
Exploration and Mining
Thermo Scientific sample collection and
preparation tools deliver a full lab-to-field
solution for on-site XRF analysis in
exploration and mining. These compact,
portable, battery-powered tools provide
everything required to deal with dry
geological material for rapid elemental
analysis in the field. The tools complement
Thermo Scientific portable XRF analyzers,
generating high-quality analytical data
within minutes, rather than days or weeks.
Everything You Need
More than 30,000 Thermo Scientific portable
x-ray fluorescence (XRF) analyzers are at
work around the world, making our customers
more efficient and competitive. Over many
years, these analyzers have proven their
performance in the field on hundreds of
thousands of geological samples. In fact, the
analytical performance using our latest
handheld and field-portable analyzers is now
so good that we realize that the key limiting
factor to receiving lab-quality results is
adequate sample preparation – especially
for the XRF analysis of elements lighter
than calcium.
The new Thermo Scientific sample collection
and preparation tool kits make it easy and
quick to set up a full laboratory in the field.
These small, lightweight, unique tool sets are
ideal for transportation to remote locations
with minimal facilities. The analytical
performance of XRF analysis on geological
materials is significantly improved by
collecting representative aliquots and proper
preparation of the sample. Material with a
particle size range of 100μm and below,
which are necessary for high-performance
lab-quality XRF analysis, cannot be practically
achieved by any manual operation.
The Thermo Scientific sample collection and preparation
tool kits offer a unique, complementary solution for XRF
analysis in exploration and mining when used with our
portable XRF equipment.
• Lab-to-field solution, with proper sample collection and preparation in
just minutes!
• Unique solutions, never presented before in a commercially available package
• Overcomes the last barrier to high-performance XRF analysis in the field
• Simple, safe, compact, and rugged tools to meet the demands of field work
Thermo Scientific Direct Rock Sampler (top)
Thermo Scientific 12VDC Hammer Mill
Part of Thermo Fisher Scientific
• Battery operated and weighing less than 14 kg, the tool kits allow a
complete laboratory to be set up anywhere – at the mine, on the back
of a truck, in a tent, or in the field
All the tools of the trade
Direct Rock Sampler Kit
Electric Hammer Mill Kit
The Thermo Scientific Direct Rock Sampler allows the
collection of fine powders from a rock face. The device
can be attached to either an AC (110/220V) or DC
(18-24V) powered commercial angle grinder. The special
diamond cutting blades easily generate a sample by
cutting slots, or even making a line cut, on the rock face
or drill cores. The powder is collected in a sample tube.
This material can then be cupped or pelletized for XRF
analysis. Proper sample collection and preparation can
result in a spatially resolved, quantitative rock-face
analysis in minutes, in the field!
The Thermo Scientific Electric Hammer Mill kit includes
the first 12VDC powered mill on the market. This powerful
device, weighing less than 5 kg, provides rapid milling of
samples and delivers a homogenized, fine powder in just
seconds. This mill operates at 150W at 12VDC, providing
hours of service on conventional automobile batteries.
The jumper-cable-type connectors are designed for
powering the mill directly from the battery posts on
your field vehicle. Rock chip size must be less than
8 mm to feed the mill. Included in the kit is a “Crusher
Tool” to reduce the size of larger rocks.
Rock sampling
Collect sample chips
Crush chips to <8 mm
Sieve crushed
sample and collect
in sieve base
Sample collection
(less than
one minute)
Feed crushed/sieved
sample to mill and collect
powder in sample bag
Compress
sample in
pellet press
Using
Thermo
Scientific
handheld
analyers
Using the
Thermo
Scientific
Niton FXL
analyzer
Insert sample into
pellet press
Insert pellet tube into Field
Mate test stand
Place pellet directly on Niton
FXL head assembly
Analyze sample
Analyze sample
Results
Results
Both kits are complemented by the Thermo Scientific Pellet Press,
which produces solid powder tablets without binder with just one
hammer stroke. Utilizing this tool to prepare a sample is extremely
important when analyzing elements lighter than calcium. It also
improves the precision and accuracy of XRF in general. This unique
sample preparation tool has three benefits:
• Generates a sample with a consistent flat surface and density,
which minimizes matrix effects.
• Requires less than 5 grams of sample, which reduces
sample collection efforts.
Cores can be scanned with the XRF analyzer while crated, and
then samples dive-cut with the Direct Rock Sampler.
• Does not require
sample film,
which reduces
light element
performance.
Sample pellets can then be
analyzed in the Thermo Scientific Field Mate Test Stand. This ultra
compact test stand offers safe and convenient operation without the
need for power.
A sample can be
quickly collected
from the rock face
with the Direct
Rock Sampler.
TOOL KITS
AT-A-GLANCE
Thermo Scientific Direct Rock Sampler Kit
Thermo Scientific Electric Hammer Mill Kit
Direct Rock Sampler Attachment**
Kinematica Polymix 12VDC Hammer Mill
**Grinder not included
Crusher Tool
Stainless Steel Pellet Press with Pellet Sleeves
Stainless Steel Pellet Press with Pellet Sleeves
Pellet Press Reamer
Pellet Press Reamer
Thermo Scientific Field Mate Test Stand
Thermo Scientific Field Mate Test Stand
Field Mate Pellet Sleeve Insert
Field Mate Pellet Sleeve Insert
Sample Collection Vials
Sieve 250μm
Miscellaneous Sample Preparation Accessories
Miscellaneous Sample Preparation Accessories
Product Specifications
The Benefits of Proper
Sample Preparation
REGRESSION Mg % no prep
REGRESSION Mg % passing 0.5 mm
100
100
10
Mg 120sec
Linear (Mg 120sec)
1
Niton
NITON %
Mg Mg
%
10
NITON Mg %
Niton % Mg
The need for preparing samples in the
lab for improved analysis results using
XRF is already proven for both lighter
and heavier elements. The set of tools
we now offer is a tremendous step
forward in our continuous efforts of
bringing the lab into the field.
Mg 120sec
Linear (Mg 120sec)
1
y = 0.5884x + 0.7288
y = 0.6444x + 1.186
R² = 0.4173
R² = 0.9496
0.1
0.1
0.1
1
10
0.1
100
1
Assay %
% MgMgAssay
% Mg – No Sample Preparation
1000
1000
Series2
Ni
120 Sec
Linear (Series2)
NITON Ni ppm
100
Niton Ni ppm
10000
NITONNi
Ni ppm
ppm
Niton
100
REGRESSION Ni ppm 0.5mm
10000
100
Ni 120sec
Linear (Ni 120sec)
10
10
y = 0.9006x + 29.313
y = 0.9372x - 20.488
R² = 0.961
R² = 0.7971
1
1
1
10
100
1000
1
10000
10
100
1000
10000
Ni ASSAY ppm
Ni Assay ppm
% Niton Assay ppm
% Niton Assay ppm
% Ni – No Sample Preparation
% Ni – With Sample Preparation
REGRESSION Fe % no prep
100
100
REGRESSION Fe % passing 0.5mm
REGRESSION Fe % passing 0.5mm
100
10
Linear (Fe% 120sec)
Niton %Fe
Fe% 120sec
NITONNITON
Fe % Fe %
Niton %Fe
NITON Fe %
10
1
10
Fe% 120sec
Linear (Fe% 120sec)
Fe% 120sec
1
Linear (Fe% 120sec)
1
y = 1.0324x - 0.8764
R²y ==1.0324x
0.8994
- 0.8764
R²
10 = 0.8994
100
y = 1.0643x - 1.1386
R² = 0.7594
0.1
0.1
0.1
1
% Fe
FeASSAY
Assay
%
10
100
% Fe – No Sample Preparation
0.1
0.1
0.1
XRF Analyzers
Americas
Europe, Middle East, Africa
and South Africa
Billerica, MA
Munich, Germany
+1 978-670-7460
+49 89 3681 380
[email protected]@thermofisher.com
Asia Pacific
New Territories, Hong Kong
+852 2885 4613
[email protected]
1
1
Fe ASSAY %
10
Fe ASSAY
%
% Fe
Assay
% Fe – With Sample Preparation
© 2012 Thermo Fisher Scientific Inc. All rights reserved. All trademarks are the property of Thermo Fisher Scientific Inc. and its subsidiaries. Specifications,
terms and pricing are subject to change. Not all products are available in all countries. Please consult your local sales representative for details.
N3 1-106 01/2012
10
% Mg – With Sample Preparation
REGRESSION Ni ppm no prep
To discuss your particular applications
and performance requirements, or to
schedule an on-site demonstration and
see for yourself how Thermo Scientific
portable XRF analyzers and accessories
can help save you time and money, please
contact your local Thermo Scientific XRF
analyzer representative or contact us
directly by email at [email protected],
or visit our website at
www.thermoscientific.com/niton
%
% Mg
MgASSAY
Assay
www.thermoscientific.com/niton
100